longtext: 1XKL-pdb

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HEADER    STRUCTURAL GENOMICS, UNKNOWN FUNCTION   29-SEP-04   1XKL
TITLE     CRYSTAL STRUCTURE OF SALICYLIC ACID-BINDING PROTEIN 2
TITLE    2 (SABP2) FROM NICOTIANA TABACUM, NESG TARGET AR2241
COMPND    MOL_ID: 1;
COMPND   2 MOLECULE: SALICYLIC ACID-BINDING PROTEIN 2;
COMPND   3 CHAIN: A, B, C, D;
COMPND   4 SYNONYM: SABP2;
COMPND   5 ENGINEERED: YES
SOURCE    MOL_ID: 1;
SOURCE   2 ORGANISM_SCIENTIFIC: NICOTIANA TABACUM;
SOURCE   3 ORGANISM_COMMON: COMMON TOBACCO;
SOURCE   4 GENE: AAR87711;
SOURCE   5 EXPRESSION_SYSTEM: ESCHERICHIA COLI;
SOURCE   6 EXPRESSION_SYSTEM_COMMON: BACTERIA;
SOURCE   7 EXPRESSION_SYSTEM_STRAIN: BL21(DE3)+MAGIC;
SOURCE   8 EXPRESSION_SYSTEM_VECTOR_TYPE: PLASMID;
SOURCE   9 EXPRESSION_SYSTEM_VECTOR: PET21;
SOURCE  10 EXPRESSION_SYSTEM_PLASMID: BL21
KEYWDS    ALPHA-BETA PROTEIN, STRUCTURAL GENOMICS, PROTEIN STRUCTURE
KEYWDS   2 INITIATIVE, PSI, NORTHEAST STRUCTURAL GENOMICS CONSORTIUM,
KEYWDS   3 NESG
EXPDTA    X-RAY DIFFRACTION
AUTHOR    F.FOROUHAR,Y.CHEN,Y.CHIANG,T.B.ACTON,G.T.MONTELIONE,
AUTHOR   2 J.F.HUNT,L.TONG,NORTHEAST STRUCTURAL GENOMICS CONSORTIUM
AUTHOR   3 (NESG)
REVDAT   1   30-NOV-04 1XKL    0
JRNL        AUTH   F.FOROUHAR,Y.CHEN,Y.CHIANG,T.B.ACTON,
JRNL        AUTH 2 G.T.MONTELIONE,J.F.HUNT,L.TONG
JRNL        TITL   CRYSTAL STRUCTURE OF SALICYLIC ACID-BINDING
JRNL        TITL 2 PROTEIN 2 (SABP2) FROM NICOTIANA TABACUM, NESG
JRNL        TITL 3 TARGET AR2241
JRNL        REF    TO BE PUBLISHED
REMARK   1
REMARK   2
REMARK   2 RESOLUTION. 2.00 ANGSTROMS.
REMARK   3
REMARK   3 REFINEMENT.
REMARK   3   PROGRAM     : CNS 1.1
REMARK   3   AUTHORS     : BRUNGER,ADAMS,CLORE,DELANO,GROS,GROSSE-
REMARK   3               : KUNSTLEVE,JIANG,KUSZEWSKI,NILGES, PANNU,
REMARK   3               : READ,RICE,SIMONSON,WARREN
REMARK   3
REMARK   3  REFINEMENT TARGET : ENGH & HUBER
REMARK   3
REMARK   3  DATA USED IN REFINEMENT.
REMARK   3   RESOLUTION RANGE HIGH (ANGSTROMS) : 2.00
REMARK   3   RESOLUTION RANGE LOW  (ANGSTROMS) : 27.15
REMARK   3   DATA CUTOFF            (SIGMA(F)) : 2.000
REMARK   3   DATA CUTOFF HIGH         (ABS(F)) : 347566.890
REMARK   3   DATA CUTOFF LOW          (ABS(F)) : 0.0000
REMARK   3   COMPLETENESS (WORKING+TEST)   (%) : 84.2
REMARK   3   NUMBER OF REFLECTIONS             : 113140
REMARK   3
REMARK   3  FIT TO DATA USED IN REFINEMENT.
REMARK   3   CROSS-VALIDATION METHOD          : THROUGHOUT
REMARK   3   FREE R VALUE TEST SET SELECTION  : RANDOM
REMARK   3   R VALUE            (WORKING SET) : 0.190
REMARK   3   FREE R VALUE                     : 0.234
REMARK   3   FREE R VALUE TEST SET SIZE   (%) : 9.800
REMARK   3   FREE R VALUE TEST SET COUNT      : 11074
REMARK   3   ESTIMATED ERROR OF FREE R VALUE  : 0.002
REMARK   3
REMARK   3  FIT IN THE HIGHEST RESOLUTION BIN.
REMARK   3   TOTAL NUMBER OF BINS USED           : 6
REMARK   3   BIN RESOLUTION RANGE HIGH       (A) : 2.00
REMARK   3   BIN RESOLUTION RANGE LOW        (A) : 2.13
REMARK   3   BIN COMPLETENESS (WORKING+TEST) (%) : 61.70
REMARK   3   REFLECTIONS IN BIN    (WORKING SET) : 12533
REMARK   3   BIN R VALUE           (WORKING SET) : 0.2180
REMARK   3   BIN FREE R VALUE                    : 0.2660
REMARK   3   BIN FREE R VALUE TEST SET SIZE  (%) : 9.40
REMARK   3   BIN FREE R VALUE TEST SET COUNT     : 1295
REMARK   3   ESTIMATED ERROR OF BIN FREE R VALUE : 0.007
REMARK   3
REMARK   3  NUMBER OF NON-HYDROGEN ATOMS USED IN REFINEMENT.
REMARK   3   PROTEIN ATOMS            : 8131
REMARK   3   NUCLEIC ACID ATOMS       : 0
REMARK   3   HETEROGEN ATOMS          : 48
REMARK   3   SOLVENT ATOMS            : 926
REMARK   3
REMARK   3  B VALUES.
REMARK   3   FROM WILSON PLOT           (A**2) : 10.80
REMARK   3   MEAN B VALUE      (OVERALL, A**2) : 25.10
REMARK   3   OVERALL ANISOTROPIC B VALUE.
REMARK   3    B11 (A**2) : -3.02000
REMARK   3    B22 (A**2) : -1.09000
REMARK   3    B33 (A**2) : 4.11000
REMARK   3    B12 (A**2) : 0.00000
REMARK   3    B13 (A**2) : 0.00000
REMARK   3    B23 (A**2) : 0.00000
REMARK   3
REMARK   3  ESTIMATED COORDINATE ERROR.
REMARK   3   ESD FROM LUZZATI PLOT        (A) : 0.21
REMARK   3   ESD FROM SIGMAA              (A) : 0.16
REMARK   3   LOW RESOLUTION CUTOFF        (A) : 5.00
REMARK   3
REMARK   3  CROSS-VALIDATED ESTIMATED COORDINATE ERROR.
REMARK   3   ESD FROM C-V LUZZATI PLOT    (A) : 0.27
REMARK   3   ESD FROM C-V SIGMAA          (A) : 0.21
REMARK   3
REMARK   3  RMS DEVIATIONS FROM IDEAL VALUES.
