longtext: 1R3D-pdb

content
HEADER    STRUCTURAL GENOMICS, UNKNOWN FUNCTION   01-OCT-03   1R3D
TITLE     CRYSTAL STRUCTURE OF HYPOTHETICAL PROTEIN VC1974 FROM
TITLE    2 VIBRIO CHOLERAE
COMPND    MOL_ID: 1;
COMPND   2 MOLECULE: CONSERVED HYPOTHETICAL PROTEIN VC1974;
COMPND   3 CHAIN: A;
COMPND   4 ENGINEERED: YES
SOURCE    MOL_ID: 1;
SOURCE   2 ORGANISM_SCIENTIFIC: VIBRIO CHOLERAE;
SOURCE   3 GENE: VC1974;
SOURCE   4 EXPRESSION_SYSTEM: ESCHERICHIA COLI;
SOURCE   5 EXPRESSION_SYSTEM_COMMON: BACTERIA;
SOURCE   6 EXPRESSION_SYSTEM_STRAIN: BL21;
SOURCE   7 EXPRESSION_SYSTEM_VECTOR_TYPE: PLASMID;
SOURCE   8 EXPRESSION_SYSTEM_PLASMID: PET28A DERIVED CUSTOM VECTOR
KEYWDS    STRUCTURAL GENOMICS, HYDROLASE, NYSGRC, NEW YORK STRUCTURAL
KEYWDS   2 GENOMICS RESEARCH CONSORTIUM, PSI, PROTEIN STRUCTURE
KEYWDS   3 INITIATIVE
EXPDTA    X-RAY DIFFRACTION
AUTHOR    J.GORMAN,L.SHAPIRO
REVDAT   1   30-NOV-04 1R3D    0
JRNL        AUTH   J.GORMAN,L.SHAPIRO
JRNL        TITL   STRUCTURAL GENOMICS TARGET NYSGRC-T920 RELATED TO
JRNL        TITL 2 A/B HYDROLASE FOLD.
JRNL        REF    TO BE PUBLISHED
JRNL        REFN
REMARK   1
REMARK   2
REMARK   2 RESOLUTION. 1.90 ANGSTROMS.
REMARK   3
REMARK   3 REFINEMENT.
REMARK   3   PROGRAM     : REFMAC 5.2.0005
REMARK   3   AUTHORS     : MURSHUDOV,VAGIN,DODSON
REMARK   3
REMARK   3    REFINEMENT TARGET : MAXIMUM LIKELIHOOD
REMARK   3
REMARK   3  DATA USED IN REFINEMENT.
REMARK   3   RESOLUTION RANGE HIGH (ANGSTROMS) : 1.90
REMARK   3   RESOLUTION RANGE LOW  (ANGSTROMS) : 20.00
REMARK   3   DATA CUTOFF            (SIGMA(F)) : NULL
REMARK   3   COMPLETENESS FOR RANGE        (%) : 98.2
REMARK   3   NUMBER OF REFLECTIONS             : 20222
REMARK   3
REMARK   3  FIT TO DATA USED IN REFINEMENT.
REMARK   3   CROSS-VALIDATION METHOD          : THROUGHOUT
REMARK   3   FREE R VALUE TEST SET SELECTION  : RANDOM
REMARK   3   R VALUE     (WORKING + TEST SET) : 0.181
REMARK   3   R VALUE            (WORKING SET) : 0.179
REMARK   3   FREE R VALUE                     : 0.216
REMARK   3   FREE R VALUE TEST SET SIZE   (%) : 5.100
REMARK   3   FREE R VALUE TEST SET COUNT      : 1089
REMARK   3
REMARK   3  FIT IN THE HIGHEST RESOLUTION BIN.