REMARK   3   BOND LENGTHS                 (A) : 0.006
REMARK   3   BOND ANGLES            (DEGREES) : 1.20
REMARK   3   DIHEDRAL ANGLES        (DEGREES) : 23.00
REMARK   3   IMPROPER ANGLES        (DEGREES) : 0.79
REMARK   3
REMARK   3  ISOTROPIC THERMAL MODEL : OVERALL
REMARK   3
REMARK   3  ISOTROPIC THERMAL FACTOR RESTRAINTS.    RMS    SIGMA
REMARK   3   MAIN-CHAIN BOND              (A**2) : NULL  ; NULL
REMARK   3   MAIN-CHAIN ANGLE             (A**2) : NULL  ; NULL
REMARK   3   SIDE-CHAIN BOND              (A**2) : NULL  ; NULL
REMARK   3   SIDE-CHAIN ANGLE             (A**2) : NULL  ; NULL
REMARK   3
REMARK   3  BULK SOLVENT MODELING.
REMARK   3   METHOD USED : FLAT MODEL
REMARK   3   KSOL        : 0.33
REMARK   3   BSOL        : 41.46
REMARK   3
REMARK   3  NCS MODEL : NULL
REMARK   3
REMARK   3  NCS RESTRAINTS.                         RMS   SIGMA/WEIGHT
REMARK   3   GROUP  1  POSITIONAL            (A) : NULL  ; NULL
REMARK   3   GROUP  1  B-FACTOR           (A**2) : NULL  ; NULL
REMARK   3
REMARK   3  PARAMETER FILE  1  : NULL
REMARK   3  TOPOLOGY FILE  1   : NULL
REMARK   3
REMARK   3  OTHER REFINEMENT REMARKS: NULL
REMARK   4
REMARK   4 1XKL COMPLIES WITH FORMAT V. 2.3, 09-JULY-1998
REMARK 100
REMARK 100 THIS ENTRY HAS BEEN PROCESSED BY RCSB ON 22-OCT-2004.
REMARK 100 THE RCSB ID CODE IS RCSB030460.
REMARK 200
REMARK 200 EXPERIMENTAL DETAILS
REMARK 200  EXPERIMENT TYPE                : X-RAY DIFFRACTION
REMARK 200  DATE OF DATA COLLECTION        : 13-SEP-2003
REMARK 200  TEMPERATURE           (KELVIN) : 100.0
REMARK 200  PH                             : 7.50
REMARK 200  NUMBER OF CRYSTALS USED        : 1
REMARK 200
REMARK 200  SYNCHROTRON              (Y/N) : Y
REMARK 200  RADIATION SOURCE               : NSLS
REMARK 200  BEAMLINE                       : X4A
REMARK 200  X-RAY GENERATOR MODEL          : NULL
REMARK 200  MONOCHROMATIC OR LAUE    (M/L) : M
REMARK 200  WAVELENGTH OR RANGE        (A) : 0.97935
REMARK 200  MONOCHROMATOR                  : SI 111 CHANNEL
REMARK 200  OPTICS                         : MIRRORS
REMARK 200
REMARK 200  DETECTOR TYPE                  : CCD
REMARK 200  DETECTOR MANUFACTURER          : ADSC QUANTUM 4
REMARK 200  INTENSITY-INTEGRATION SOFTWARE : DENZO
REMARK 200  DATA SCALING SOFTWARE          : SCALEPACK
REMARK 200
REMARK 200  NUMBER OF UNIQUE REFLECTIONS   : 131338
REMARK 200  RESOLUTION RANGE HIGH      (A) : 2.000
REMARK 200  RESOLUTION RANGE LOW       (A) : 27.200
REMARK 200  REJECTION CRITERIA  (SIGMA(I)) : 2.000
REMARK 200
REMARK 200 OVERALL.
REMARK 200  COMPLETENESS FOR RANGE     (%) : 96.6
REMARK 200  DATA REDUNDANCY                : 5.600
REMARK 200  R MERGE                    (I) : 0.07500
REMARK 200  R SYM                      (I) : 0.06800
REMARK 200   FOR THE DATA SET  : 19.5000
REMARK 200
REMARK 200 IN THE HIGHEST RESOLUTION SHELL.
REMARK 200  HIGHEST RESOLUTION SHELL, RANGE HIGH (A) : 2.00
REMARK 200  HIGHEST RESOLUTION SHELL, RANGE LOW  (A) : 2.07
REMARK 200  COMPLETENESS FOR SHELL     (%) : 82.2
REMARK 200  DATA REDUNDANCY IN SHELL       : 4.30
REMARK 200  R MERGE FOR SHELL          (I) : 0.29000
REMARK 200  R SYM FOR SHELL            (I) : 0.27800
REMARK 200   FOR SHELL         : 2.900
REMARK 200
REMARK 200 DIFFRACTION PROTOCOL: SINGLE WAVELENGTH
REMARK 200 METHOD USED TO DETERMINE THE STRUCTURE: SAD
REMARK 200 SOFTWARE USED: SNB THEN SOLVE
REMARK 200 STARTING MODEL: NULL
REMARK 200
REMARK 200 REMARK: NULL
REMARK 280
REMARK 280 CRYSTAL
REMARK 280 SOLVENT CONTENT, VS   (%): 41.00
REMARK 280 MATTHEWS COEFFICIENT, VM (ANGSTROMS**3/DA): 2.10
REMARK 280
REMARK 280 CRYSTALLIZATION CONDITIONS: 100 MM HEPES-NAOH, 20% PEG3350, 5
REMARK 280  MM SA, PH 7.5, VAPOR DIFFUSION, HANGING DROP, TEMPERATURE 277 K
REMARK 290
REMARK 290 CRYSTALLOGRAPHIC SYMMETRY
REMARK 290 SYMMETRY OPERATORS FOR SPACE GROUP: P 21 21 2
REMARK 290
REMARK 290      SYMOP   SYMMETRY
REMARK 290     NNNMMM   OPERATOR
REMARK 290       1555   X,Y,Z
REMARK 290       2555   -X,-Y,Z
REMARK 290       3555   1/2-X,1/2+Y,-Z
REMARK 290       4555   1/2+X,1/2-Y,-Z
REMARK 290
REMARK 290     WHERE NNN -> OPERATOR NUMBER
REMARK 290           MMM -> TRANSLATION VECTOR
REMARK 290
REMARK 290 CRYSTALLOGRAPHIC SYMMETRY TRANSFORMATIONS
REMARK 290 THE FOLLOWING TRANSFORMATIONS OPERATE ON THE ATOM/HETATM
REMARK 290 RECORDS IN THIS ENTRY TO PRODUCE CRYSTALLOGRAPHICALLY
REMARK 290 RELATED MOLECULES.
REMARK 290   SMTRY1   1  1.000000  0.000000  0.000000        0.00000
REMARK 290   SMTRY2   1  0.000000  1.000000  0.000000        0.00000
REMARK 290   SMTRY3   1  0.000000  0.000000  1.000000        0.00000
REMARK 290   SMTRY1   2 -1.000000  0.000000  0.000000        0.00000
REMARK 290   SMTRY2   2  0.000000 -1.000000  0.000000        0.00000
REMARK 290   SMTRY3   2  0.000000  0.000000  1.000000        0.00000
REMARK 290   SMTRY1   3 -1.000000  0.000000  0.000000       68.22850
REMARK 290   SMTRY2   3  0.000000  1.000000  0.000000       83.88650
REMARK 290   SMTRY3   3  0.000000  0.000000 -1.000000        0.00000
REMARK 290   SMTRY1   4  1.000000  0.000000  0.000000       68.22850
REMARK 290   SMTRY2   4  0.000000 -1.000000  0.000000       83.88650
REMARK 290   SMTRY3   4  0.000000  0.000000 -1.000000        0.00000
REMARK 290
REMARK 290 REMARK: NULL
REMARK 300
REMARK 300 BIOMOLECULE: 1
REMARK 300 THIS ENTRY CONTAINS THE CRYSTALLOGRAPHIC ASYMMETRIC UNIT
REMARK 300 WHICH CONSISTS OF 4 CHAIN(S). SEE REMARK 350 FOR
REMARK 300 INFORMATION ON GENERATING THE BIOLOGICAL MOLECULE(S).