REMARK   3   TOTAL NUMBER OF BINS USED           : 20
REMARK   3   BIN RESOLUTION RANGE HIGH           : 1.90
REMARK   3   BIN RESOLUTION RANGE LOW            : 1.95
REMARK   3   REFLECTION IN BIN     (WORKING SET) : 1481
REMARK   3   BIN COMPLETENESS (WORKING+TEST) (%) : 99.30
REMARK   3   BIN R VALUE           (WORKING SET) : 0.1790
REMARK   3   BIN FREE R VALUE SET COUNT          : 70
REMARK   3   BIN FREE R VALUE                    : 0.2000
REMARK   3
REMARK   3  NUMBER OF NON-HYDROGEN ATOMS USED IN REFINEMENT.
REMARK   3   ALL ATOMS                : 2149
REMARK   3
REMARK   3  B VALUES.
REMARK   3   FROM WILSON PLOT           (A**2) : NULL
REMARK   3   MEAN B VALUE      (OVERALL, A**2) : 27.27
REMARK   3   OVERALL ANISOTROPIC B VALUE.
REMARK   3    B11 (A**2) : 0.49000
REMARK   3    B22 (A**2) : 0.49000
REMARK   3    B33 (A**2) : -0.98000
REMARK   3    B12 (A**2) : 0.00000
REMARK   3    B13 (A**2) : 0.00000
REMARK   3    B23 (A**2) : 0.00000
REMARK   3
REMARK   3  ESTIMATED OVERALL COORDINATE ERROR.
REMARK   3   ESU BASED ON R VALUE                            (A): 0.150
REMARK   3   ESU BASED ON FREE R VALUE                       (A): 0.137
REMARK   3   ESU BASED ON MAXIMUM LIKELIHOOD                 (A): 0.085
REMARK   3   ESU FOR B VALUES BASED ON MAXIMUM LIKELIHOOD (A**2): 2.770
REMARK   3
REMARK   3 CORRELATION COEFFICIENTS.
REMARK   3   CORRELATION COEFFICIENT FO-FC      : 0.958
REMARK   3   CORRELATION COEFFICIENT FO-FC FREE : 0.942
REMARK   3
REMARK   3  RMS DEVIATIONS FROM IDEAL VALUES        COUNT    RMS    WEIGHT
REMARK   3   BOND LENGTHS REFINED ATOMS        (A):  2030 ; 0.016 ; 0.021
REMARK   3   BOND LENGTHS OTHERS               (A):  1822 ; 0.001 ; 0.020
REMARK   3   BOND ANGLES REFINED ATOMS   (DEGREES):  2759 ; 1.439 ; 1.932
REMARK   3   BOND ANGLES OTHERS          (DEGREES):  4240 ; 0.829 ; 3.000
REMARK   3   TORSION ANGLES, PERIOD 1    (DEGREES):   255 ; 5.820 ; 5.000
REMARK   3   TORSION ANGLES, PERIOD 2    (DEGREES):    95 ;39.752 ;24.737
REMARK   3   TORSION ANGLES, PERIOD 3    (DEGREES):   329 ;14.429 ;15.000
REMARK   3   TORSION ANGLES, PERIOD 4    (DEGREES):     9 ;20.881 ;15.000
REMARK   3   CHIRAL-CENTER RESTRAINTS       (A**3):   310 ; 0.090 ; 0.200
REMARK   3   GENERAL PLANES REFINED ATOMS      (A):  2282 ; 0.006 ; 0.020
REMARK   3   GENERAL PLANES OTHERS             (A):   387 ; 0.001 ; 0.020
REMARK   3   NON-BONDED CONTACTS REFINED ATOMS (A):   413 ; 0.234 ; 0.200
REMARK   3   NON-BONDED CONTACTS OTHERS        (A):  1770 ; 0.190 ; 0.200
REMARK   3   NON-BONDED TORSION REFINED ATOMS  (A):   977 ; 0.174 ; 0.200
REMARK   3   NON-BONDED TORSION OTHERS         (A):  1145 ; 0.088 ; 0.200
REMARK   3   H-BOND (X...Y) REFINED ATOMS      (A):   119 ; 0.141 ; 0.200
REMARK   3   H-BOND (X...Y) OTHERS             (A):  NULL ;  NULL ;  NULL
REMARK   3   POTENTIAL METAL-ION REFINED ATOMS (A):  NULL ;  NULL ;  NULL
REMARK   3   POTENTIAL METAL-ION OTHERS        (A):  NULL ;  NULL ;  NULL