REMARK 350
REMARK 350 GENERATING THE BIOMOLECULE
REMARK 350 COORDINATES FOR A COMPLETE MULTIMER REPRESENTING THE KNOWN
REMARK 350 BIOLOGICALLY SIGNIFICANT OLIGOMERIZATION STATE OF THE
REMARK 350 MOLECULE CAN BE GENERATED BY APPLYING BIOMT TRANSFORMATIONS
REMARK 350 GIVEN BELOW.  BOTH NON-CRYSTALLOGRAPHIC AND
REMARK 350 CRYSTALLOGRAPHIC OPERATIONS ARE GIVEN.
REMARK 350
REMARK 350 BIOMOLECULE: 1
REMARK 350 APPLY THE FOLLOWING TO CHAINS: A, B, C, D
REMARK 350   BIOMT1   1  1.000000  0.000000  0.000000        0.00000
REMARK 350   BIOMT2   1  0.000000  1.000000  0.000000        0.00000
REMARK 350   BIOMT3   1  0.000000  0.000000  1.000000        0.00000
REMARK 375
REMARK 375 SPECIAL POSITION
REMARK 375 THE FOLLOWING ATOMS ARE FOUND TO BE WITHIN 0.15 ANGSTROMS
REMARK 375 OF A SYMMETRY RELATED ATOM AND ARE ASSUMED TO BE ON SPECIAL
REMARK 375 POSITIONS.
REMARK 375
REMARK 375 ATOM RES CSSEQI
REMARK 375      HOH   878   LIES ON A SPECIAL POSITION.
REMARK 465
REMARK 465 MISSING RESIDUES
REMARK 465 THE FOLLOWING RESIDUES WERE NOT LOCATED IN THE
REMARK 465 EXPERIMENT. (M=MODEL NUMBER; RES=RESIDUE NAME; C=CHAIN
REMARK 465 IDENTIFIER; SSSEQ=SEQUENCE NUMBER; I=INSERTION CODE.)
REMARK 465
REMARK 465   M RES C SSSEQI
REMARK 465     MET A     1
REMARK 465     LYS A     2
REMARK 465     MET A   261
REMARK 465     ALA A   262
REMARK 465     GLY A   263
REMARK 465     ASP A   264
REMARK 465     PRO A   265
REMARK 465     LEU A   266
REMARK 465     GLU A   267
REMARK 465     HIS A   268
REMARK 465     HIS A   269
REMARK 465     HIS A   270
REMARK 465     HIS A   271
REMARK 465     HIS A   272
REMARK 465     HIS A   273
REMARK 465     MET B     1
REMARK 465     LYS B     2
REMARK 465     TYR B   259
REMARK 465     ASN B   260
REMARK 465     MET B   261
REMARK 465     ALA B   262
REMARK 465     GLY B   263
REMARK 465     ASP B   264
REMARK 465     PRO B   265
REMARK 465     LEU B   266
REMARK 465     GLU B   267
REMARK 465     HIS B   268
REMARK 465     HIS B   269
REMARK 465     HIS B   270
REMARK 465     HIS B   271
REMARK 465     HIS B   272
REMARK 465     HIS B   273
REMARK 465     MET C     1
REMARK 465     LYS C     2
REMARK 465     ASN C   260
REMARK 465     MET C   261
REMARK 465     ALA C   262
REMARK 465     GLY C   263
REMARK 465     ASP C   264
REMARK 465     PRO C   265
REMARK 465     LEU C   266
REMARK 465     GLU C   267
REMARK 465     HIS C   268
REMARK 465     HIS C   269
REMARK 465     HIS C   270
REMARK 465     HIS C   271
REMARK 465     HIS C   272
REMARK 465     HIS C   273
REMARK 465     MET D     1
REMARK 465     LYS D     2
REMARK 465     LYS D   190
REMARK 465     MET D   261
REMARK 465     ALA D   262
REMARK 465     GLY D   263
REMARK 465     ASP D   264
REMARK 465     PRO D   265
REMARK 465     LEU D   266
REMARK 465     GLU D   267
REMARK 465     HIS D   268
REMARK 465     HIS D   269
REMARK 465     HIS D   270
REMARK 465     HIS D   271
REMARK 465     HIS D   272
REMARK 465     HIS D   273
REMARK 500
REMARK 500 GEOMETRY AND STEREOCHEMISTRY
REMARK 500 SUBTOPIC: CLOSE CONTACTS
REMARK 500
REMARK 500 THE FOLLOWING ATOMS THAT ARE RELATED BY CRYSTALLOGRAPHIC
REMARK 500 SYMMETRY ARE IN CLOSE CONTACT.  AN ATOM LOCATED WITHIN 0.15
REMARK 500 ANGSTROMS OF A SYMMETRY RELATED ATOM IS ASSUMED TO BE ON A
REMARK 500 SPECIAL POSITION AND IS, THEREFORE, LISTED IN REMARK 375
REMARK 500 INSTEAD OF REMARK 500.  ATOMS WITH NON-BLANK ALTERNATE
REMARK 500 LOCATION INDICATORS ARE NOT INCLUDED IN THE CALCULATIONS.
REMARK 500
REMARK 500 DISTANCE CUTOFF:
REMARK 500 2.2 ANGSTROMS FOR CONTACTS NOT INVOLVING HYDROGEN ATOMS
REMARK 500 1.6 ANGSTROMS FOR CONTACTS INVOLVING HYDROGEN ATOMS
REMARK 500
REMARK 500  ATM1  RES C  SSEQI   ATM2  RES C  SSEQI  SSYMOP   DISTANCE
REMARK 500   O    HOH     917     O    HOH     917     2665     1.30
REMARK 500   O    HOH     918     O    HOH     918     2665     1.51
REMARK 500
REMARK 500 GEOMETRY AND STEREOCHEMISTRY
REMARK 500 SUBTOPIC: COVALENT BOND LENGTHS
REMARK 500
REMARK 500 THE STEREOCHEMICAL PARAMETERS OF THE FOLLOWING RESIDUES
REMARK 500 HAVE VALUES WHICH DEVIATE FROM EXPECTED VALUES BY MORE
REMARK 500 THAN 6*RMSD (M=MODEL NUMBER; RES=RESIDUE NAME; C=CHAIN
REMARK 500 IDENTIFIER; SSEQ=SEQUENCE NUMBER; I=INSERTION CODE).
REMARK 500
REMARK 500 STANDARD TABLE:
REMARK 500 FORMAT: (10X,I3,1X,2(A3,1X,A1,I4,A1,1X,A4,3X),F6.3)
REMARK 500
REMARK 500 EXPECTED VALUES: ENGH AND HUBER, 1991
REMARK 500
REMARK 500  M RES CSSEQI ATM1   RES CSSEQI ATM2   DEVIATION
REMARK 500    SER A  81   N     SER A  81   CA    -0.106
REMARK 500    SER B  81   N     SER B  81   CA    -0.111
REMARK 500    SER C  81   N     SER C  81   CA    -0.116
REMARK 500    SER D  81   N     SER D  81   CA    -0.113
REMARK 500
REMARK 500 GEOMETRY AND STEREOCHEMISTRY
REMARK 500 SUBTOPIC: COVALENT BOND ANGLES
REMARK 500
REMARK 500 THE STEREOCHEMICAL PARAMETERS OF THE FOLLOWING RESIDUES
REMARK 500 HAVE VALUES WHICH DEVIATE FROM EXPECTED VALUES BY MORE
REMARK 500 THAN 6*RMSD (M=MODEL NUMBER; RES=RESIDUE NAME; C=CHAIN
REMARK 500 IDENTIFIER; SSEQ=SEQUENCE NUMBER; I=INSERTION CODE).
REMARK 500
REMARK 500 STANDARD TABLE:
REMARK 500 FORMAT: (10X,I3,1X,A3,1X,A1,I4,A1,3(1X,A4,2X),12X,F5.1)
REMARK 500
REMARK 500 EXPECTED VALUES: ENGH AND HUBER, 1991
REMARK 500
REMARK 500  M RES CSSEQI ATM1   ATM2   ATM3
REMARK 500    ASP A  72   N   -  CA  -  C   ANGL. DEV. = -7.8 DEGREES
REMARK 500    SER A  81   CA  -  CB  -  OG  ANGL. DEV. = 17.2 DEGREES
REMARK 500    PHE A 107   N   -  CA  -  C   ANGL. DEV. = -9.6 DEGREES
REMARK 500    TYR A 191   N   -  CA  -  C   ANGL. DEV. =  7.7 DEGREES
REMARK 500    ILE A 213   N   -  CA  -  C   ANGL. DEV. =-11.4 DEGREES
REMARK 500    SER B  81   CA  -  CB  -  OG  ANGL. DEV. = 17.0 DEGREES
REMARK 500    PHE B 107   N   -  CA  -  C   ANGL. DEV. = -9.7 DEGREES
REMARK 500    LYS B 159   N   -  CA  -  C   ANGL. DEV. =  7.7 DEGREES
REMARK 500    LEU B 175   N   -  CA  -  C   ANGL. DEV. =  7.4 DEGREES
REMARK 500    THR B 208   N   -  CA  -  C   ANGL. DEV. =  7.4 DEGREES
REMARK 500    ILE B 213   N   -  CA  -  C   ANGL. DEV. =-11.1 DEGREES
REMARK 500    ASP C  38   N   -  CA  -  C   ANGL. DEV. = -7.9 DEGREES
REMARK 500    LEU C  39   N   -  CA  -  C   ANGL. DEV. = -7.6 DEGREES
REMARK 500    ILE C  76   N   -  CA  -  C   ANGL. DEV. = -9.0 DEGREES
REMARK 500    SER C  81   CA  -  CB  -  OG  ANGL. DEV. = 17.0 DEGREES
REMARK 500    PHE C 107   N   -  CA  -  C   ANGL. DEV. = -9.6 DEGREES
REMARK 500    CYS C 207   N   -  CA  -  C   ANGL. DEV. = -7.7 DEGREES
REMARK 500    THR C 208   N   -  CA  -  C   ANGL. DEV. =  7.8 DEGREES
REMARK 500    ILE C 213   N   -  CA  -  C   ANGL. DEV. =-11.6 DEGREES
REMARK 500    SER D  81   CA  -  CB  -  OG  ANGL. DEV. = 16.8 DEGREES
REMARK 500    PHE D 107   N   -  CA  -  C   ANGL. DEV. = -9.9 DEGREES
REMARK 500    ILE D 213   N   -  CA  -  C   ANGL. DEV. = -9.4 DEGREES
REMARK 500
REMARK 500 GEOMETRY AND STEREOCHEMISTRY
REMARK 500 SUBTOPIC: TORSION ANGLES
REMARK 500
REMARK 500 TORSION ANGLES OUTSIDE THE EXPECTED RAMACHANDRAN REGIONS:
REMARK 500 (M=MODEL NUMBER; RES=RESIDUE NAME; C=CHAIN IDENTIFIER;
REMARK 500 SSEQ=SEQUENCE NUMBER; I=INSERTION CODE).
REMARK 500
REMARK 500 STANDARD TABLE:
REMARK 500 FORMAT:(10X,I3,1X,A3,1X,A1,I4,A1,4X,F7.2,3X,F7.2)
REMARK 500
REMARK 500  M RES CSSEQI        PSI       PHI
REMARK 500    ALA A  71      -30.93     76.68
REMARK 500    LEU B 132     -116.11     54.58
REMARK 500    LEU C 132     -119.87     51.71
REMARK 525
REMARK 525 SOLVENT
REMARK 525 THE FOLLOWING SOLVENT MOLECULES LIE FARTHER THAN EXPECTED
REMARK 525 FROM THE PROTEIN OR NUCLEIC ACID MOLECULE AND MAY BE
REMARK 525 ASSOCIATED WITH A SYMMETRY RELATED MOLECULE (M=MODEL
REMARK 525 NUMBER; RES=RESIDUE NAME; C=CHAIN IDENTIFIER; SSEQ=SEQUENCE
REMARK 525 NUMBER; I=INSERTION CODE):
REMARK 525
REMARK 525  M RES CSSEQI
REMARK 525    HOH   583        DISTANCE =  5.04 ANGSTROMS
REMARK 525    HOH   621        DISTANCE =  5.85 ANGSTROMS
REMARK 525    HOH   705        DISTANCE =  6.15 ANGSTROMS
REMARK 900
REMARK 900 RELATED ENTRIES
REMARK 900 RELATED ID: AR2241   RELATED DB: TARGETDB
DBREF  1XKL A    1   260  GB     40549303 AAR87711         1    260
DBREF  1XKL B    1   260  GB     40549303 AAR87711         1    260
DBREF  1XKL C    1   260  GB     40549303 AAR87711         1    260
DBREF  1XKL D    1   260  GB     40549303 AAR87711         1    260
SEQADV 1XKL MSE A   63  GB   40549303  MET    63 MODIFIED RESIDUE
SEQADV 1XKL MSE A   66  GB   40549303  MET    66 MODIFIED RESIDUE
SEQADV 1XKL MSE A   85  GB   40549303  MET    85 MODIFIED RESIDUE
SEQADV 1XKL MSE A   91  GB   40549303  MET    91 MODIFIED RESIDUE
SEQADV 1XKL MSE A  108  GB   40549303  MET   108 MODIFIED RESIDUE
SEQADV 1XKL MSE A  149  GB   40549303  MET   149 MODIFIED RESIDUE
SEQADV 1XKL MSE A  183  GB   40549303  MET   183 MODIFIED RESIDUE
SEQADV 1XKL MSE A  239  GB   40549303  MET   239 MODIFIED RESIDUE
SEQADV 1XKL MSE A  241  GB   40549303  MET   241 MODIFIED RESIDUE
SEQADV 1XKL MET A  261  GB   40549303            CLONING ARTIFACT
SEQADV 1XKL ALA A  262  GB   40549303            CLONING ARTIFACT
SEQADV 1XKL GLY A  263  GB   40549303            CLONING ARTIFACT
SEQADV 1XKL ASP A  264  GB   40549303            CLONING ARTIFACT
SEQADV 1XKL PRO A  265  GB   40549303            CLONING ARTIFACT
SEQADV 1XKL LEU A  266  GB   40549303            CLONING ARTIFACT
SEQADV 1XKL GLU A  267  GB   40549303            CLONING ARTIFACT