REMARK   3   SYMMETRY VDW REFINED ATOMS        (A):     7 ; 0.186 ; 0.200
REMARK   3   SYMMETRY VDW OTHERS               (A):    50 ; 0.249 ; 0.200
REMARK   3   SYMMETRY H-BOND REFINED ATOMS     (A):    14 ; 0.136 ; 0.200
REMARK   3   SYMMETRY H-BOND OTHERS            (A):  NULL ;  NULL ;  NULL
REMARK   3
REMARK   3  ISOTROPIC THERMAL FACTOR RESTRAINTS.     COUNT   RMS    WEIGHT
REMARK   3   MAIN-CHAIN BOND REFINED ATOMS  (A**2):  1541 ; 1.385 ; 1.500
REMARK   3   MAIN-CHAIN BOND OTHER ATOMS    (A**2):   523 ; 0.276 ; 1.500
REMARK   3   MAIN-CHAIN ANGLE REFINED ATOMS (A**2):  2038 ; 1.740 ; 2.000
REMARK   3   SIDE-CHAIN BOND REFINED ATOMS  (A**2):   825 ; 3.061 ; 3.000
REMARK   3   SIDE-CHAIN ANGLE REFINED ATOMS (A**2):   721 ; 4.480 ; 4.500
REMARK   3
REMARK   3 ANISOTROPIC THERMAL FACTOR RESTRAINTS.    COUNT   RMS   WEIGHT
REMARK   3   RIGID-BOND RESTRAINTS          (A**2):  NULL ;  NULL ;  NULL
REMARK   3   SPHERICITY; FREE ATOMS         (A**2):  NULL ;  NULL ;  NULL
REMARK   3   SPHERICITY; BONDED ATOMS       (A**2):  NULL ;  NULL ;  NULL
REMARK   3
REMARK   3  NCS RESTRAINTS STATISTICS
REMARK   3   NUMBER OF DIFFERENT NCS GROUPS : 0
REMARK   3
REMARK   3  TLS DETAILS
REMARK   3   NUMBER OF TLS GROUPS  : 0
REMARK   3
REMARK   3  BULK SOLVENT MODELLING.
REMARK   3   METHOD USED : MASK
REMARK   3   PARAMETERS FOR MASK CALCULATION
REMARK   3   VDW PROBE RADIUS   : 1.20
REMARK   3   ION PROBE RADIUS   : 0.80
REMARK   3   SHRINKAGE RADIUS   : 0.80
REMARK   3
REMARK   3  OTHER REFINEMENT REMARKS: HYDROGENS HAVE BEEN ADDED IN THE
REMARK   3  RIDING POSITIONS
REMARK   4
REMARK   4 1R3D COMPLIES WITH FORMAT V. 2.3, 09-JULY-1998
REMARK 100
REMARK 100 THIS ENTRY HAS BEEN PROCESSED BY RCSB ON 02-OCT-2003.
REMARK 100 THE RCSB ID CODE IS RCSB020386.
REMARK 200
REMARK 200 EXPERIMENTAL DETAILS
REMARK 200  EXPERIMENT TYPE                : X-RAY DIFFRACTION
REMARK 200  DATE OF DATA COLLECTION        : 24-AUG-2003
REMARK 200  TEMPERATURE           (KELVIN) : 100.0
REMARK 200  PH                             : 8.00
REMARK 200  NUMBER OF CRYSTALS USED        : 1
REMARK 200
REMARK 200  SYNCHROTRON              (Y/N) : Y
REMARK 200  RADIATION SOURCE               : APS
REMARK 200  BEAMLINE                       : 8BM
REMARK 200  X-RAY GENERATOR MODEL          : NULL
REMARK 200  MONOCHROMATIC OR LAUE    (M/L) : M
REMARK 200  WAVELENGTH OR RANGE        (A) : .978
REMARK 200  MONOCHROMATOR                  : SI 111
REMARK 200  OPTICS                         : NULL
REMARK 200
REMARK 200  DETECTOR TYPE                  : CCD
REMARK 200  DETECTOR MANUFACTURER          : ADSC QUANTUM 315
REMARK 200  INTENSITY-INTEGRATION SOFTWARE : DENZO
REMARK 200  DATA SCALING SOFTWARE          : SCALEPACK
REMARK 200
REMARK 200  NUMBER OF UNIQUE REFLECTIONS   : 21381
REMARK 200  RESOLUTION RANGE HIGH      (A) : 1.900
REMARK 200  RESOLUTION RANGE LOW       (A) : 20.000
REMARK 200  REJECTION CRITERIA  (SIGMA(I)) : -3.000
REMARK 200
REMARK 200 OVERALL.