SEQADV 1XKL HIS A  268  GB   40549303            HIS TAG
SEQADV 1XKL HIS A  269  GB   40549303            HIS TAG
SEQADV 1XKL HIS A  270  GB   40549303            HIS TAG
SEQADV 1XKL HIS A  271  GB   40549303            HIS TAG
SEQADV 1XKL HIS A  272  GB   40549303            HIS TAG
SEQADV 1XKL HIS A  273  GB   40549303            HIS TAG
SEQADV 1XKL MSE B   63  GB   40549303  MET    63 MODIFIED RESIDUE
SEQADV 1XKL MSE B   66  GB   40549303  MET    66 MODIFIED RESIDUE
SEQADV 1XKL MSE B   85  GB   40549303  MET    85 MODIFIED RESIDUE
SEQADV 1XKL MSE B   91  GB   40549303  MET    91 MODIFIED RESIDUE
SEQADV 1XKL MSE B  108  GB   40549303  MET   108 MODIFIED RESIDUE
SEQADV 1XKL MSE B  149  GB   40549303  MET   149 MODIFIED RESIDUE
SEQADV 1XKL MSE B  183  GB   40549303  MET   183 MODIFIED RESIDUE
SEQADV 1XKL MSE B  239  GB   40549303  MET   239 MODIFIED RESIDUE
SEQADV 1XKL MSE B  241  GB   40549303  MET   241 MODIFIED RESIDUE
SEQADV 1XKL MET B  261  GB   40549303            CLONING ARTIFACT
SEQADV 1XKL ALA B  262  GB   40549303            CLONING ARTIFACT
SEQADV 1XKL GLY B  263  GB   40549303            CLONING ARTIFACT
SEQADV 1XKL ASP B  264  GB   40549303            CLONING ARTIFACT
SEQADV 1XKL PRO B  265  GB   40549303            CLONING ARTIFACT
SEQADV 1XKL LEU B  266  GB   40549303            CLONING ARTIFACT
SEQADV 1XKL GLU B  267  GB   40549303            CLONING ARTIFACT
SEQADV 1XKL HIS B  268  GB   40549303            HIS TAG
SEQADV 1XKL HIS B  269  GB   40549303            HIS TAG
SEQADV 1XKL HIS B  270  GB   40549303            HIS TAG
SEQADV 1XKL HIS B  271  GB   40549303            HIS TAG
SEQADV 1XKL HIS B  272  GB   40549303            HIS TAG
SEQADV 1XKL HIS B  273  GB   40549303            HIS TAG
SEQADV 1XKL MSE C   63  GB   40549303  MET    63 MODIFIED RESIDUE
SEQADV 1XKL MSE C   66  GB   40549303  MET    66 MODIFIED RESIDUE
SEQADV 1XKL MSE C   85  GB   40549303  MET    85 MODIFIED RESIDUE
SEQADV 1XKL MSE C   91  GB   40549303  MET    91 MODIFIED RESIDUE
SEQADV 1XKL MSE C  108  GB   40549303  MET   108 MODIFIED RESIDUE
SEQADV 1XKL MSE C  149  GB   40549303  MET   149 MODIFIED RESIDUE
SEQADV 1XKL MSE C  183  GB   40549303  MET   183 MODIFIED RESIDUE
SEQADV 1XKL MSE C  239  GB   40549303  MET   239 MODIFIED RESIDUE
SEQADV 1XKL MSE C  241  GB   40549303  MET   241 MODIFIED RESIDUE
SEQADV 1XKL MET C  261  GB   40549303            CLONING ARTIFACT
SEQADV 1XKL ALA C  262  GB   40549303            CLONING ARTIFACT
SEQADV 1XKL GLY C  263  GB   40549303            CLONING ARTIFACT
SEQADV 1XKL ASP C  264  GB   40549303            CLONING ARTIFACT
SEQADV 1XKL PRO C  265  GB   40549303            CLONING ARTIFACT
SEQADV 1XKL LEU C  266  GB   40549303            CLONING ARTIFACT
SEQADV 1XKL GLU C  267  GB   40549303            CLONING ARTIFACT
SEQADV 1XKL HIS C  268  GB   40549303            HIS TAG
SEQADV 1XKL HIS C  269  GB   40549303            HIS TAG
SEQADV 1XKL HIS C  270  GB   40549303            HIS TAG
SEQADV 1XKL HIS C  271  GB   40549303            HIS TAG
SEQADV 1XKL HIS C  272  GB   40549303            HIS TAG
SEQADV 1XKL HIS C  273  GB   40549303            HIS TAG
SEQADV 1XKL MSE D   63  GB   40549303  MET    63 MODIFIED RESIDUE
SEQADV 1XKL MSE D   66  GB   40549303  MET    66 MODIFIED RESIDUE
SEQADV 1XKL MSE D   85  GB   40549303  MET    85 MODIFIED RESIDUE
SEQADV 1XKL MSE D   91  GB   40549303  MET    91 MODIFIED RESIDUE
SEQADV 1XKL MSE D  108  GB   40549303  MET   108 MODIFIED RESIDUE
SEQADV 1XKL MSE D  149  GB   40549303  MET   149 MODIFIED RESIDUE
SEQADV 1XKL MSE D  183  GB   40549303  MET   183 MODIFIED RESIDUE
SEQADV 1XKL MSE D  239  GB   40549303  MET   239 MODIFIED RESIDUE
SEQADV 1XKL MSE D  241  GB   40549303  MET   241 MODIFIED RESIDUE
SEQADV 1XKL MET D  261  GB   40549303            CLONING ARTIFACT
SEQADV 1XKL ALA D  262  GB   40549303            CLONING ARTIFACT
SEQADV 1XKL GLY D  263  GB   40549303            CLONING ARTIFACT
SEQADV 1XKL ASP D  264  GB   40549303            CLONING ARTIFACT
SEQADV 1XKL PRO D  265  GB   40549303            CLONING ARTIFACT
SEQADV 1XKL LEU D  266  GB   40549303            CLONING ARTIFACT
SEQADV 1XKL GLU D  267  GB   40549303            CLONING ARTIFACT
SEQADV 1XKL HIS D  268  GB   40549303            HIS TAG
SEQADV 1XKL HIS D  269  GB   40549303            HIS TAG
SEQADV 1XKL HIS D  270  GB   40549303            HIS TAG
SEQADV 1XKL HIS D  271  GB   40549303            HIS TAG
SEQADV 1XKL HIS D  272  GB   40549303            HIS TAG
SEQADV 1XKL HIS D  273  GB   40549303            HIS TAG
SEQRES   1 A  273  MET LYS GLU GLY LYS HIS PHE VAL LEU VAL HIS GLY ALA
SEQRES   2 A  273  CYS HIS GLY GLY TRP SER TRP TYR LYS LEU LYS PRO LEU
SEQRES   3 A  273  LEU GLU ALA ALA GLY HIS LYS VAL THR ALA LEU ASP LEU
SEQRES   4 A  273  ALA ALA SER GLY THR ASP LEU ARG LYS ILE GLU GLU LEU
SEQRES   5 A  273  ARG THR LEU TYR ASP TYR THR LEU PRO LEU MSE GLU LEU
SEQRES   6 A  273  MSE GLU SER LEU SER ALA ASP GLU LYS VAL ILE LEU VAL
SEQRES   7 A  273  GLY HIS SER LEU GLY GLY MSE ASN LEU GLY LEU ALA MSE
SEQRES   8 A  273  GLU LYS TYR PRO GLN LYS ILE TYR ALA ALA VAL PHE LEU
SEQRES   9 A  273  ALA ALA PHE MSE PRO ASP SER VAL HIS ASN SER SER PHE
SEQRES  10 A  273  VAL LEU GLU GLN TYR ASN GLU ARG THR PRO ALA GLU ASN
SEQRES  11 A  273  TRP LEU ASP THR GLN PHE LEU PRO TYR GLY SER PRO GLU
SEQRES  12 A  273  GLU PRO LEU THR SER MSE PHE PHE GLY PRO LYS PHE LEU
SEQRES  13 A  273  ALA HIS LYS LEU TYR GLN LEU CYS SER PRO GLU ASP LEU
SEQRES  14 A  273  ALA LEU ALA SER SER LEU VAL ARG PRO SER SER LEU PHE
SEQRES  15 A  273  MSE GLU ASP LEU SER LYS ALA LYS TYR PHE THR ASP GLU
SEQRES  16 A  273  ARG PHE GLY SER VAL LYS ARG VAL TYR ILE VAL CYS THR
SEQRES  17 A  273  GLU ASP LYS GLY ILE PRO GLU GLU PHE GLN ARG TRP GLN
SEQRES  18 A  273  ILE ASP ASN ILE GLY VAL THR GLU ALA ILE GLU ILE LYS
SEQRES  19 A  273  GLY ALA ASP HIS MSE ALA MSE LEU CYS GLU PRO GLN LYS
SEQRES  20 A  273  LEU CYS ALA SER LEU LEU GLU ILE ALA HIS LYS TYR ASN
SEQRES  21 A  273  MET ALA GLY ASP PRO LEU GLU HIS HIS HIS HIS HIS HIS
SEQRES   1 B  273  MET LYS GLU GLY LYS HIS PHE VAL LEU VAL HIS GLY ALA
SEQRES   2 B  273  CYS HIS GLY GLY TRP SER TRP TYR LYS LEU LYS PRO LEU
SEQRES   3 B  273  LEU GLU ALA ALA GLY HIS LYS VAL THR ALA LEU ASP LEU
SEQRES   4 B  273  ALA ALA SER GLY THR ASP LEU ARG LYS ILE GLU GLU LEU
SEQRES   5 B  273  ARG THR LEU TYR ASP TYR THR LEU PRO LEU MSE GLU LEU
SEQRES   6 B  273  MSE GLU SER LEU SER ALA ASP GLU LYS VAL ILE LEU VAL
SEQRES   7 B  273  GLY HIS SER LEU GLY GLY MSE ASN LEU GLY LEU ALA MSE
SEQRES   8 B  273  GLU LYS TYR PRO GLN LYS ILE TYR ALA ALA VAL PHE LEU
SEQRES   9 B  273  ALA ALA PHE MSE PRO ASP SER VAL HIS ASN SER SER PHE
SEQRES  10 B  273  VAL LEU GLU GLN TYR ASN GLU ARG THR PRO ALA GLU ASN
SEQRES  11 B  273  TRP LEU ASP THR GLN PHE LEU PRO TYR GLY SER PRO GLU
SEQRES  12 B  273  GLU PRO LEU THR SER MSE PHE PHE GLY PRO LYS PHE LEU
SEQRES  13 B  273  ALA HIS LYS LEU TYR GLN LEU CYS SER PRO GLU ASP LEU
SEQRES  14 B  273  ALA LEU ALA SER SER LEU VAL ARG PRO SER SER LEU PHE
SEQRES  15 B  273  MSE GLU ASP LEU SER LYS ALA LYS TYR PHE THR ASP GLU
SEQRES  16 B  273  ARG PHE GLY SER VAL LYS ARG VAL TYR ILE VAL CYS THR
SEQRES  17 B  273  GLU ASP LYS GLY ILE PRO GLU GLU PHE GLN ARG TRP GLN
SEQRES  18 B  273  ILE ASP ASN ILE GLY VAL THR GLU ALA ILE GLU ILE LYS
SEQRES  19 B  273  GLY ALA ASP HIS MSE ALA MSE LEU CYS GLU PRO GLN LYS
SEQRES  20 B  273  LEU CYS ALA SER LEU LEU GLU ILE ALA HIS LYS TYR ASN
SEQRES  21 B  273  MET ALA GLY ASP PRO LEU GLU HIS HIS HIS HIS HIS HIS
SEQRES   1 C  273  MET LYS GLU GLY LYS HIS PHE VAL LEU VAL HIS GLY ALA
SEQRES   2 C  273  CYS HIS GLY GLY TRP SER TRP TYR LYS LEU LYS PRO LEU
SEQRES   3 C  273  LEU GLU ALA ALA GLY HIS LYS VAL THR ALA LEU ASP LEU
SEQRES   4 C  273  ALA ALA SER GLY THR ASP LEU ARG LYS ILE GLU GLU LEU
SEQRES   5 C  273  ARG THR LEU TYR ASP TYR THR LEU PRO LEU MSE GLU LEU
SEQRES   6 C  273  MSE GLU SER LEU SER ALA ASP GLU LYS VAL ILE LEU VAL
SEQRES   7 C  273  GLY HIS SER LEU GLY GLY MSE ASN LEU GLY LEU ALA MSE
SEQRES   8 C  273  GLU LYS TYR PRO GLN LYS ILE TYR ALA ALA VAL PHE LEU
SEQRES   9 C  273  ALA ALA PHE MSE PRO ASP SER VAL HIS ASN SER SER PHE
SEQRES  10 C  273  VAL LEU GLU GLN TYR ASN GLU ARG THR PRO ALA GLU ASN
SEQRES  11 C  273  TRP LEU ASP THR GLN PHE LEU PRO TYR GLY SER PRO GLU
SEQRES  12 C  273  GLU PRO LEU THR SER MSE PHE PHE GLY PRO LYS PHE LEU
SEQRES  13 C  273  ALA HIS LYS LEU TYR GLN LEU CYS SER PRO GLU ASP LEU
SEQRES  14 C  273  ALA LEU ALA SER SER LEU VAL ARG PRO SER SER LEU PHE
SEQRES  15 C  273  MSE GLU ASP LEU SER LYS ALA LYS TYR PHE THR ASP GLU
SEQRES  16 C  273  ARG PHE GLY SER VAL LYS ARG VAL TYR ILE VAL CYS THR
SEQRES  17 C  273  GLU ASP LYS GLY ILE PRO GLU GLU PHE GLN ARG TRP GLN
SEQRES  18 C  273  ILE ASP ASN ILE GLY VAL THR GLU ALA ILE GLU ILE LYS
SEQRES  19 C  273  GLY ALA ASP HIS MSE ALA MSE LEU CYS GLU PRO GLN LYS
SEQRES  20 C  273  LEU CYS ALA SER LEU LEU GLU ILE ALA HIS LYS TYR ASN
SEQRES  21 C  273  MET ALA GLY ASP PRO LEU GLU HIS HIS HIS HIS HIS HIS
SEQRES   1 D  273  MET LYS GLU GLY LYS HIS PHE VAL LEU VAL HIS GLY ALA
SEQRES   2 D  273  CYS HIS GLY GLY TRP SER TRP TYR LYS LEU LYS PRO LEU
SEQRES   3 D  273  LEU GLU ALA ALA GLY HIS LYS VAL THR ALA LEU ASP LEU
SEQRES   4 D  273  ALA ALA SER GLY THR ASP LEU ARG LYS ILE GLU GLU LEU
SEQRES   5 D  273  ARG THR LEU TYR ASP TYR THR LEU PRO LEU MSE GLU LEU
SEQRES   6 D  273  MSE GLU SER LEU SER ALA ASP GLU LYS VAL ILE LEU VAL
SEQRES   7 D  273  GLY HIS SER LEU GLY GLY MSE ASN LEU GLY LEU ALA MSE
SEQRES   8 D  273  GLU LYS TYR PRO GLN LYS ILE TYR ALA ALA VAL PHE LEU
SEQRES   9 D  273  ALA ALA PHE MSE PRO ASP SER VAL HIS ASN SER SER PHE
SEQRES  10 D  273  VAL LEU GLU GLN TYR ASN GLU ARG THR PRO ALA GLU ASN
SEQRES  11 D  273  TRP LEU ASP THR GLN PHE LEU PRO TYR GLY SER PRO GLU
SEQRES  12 D  273  GLU PRO LEU THR SER MSE PHE PHE GLY PRO LYS PHE LEU
SEQRES  13 D  273  ALA HIS LYS LEU TYR GLN LEU CYS SER PRO GLU ASP LEU
SEQRES  14 D  273  ALA LEU ALA SER SER LEU VAL ARG PRO SER SER LEU PHE
SEQRES  15 D  273  MSE GLU ASP LEU SER LYS ALA LYS TYR PHE THR ASP GLU
SEQRES  16 D  273  ARG PHE GLY SER VAL LYS ARG VAL TYR ILE VAL CYS THR
SEQRES  17 D  273  GLU ASP LYS GLY ILE PRO GLU GLU PHE GLN ARG TRP GLN