REMARK 200  COMPLETENESS FOR RANGE     (%) : NULL
REMARK 200  DATA REDUNDANCY                : NULL
REMARK 200  R MERGE                    (I) : 0.08900
REMARK 200  R SYM                      (I) : NULL
REMARK 200   FOR THE DATA SET  : 18.3000
REMARK 200
REMARK 200 IN THE HIGHEST RESOLUTION SHELL.
REMARK 200  HIGHEST RESOLUTION SHELL, RANGE HIGH (A) : 1.90
REMARK 200  HIGHEST RESOLUTION SHELL, RANGE LOW  (A) : 1.97
REMARK 200  COMPLETENESS FOR SHELL     (%) : 99.5
REMARK 200  DATA REDUNDANCY IN SHELL       : NULL
REMARK 200  R MERGE FOR SHELL          (I) : 0.41000
REMARK 200  R SYM FOR SHELL            (I) : NULL
REMARK 200   FOR SHELL         : 6.500
REMARK 200
REMARK 200 DIFFRACTION PROTOCOL: SINGLE WAVELENGTH
REMARK 200 METHOD USED TO DETERMINE THE STRUCTURE: SAD
REMARK 200 SOFTWARE USED: SOLVE
REMARK 200 STARTING MODEL: NULL
REMARK 200
REMARK 200 REMARK: NULL
REMARK 280
REMARK 280 CRYSTAL
REMARK 280 SOLVENT CONTENT, VS   (%): NULL
REMARK 280 MATTHEWS COEFFICIENT, VM (ANGSTROMS**3/DA): NULL
REMARK 280
REMARK 280 CRYSTALLIZATION CONDITIONS: 32% PEG 4000, .1M TRIS PH 8.0, 10%
REMARK 280  ISOPROPANOL, .24M NA ACETATE, VAPOR DIFFUSION, HANGING DROP,
REMARK 280  TEMPERATURE 293K
REMARK 290
REMARK 290 CRYSTALLOGRAPHIC SYMMETRY
REMARK 290 SYMMETRY OPERATORS FOR SPACE GROUP: P 42 21 2
REMARK 290
REMARK 290      SYMOP   SYMMETRY
REMARK 290     NNNMMM   OPERATOR
REMARK 290       1555   X,Y,Z
REMARK 290       2555   -X,-Y,Z
REMARK 290       3555   1/2-Y,1/2+X,1/2+Z
REMARK 290       4555   1/2+Y,1/2-X,1/2+Z
REMARK 290       5555   1/2-X,1/2+Y,1/2-Z
REMARK 290       6555   1/2+X,1/2-Y,1/2-Z
REMARK 290       7555   Y,X,-Z
REMARK 290       8555   -Y,-X,-Z
REMARK 290
REMARK 290     WHERE NNN -> OPERATOR NUMBER
REMARK 290           MMM -> TRANSLATION VECTOR
REMARK 290
REMARK 290 CRYSTALLOGRAPHIC SYMMETRY TRANSFORMATIONS
REMARK 290 THE FOLLOWING TRANSFORMATIONS OPERATE ON THE ATOM/HETATM
REMARK 290 RECORDS IN THIS ENTRY TO PRODUCE CRYSTALLOGRAPHICALLY
REMARK 290 RELATED MOLECULES.