SEQRES  18 D  273  ILE ASP ASN ILE GLY VAL THR GLU ALA ILE GLU ILE LYS
SEQRES  19 D  273  GLY ALA ASP HIS MSE ALA MSE LEU CYS GLU PRO GLN LYS
SEQRES  20 D  273  LEU CYS ALA SER LEU LEU GLU ILE ALA HIS LYS TYR ASN
SEQRES  21 D  273  MET ALA GLY ASP PRO LEU GLU HIS HIS HIS HIS HIS HIS
MODRES 1XKL MSE A   63  MET  SELENOMETHIONINE
MODRES 1XKL MSE A   66  MET  SELENOMETHIONINE
MODRES 1XKL MSE A   85  MET  SELENOMETHIONINE
MODRES 1XKL MSE A   91  MET  SELENOMETHIONINE
MODRES 1XKL MSE A  108  MET  SELENOMETHIONINE
MODRES 1XKL MSE A  149  MET  SELENOMETHIONINE
MODRES 1XKL MSE A  183  MET  SELENOMETHIONINE
MODRES 1XKL MSE A  239  MET  SELENOMETHIONINE
MODRES 1XKL MSE A  241  MET  SELENOMETHIONINE
MODRES 1XKL MSE B   63  MET  SELENOMETHIONINE
MODRES 1XKL MSE B   66  MET  SELENOMETHIONINE
MODRES 1XKL MSE B   85  MET  SELENOMETHIONINE
MODRES 1XKL MSE B   91  MET  SELENOMETHIONINE
MODRES 1XKL MSE B  108  MET  SELENOMETHIONINE
MODRES 1XKL MSE B  149  MET  SELENOMETHIONINE
MODRES 1XKL MSE B  183  MET  SELENOMETHIONINE
MODRES 1XKL MSE B  239  MET  SELENOMETHIONINE
MODRES 1XKL MSE B  241  MET  SELENOMETHIONINE
MODRES 1XKL MSE C   63  MET  SELENOMETHIONINE
MODRES 1XKL MSE C   66  MET  SELENOMETHIONINE
MODRES 1XKL MSE C   85  MET  SELENOMETHIONINE
MODRES 1XKL MSE C   91  MET  SELENOMETHIONINE
MODRES 1XKL MSE C  108  MET  SELENOMETHIONINE
MODRES 1XKL MSE C  149  MET  SELENOMETHIONINE
MODRES 1XKL MSE C  183  MET  SELENOMETHIONINE
MODRES 1XKL MSE C  239  MET  SELENOMETHIONINE
MODRES 1XKL MSE C  241  MET  SELENOMETHIONINE
MODRES 1XKL MSE D   63  MET  SELENOMETHIONINE
MODRES 1XKL MSE D   66  MET  SELENOMETHIONINE
MODRES 1XKL MSE D   85  MET  SELENOMETHIONINE
MODRES 1XKL MSE D   91  MET  SELENOMETHIONINE
MODRES 1XKL MSE D  108  MET  SELENOMETHIONINE
MODRES 1XKL MSE D  149  MET  SELENOMETHIONINE
MODRES 1XKL MSE D  183  MET  SELENOMETHIONINE
MODRES 1XKL MSE D  239  MET  SELENOMETHIONINE
MODRES 1XKL MSE D  241  MET  SELENOMETHIONINE
HET    MSE  A  63       8
HET    MSE  A  66       8
HET    MSE  A  85       8
HET    MSE  A  91       8
HET    MSE  A 108       8
HET    MSE  A 149       8
HET    MSE  A 183       8
HET    MSE  A 239       8
HET    MSE  A 241       8
HET    MSE  B  63       8
HET    MSE  B  66       8
HET    MSE  B  85       8
HET    MSE  B  91       8
HET    MSE  B 108       8
HET    MSE  B 149       8
HET    MSE  B 183       8
HET    MSE  B 239       8
HET    MSE  B 241       8
HET    MSE  C  63       8
HET    MSE  C  66       8
HET    MSE  C  85       8
HET    MSE  C  91       8
HET    MSE  C 108       8
HET    MSE  C 149       8
HET    MSE  C 183       8
HET    MSE  C 239       8
HET    MSE  C 241       8
HET    MSE  D  63       8
HET    MSE  D  66       8
HET    MSE  D  85       8
HET    MSE  D  91       8
HET    MSE  D 108       8
HET    MSE  D 149       8
HET    MSE  D 183       8
HET    MSE  D 239       8
HET    MSE  D 241       8
HET    STH  A 297      12
HET    STH  B 298      12
HET    STH  C 299      12
HET    STH  D 300      12
HETNAM     MSE SELENOMETHIONINE
HETNAM     STH 2-AMINO-4H-1,3-BENZOXATHIIN-4-OL
FORMUL   1  MSE    36(C5 H11 N1 O2 SE1)
FORMUL   5  STH    4(C8 H9 N1 O2 S1)
FORMUL   9  HOH   *926(H2 O1)
HELIX    1   1 GLY A   16  TYR A   21  5                                   6
HELIX    2   2 LYS A   22  ALA A   30  1                                   9
HELIX    3   3 LYS A   48  LEU A   52  5                                   5
HELIX    4   4 THR A   54  SER A   68  1                                  15
HELIX    5   5 LEU A   82  TYR A   94  1                                  13
HELIX    6   6 SER A  116  ARG A  125  1                                  10
HELIX    7   7 GLY A  152  LEU A  160  1                                   9
HELIX    8   8 SER A  165  VAL A  176  1                                  12
HELIX    9   9 PHE A  182  ALA A  189  1                                   8
HELIX   10  10 ARG A  196  VAL A  200  5                                   5
HELIX   11  11 PRO A  214  GLY A  226  1                                  13
HELIX   12  12 MSE A  239  GLU A  244  1                                   6
HELIX   13  13 GLU A  244  TYR A  259  1                                  16
HELIX   14  14 GLY B   16  TYR B   21  5                                   6
HELIX   15  15 LYS B   22  ALA B   30  1                                   9
HELIX   16  16 LYS B   48  LEU B   52  5                                   5
HELIX   17  17 THR B   54  SER B   68  1                                  15
HELIX   18  18 LEU B   82  TYR B   94  1                                  13
HELIX   19  19 SER B  116  THR B  126  1                                  11
HELIX   20  20 PRO B  127  LEU B  132  5                                   6
HELIX   21  21 GLY B  152  LEU B  160  1                                   9
HELIX   22  22 SER B  165  VAL B  176  1                                  12
HELIX   23  23 PHE B  182  ALA B  189  1                                   8
HELIX   24  24 ARG B  196  VAL B  200  5                                   5
HELIX   25  25 PRO B  214  GLY B  226  1                                  13