REMARK 290   SMTRY1   1  1.000000  0.000000  0.000000        0.00000
REMARK 290   SMTRY2   1  0.000000  1.000000  0.000000        0.00000
REMARK 290   SMTRY3   1  0.000000  0.000000  1.000000        0.00000
REMARK 290   SMTRY1   2 -1.000000  0.000000  0.000000        0.00000
REMARK 290   SMTRY2   2  0.000000 -1.000000  0.000000        0.00000
REMARK 290   SMTRY3   2  0.000000  0.000000  1.000000        0.00000
REMARK 290   SMTRY1   3  0.000000 -1.000000  0.000000       49.73500
REMARK 290   SMTRY2   3  1.000000  0.000000  0.000000       49.73500
REMARK 290   SMTRY3   3  0.000000  0.000000  1.000000       26.74600
REMARK 290   SMTRY1   4  0.000000  1.000000  0.000000       49.73500
REMARK 290   SMTRY2   4 -1.000000  0.000000  0.000000       49.73500
REMARK 290   SMTRY3   4  0.000000  0.000000  1.000000       26.74600
REMARK 290   SMTRY1   5 -1.000000  0.000000  0.000000       49.73500
REMARK 290   SMTRY2   5  0.000000  1.000000  0.000000       49.73500
REMARK 290   SMTRY3   5  0.000000  0.000000 -1.000000       26.74600
REMARK 290   SMTRY1   6  1.000000  0.000000  0.000000       49.73500
REMARK 290   SMTRY2   6  0.000000 -1.000000  0.000000       49.73500
REMARK 290   SMTRY3   6  0.000000  0.000000 -1.000000       26.74600
REMARK 290   SMTRY1   7  0.000000  1.000000  0.000000        0.00000
REMARK 290   SMTRY2   7  1.000000  0.000000  0.000000        0.00000
REMARK 290   SMTRY3   7  0.000000  0.000000 -1.000000        0.00000
REMARK 290   SMTRY1   8  0.000000 -1.000000  0.000000        0.00000
REMARK 290   SMTRY2   8 -1.000000  0.000000  0.000000        0.00000
REMARK 290   SMTRY3   8  0.000000  0.000000 -1.000000        0.00000
REMARK 290
REMARK 290 REMARK: NULL
REMARK 300
REMARK 300 BIOMOLECULE: 1
REMARK 300 THIS ENTRY CONTAINS THE CRYSTALLOGRAPHIC ASYMMETRIC UNIT
REMARK 300 WHICH CONSISTS OF 1 CHAIN(S). SEE REMARK 350 FOR
REMARK 300 INFORMATION ON GENERATING THE BIOLOGICAL MOLECULE(S).
REMARK 350
REMARK 350 GENERATING THE BIOMOLECULE
REMARK 350 COORDINATES FOR A COMPLETE MULTIMER REPRESENTING THE KNOWN
REMARK 350 BIOLOGICALLY SIGNIFICANT OLIGOMERIZATION STATE OF THE
REMARK 350 MOLECULE CAN BE GENERATED BY APPLYING BIOMT TRANSFORMATIONS
REMARK 350 GIVEN BELOW.  BOTH NON-CRYSTALLOGRAPHIC AND
REMARK 350 CRYSTALLOGRAPHIC OPERATIONS ARE GIVEN.
REMARK 350
REMARK 350 BIOMOLECULE: 1
REMARK 350 APPLY THE FOLLOWING TO CHAINS: A
REMARK 350   BIOMT1   1  1.000000  0.000000  0.000000        0.00000
REMARK 350   BIOMT2   1  0.000000  1.000000  0.000000        0.00000
REMARK 350   BIOMT3   1  0.000000  0.000000  1.000000        0.00000
REMARK 375
REMARK 375 SPECIAL POSITION
REMARK 375 THE FOLLOWING ATOMS ARE FOUND TO BE WITHIN 0.15 ANGSTROMS
REMARK 375 OF A SYMMETRY RELATED ATOM AND ARE ASSUMED TO BE ON SPECIAL
REMARK 375 POSITIONS.
REMARK 375
REMARK 375 ATOM RES CSSEQI
REMARK 375      HOH    23   LIES ON A SPECIAL POSITION.
REMARK 375      HOH    70   LIES ON A SPECIAL POSITION.
REMARK 465
REMARK 465 MISSING RESIDUES
REMARK 465 THE FOLLOWING RESIDUES WERE NOT LOCATED IN THE
REMARK 465 EXPERIMENT. (M=MODEL NUMBER; RES=RESIDUE NAME; C=CHAIN
REMARK 465 IDENTIFIER; SSSEQ=SEQUENCE NUMBER; I=INSERTION CODE.)
REMARK 465
REMARK 465   M RES C SSSEQI
REMARK 465     GLU A    58
REMARK 465     ARG A    59
REMARK 465     HIS A    60
REMARK 465     CYS A    61
REMARK 465     ASP A    62
REMARK 465     ASN A    63
REMARK 465     PHE A    64
REMARK 500
REMARK 500 GEOMETRY AND STEREOCHEMISTRY
REMARK 500 SUBTOPIC: TORSION ANGLES
REMARK 500
REMARK 500 TORSION ANGLES OUTSIDE THE EXPECTED RAMACHANDRAN REGIONS:
REMARK 500 (M=MODEL NUMBER; RES=RESIDUE NAME; C=CHAIN IDENTIFIER;
REMARK 500 SSEQ=SEQUENCE NUMBER; I=INSERTION CODE).
REMARK 500
REMARK 500 STANDARD TABLE:
REMARK 500 FORMAT:(10X,I3,1X,A3,1X,A1,I4,A1,4X,F7.2,3X,F7.2)
REMARK 500
REMARK 500  M RES CSSEQI        PSI       PHI
REMARK 500    PHE A   8      -59.19     79.89
REMARK 900
REMARK 900 RELATED ENTRIES
REMARK 900 RELATED ID: T920   RELATED DB: TARGETDB
DBREF  1R3D A    2   263  GB     15641976 NP_231608        2    263
SEQADV 1R3D SER A    0  GB   15641976            CLONING ARTIFACT
SEQADV 1R3D LEU A    1  GB   15641976            CLONING ARTIFACT
SEQADV 1R3D MSE A   70  GB   15641976  MET    70 MODIFIED RESIDUE
SEQADV 1R3D MSE A   98  GB   15641976  MET    98 MODIFIED RESIDUE
SEQADV 1R3D MSE A  187  GB   15641976  MET   187 MODIFIED RESIDUE
SEQADV 1R3D MSE A  257  GB   15641976  MET   257 MODIFIED RESIDUE
SEQRES   1 A  264  SER LEU LEU SER ASN GLN LEU HIS PHE ALA LYS PRO THR
SEQRES   2 A  264  ALA ARG THR PRO LEU VAL VAL LEU VAL HIS GLY LEU LEU
SEQRES   3 A  264  GLY SER GLY ALA ASP TRP GLN PRO VAL LEU SER HIS LEU
SEQRES   4 A  264  ALA ARG THR GLN CYS ALA ALA LEU THR LEU ASP LEU PRO
SEQRES   5 A  264  GLY HIS GLY THR ASN PRO GLU ARG HIS CYS ASP ASN PHE
SEQRES   6 A  264  ALA GLU ALA VAL GLU MSE ILE GLU GLN THR VAL GLN ALA
SEQRES   7 A  264  HIS VAL THR SER GLU VAL PRO VAL ILE LEU VAL GLY TYR
SEQRES   8 A  264  SER LEU GLY GLY ARG LEU ILE MSE HIS GLY LEU ALA GLN
SEQRES   9 A  264  GLY ALA PHE SER ARG LEU ASN LEU ARG GLY ALA ILE ILE
SEQRES  10 A  264  GLU GLY GLY HIS PHE GLY LEU GLN GLU ASN GLU GLU LYS
SEQRES  11 A  264  ALA ALA ARG TRP GLN HIS ASP GLN GLN TRP ALA GLN ARG
SEQRES  12 A  264  PHE SER GLN GLN PRO ILE GLU HIS VAL LEU SER ASP TRP
SEQRES  13 A  264  TYR GLN GLN ALA VAL PHE SER SER LEU ASN HIS GLU GLN
SEQRES  14 A  264  ARG GLN THR LEU ILE ALA GLN ARG SER ALA ASN LEU GLY
SEQRES  15 A  264  SER SER VAL ALA HIS MSE LEU LEU ALA THR SER LEU ALA
SEQRES  16 A  264  LYS GLN PRO TYR LEU LEU PRO ALA LEU GLN ALA LEU LYS