HELIX   26  26 MSE B  239  GLU B  244  1                                   6
HELIX   27  27 GLU B  244  ILE B  255  1                                  12
HELIX   28  28 GLY C   16  TYR C   21  5                                   6
HELIX   29  29 LYS C   22  ALA C   30  1                                   9
HELIX   30  30 LYS C   48  LEU C   52  5                                   5
HELIX   31  31 THR C   54  LEU C   69  1                                  16
HELIX   32  32 LEU C   82  TYR C   94  1                                  13
HELIX   33  33 SER C  116  THR C  126  1                                  11
HELIX   34  34 PRO C  127  LEU C  132  5                                   6
HELIX   35  35 GLY C  152  LEU C  160  1                                   9
HELIX   36  36 SER C  165  VAL C  176  1                                  12
HELIX   37  37 PHE C  182  LYS C  188  1                                   7
HELIX   38  38 ARG C  196  VAL C  200  5                                   5
HELIX   39  39 PRO C  214  GLY C  226  1                                  13
HELIX   40  40 MSE C  239  GLU C  244  1                                   6
HELIX   41  41 GLU C  244  ALA C  256  1                                  13
HELIX   42  42 GLY D   16  TYR D   21  5                                   6
HELIX   43  43 LEU D   23  ALA D   30  1                                   8
HELIX   44  44 LYS D   48  LEU D   52  5                                   5
HELIX   45  45 THR D   54  LEU D   69  1                                  16
HELIX   46  46 LEU D   82  TYR D   94  1                                  13
HELIX   47  47 SER D  116  ARG D  125  1                                  10
HELIX   48  48 PRO D  127  LEU D  132  5                                   6
HELIX   49  49 GLY D  152  LEU D  160  1                                   9
HELIX   50  50 SER D  165  VAL D  176  1                                  12
HELIX   51  51 PHE D  182  SER D  187  1                                   6
HELIX   52  52 ARG D  196  VAL D  200  5                                   5
HELIX   53  53 PRO D  214  ILE D  225  1                                  12
HELIX   54  54 MSE D  239  GLU D  244  1                                   6
HELIX   55  55 GLU D  244  TYR D  259  1                                  16
SHEET    1   A 6 LYS A  33  ALA A  36  0
SHEET    2   A 6 HIS A   6  VAL A  10  1  N  PHE A   7   O  LYS A  33
SHEET    3   A 6 VAL A  75  HIS A  80  1  O  VAL A  78   N  VAL A  10
SHEET    4   A 6 ILE A  98  LEU A 104  1  O  VAL A 102   N  LEU A  77
SHEET    5   A 6 ARG A 202  CYS A 207  1  O  VAL A 203   N  PHE A 103
SHEET    6   A 6 GLU A 229  ILE A 233  1  O  ILE A 233   N  VAL A 206
SHEET    1   B 2 GLN A 135  PRO A 138  0
SHEET    2   B 2 THR A 147  PHE A 150 -1  O  SER A 148   N  LEU A 137
SHEET    1   C 6 LYS B  33  ALA B  36  0
SHEET    2   C 6 HIS B   6  VAL B  10  1  N  PHE B   7   O  LYS B  33
SHEET    3   C 6 VAL B  75  HIS B  80  1  O  VAL B  78   N  VAL B  10
SHEET    4   C 6 ILE B  98  LEU B 104  1  O  VAL B 102   N  LEU B  77
SHEET    5   C 6 ARG B 202  CYS B 207  1  O  VAL B 203   N  PHE B 103
SHEET    6   C 6 GLU B 229  ILE B 233  1  O  ILE B 233   N  VAL B 206
SHEET    1   D 2 GLN B 135  PRO B 138  0
SHEET    2   D 2 THR B 147  PHE B 150 -1  O  PHE B 150   N  GLN B 135
SHEET    1   E 6 LYS C  33  LEU C  37  0
SHEET    2   E 6 HIS C   6  VAL C  10  1  N  PHE C   7   O  LYS C  33
SHEET    3   E 6 VAL C  75  HIS C  80  1  O  VAL C  78   N  VAL C  10
SHEET    4   E 6 ILE C  98  LEU C 104  1  O  VAL C 102   N  LEU C  77
SHEET    5   E 6 ARG C 202  CYS C 207  1  O  VAL C 203   N  PHE C 103
SHEET    6   E 6 GLU C 229  ILE C 233  1  O  ILE C 233   N  VAL C 206
SHEET    1   F 2 GLN C 135  PRO C 138  0
SHEET    2   F 2 THR C 147  PHE C 150 -1  O  SER C 148   N  LEU C 137
SHEET    1   G 6 LYS D  33  ALA D  36  0
SHEET    2   G 6 HIS D   6  VAL D  10  1  N  PHE D   7   O  LYS D  33
SHEET    3   G 6 VAL D  75  HIS D  80  1  O  VAL D  78   N  VAL D  10
SHEET    4   G 6 ILE D  98  LEU D 104  1  O  VAL D 102   N  LEU D  77
SHEET    5   G 6 ARG D 202  CYS D 207  1  O  VAL D 203   N  PHE D 103
SHEET    6   G 6 GLU D 229  ILE D 233  1  O  ILE D 233   N  VAL D 206
SHEET    1   H 2 GLN D 135  PRO D 138  0
SHEET    2   H 2 THR D 147  PHE D 150 -1  O  SER D 148   N  LEU D 137
LINK         OG  SER A  81                 C7  STH A 297
LINK         OG  SER B  81                 C7  STH B 298
LINK         OG  SER C  81                 C7  STH C 299
LINK         OG  SER D  81                 C7  STH D 300
CRYST1  136.457  167.773   44.831  90.00  90.00  90.00 P 21 21 2    16
ORIGX1      1.000000  0.000000  0.000000        0.00000
ORIGX2      0.000000  1.000000  0.000000        0.00000
ORIGX3      0.000000  0.000000  1.000000        0.00000
SCALE1      0.007328  0.000000  0.000000        0.00000
SCALE2      0.000000  0.005960  0.000000        0.00000
SCALE3      0.000000  0.000000  0.022306        0.00000
TER    2043      ASN A 260
TER    4066      LYS B 258
TER    6101      TYR C 259
TER    8135      ASN D 260
MASTER      390    0   40   55   32    0    0    6 9105    4  340   84
END