SEQRES  17 A  264  LEU PRO ILE HIS TYR VAL CYS GLY GLU GLN ASP SER LYS
SEQRES  18 A  264  PHE GLN GLN LEU ALA GLU SER SER GLY LEU SER TYR SER
SEQRES  19 A  264  GLN VAL ALA GLN ALA GLY HIS ASN VAL HIS HIS GLU GLN
SEQRES  20 A  264  PRO GLN ALA PHE ALA LYS ILE VAL GLN ALA MSE ILE HIS
SEQRES  21 A  264  SER ILE ILE ASP
MODRES 1R3D MSE A   70  MET  SELENOMETHIONINE
MODRES 1R3D MSE A   98  MET  SELENOMETHIONINE
MODRES 1R3D MSE A  187  MET  SELENOMETHIONINE
MODRES 1R3D MSE A  257  MET  SELENOMETHIONINE
HET    MSE  A  70       8
HET    MSE  A  98       8
HET    MSE  A 187       8
HET    MSE  A 257       8
HETNAM     MSE SELENOMETHIONINE
FORMUL   1  MSE    4(C5 H11 N1 O2 SE1)
FORMUL   2  HOH   *164(H2 O1)
HELIX    1   1 SER A   27  ASP A   30  5                                   4
HELIX    2   2 TRP A   31  ALA A   39  1                                   9
HELIX    3   3 ALA A   65  ALA A   77  1                                  13
HELIX    4   4 SER A   91  GLY A  104  1                                  14
HELIX    5   5 GLU A  125  GLN A  146  1                                  22
HELIX    6   6 PRO A  147  TYR A  156  1                                  10
HELIX    7   7 GLN A  157  SER A  162  5                                   6
HELIX    8   8 ASN A  165  SER A  177  1                                  13
HELIX    9   9 LEU A  180  THR A  191  1                                  12
HELIX   10  10 SER A  192  GLN A  196  5                                   5
HELIX   11  11 LEU A  199  ALA A  205  1                                   7
HELIX   12  12 ASP A  218  GLY A  229  1                                  12
HELIX   13  13 ASN A  241  GLN A  246  1                                   6
HELIX   14  14 GLN A  246  ILE A  262  1                                  17
SHEET    1   A 7 ASN A   4  HIS A   7  0
SHEET    2   A 7 ALA A  44  LEU A  48 -1  O  ALA A  45   N  HIS A   7
SHEET    3   A 7 LEU A  17  VAL A  21  1  N  LEU A  20   O  LEU A  46
SHEET    4   A 7 PRO A  84  TYR A  90  1  O  ILE A  86   N  VAL A  19
SHEET    5   A 7 ASN A 110  GLU A 117  1  O  ARG A 112   N  VAL A  85
SHEET    6   A 7 ILE A 210  GLY A 215  1  O  VAL A 213   N  ILE A 116
SHEET    7   A 7 SER A 231  VAL A 235  1  O  VAL A 235   N  CYS A 214
CRYST1   99.470   99.470   53.492  90.00  90.00  90.00 P 42 21 2     8
ORIGX1      1.000000  0.000000  0.000000        0.00000
ORIGX2      0.000000  1.000000  0.000000        0.00000
ORIGX3      0.000000  0.000000  1.000000        0.00000
SCALE1      0.010053  0.000000  0.000000        0.00000
SCALE2      0.000000  0.010053  0.000000        0.00000
SCALE3      0.000000  0.000000  0.018694        0.00000
TER    1986      ASP A 263
MASTER      278    0    4   14    7    0    0    6 2149    1   32   21
END