longtext: 2XE4-pdb

content
HEADER    HYDROLASE/INHIBITOR                     11-MAY-10   2XE4
TITLE     STRUCTURE OF OLIGOPEPTIDASE B FROM LEISHMANIA MAJOR
COMPND    MOL_ID: 1;
COMPND   2 MOLECULE: OLIGOPEPTIDASE B;
COMPND   3 CHAIN: A;
COMPND   4 SYNONYM: FAMILY S9A-LIKE PROTEIN, SERINE PEPTIDASE;
COMPND   5 EC: 3.4.21.83;
COMPND   6 ENGINEERED: YES;
COMPND   7 MUTATION: YES;
COMPND   8 MOL_ID: 2;
COMPND   9 MOLECULE: ANTIPAIN;
COMPND  10 CHAIN: B
SOURCE    MOL_ID: 1;
SOURCE   2 ORGANISM_SCIENTIFIC: LEISHMANIA MAJOR;
SOURCE   3 ORGANISM_TAXID: 5664;
SOURCE   4 STRAIN: FRIEDLIN;
SOURCE   5 EXPRESSION_SYSTEM: ESCHERICHIA COLI;
SOURCE   6 EXPRESSION_SYSTEM_TAXID: 469008;
SOURCE   7 EXPRESSION_SYSTEM_STRAIN: BL21(DE3)(PLYS);
SOURCE   8 EXPRESSION_SYSTEM_VECTOR: PET28A;
SOURCE   9 EXPRESSION_SYSTEM_PLASMID: PBP218;
SOURCE  10 MOL_ID: 2;
SOURCE  11 ORGANISM_SCIENTIFIC: ACTINOBACTERIA;
SOURCE  12 ORGANISM_TAXID: 1760
KEYWDS    HYDROLASE-INHIBITOR COMPLEX, HYDROLASE, PROTEASE INHIBITOR
KEYWDS   2 TRYPANOSOMES, CLAN SC
EXPDTA    X-RAY DIFFRACTION
AUTHOR    K.MCLUSKEY,N.G.PATERSON,N.D.BLAND,J.C.MOTTRAM,N.W.ISAACS
REVDAT   1   06-OCT-10 2XE4    0
JRNL        AUTH   K.MCLUSKEY,N.G.PATERSON,N.D.BLAND,J.C.MOTTRAM,N.W.ISAACS
JRNL        TITL   THE CRYSTAL STRUCTURE OF LEISHMANIA MAJOR OLIGOPEPTIDASE B
JRNL        TITL 2 GIVES INSIGHT INTO THE ENZYMATIC PROPERTIES OF A
JRNL        TITL 3 TRYPANOSOMATID VIRULENCE FACTOR
JRNL        REF    TO BE PUBLISHED
JRNL        REFN
REMARK   2
REMARK   2 RESOLUTION.    1.65 ANGSTROMS.
REMARK   3
REMARK   3 REFINEMENT.
REMARK   3   PROGRAM     : REFMAC 5.5.0102
REMARK   3   AUTHORS     : MURSHUDOV,VAGIN,DODSON
REMARK   3
REMARK   3    REFINEMENT TARGET : MAXIMUM LIKELIHOOD
REMARK   3
REMARK   3  DATA USED IN REFINEMENT.
REMARK   3   RESOLUTION RANGE HIGH (ANGSTROMS) : 1.650
REMARK   3   RESOLUTION RANGE LOW  (ANGSTROMS) : 117.851
REMARK   3   DATA CUTOFF            (SIGMA(F)) : NONE
REMARK   3   COMPLETENESS FOR RANGE        (%) : 98.007
REMARK   3   NUMBER OF REFLECTIONS             : 167169
REMARK   3
REMARK   3  FIT TO DATA USED IN REFINEMENT.
REMARK   3   CROSS-VALIDATION METHOD          : THROUGHOUT
REMARK   3   FREE R VALUE TEST SET SELECTION  : RANDOM
REMARK   3   R VALUE     (WORKING + TEST SET) : 0.142
REMARK   3   R VALUE            (WORKING SET) : 0.1403
REMARK   3   FREE R VALUE                     : 0.1780
REMARK   3   FREE R VALUE TEST SET SIZE   (%) : 5.08
REMARK   3   FREE R VALUE TEST SET COUNT      : 8321
REMARK   3
REMARK   3  FIT IN THE HIGHEST RESOLUTION BIN.
REMARK   3   TOTAL NUMBER OF BINS USED           : 20
REMARK   3   BIN RESOLUTION RANGE HIGH       (A) : 1.65
REMARK   3   BIN RESOLUTION RANGE LOW        (A) : 1.693
REMARK   3   REFLECTION IN BIN     (WORKING SET) : 11787
REMARK   3   BIN COMPLETENESS (WORKING+TEST) (%) : 98.914
REMARK   3   BIN R VALUE           (WORKING SET) : 0.293
REMARK   3   BIN FREE R VALUE SET COUNT          : 605
REMARK   3   BIN FREE R VALUE                    : 0.342
REMARK   3
REMARK   3  NUMBER OF NON-HYDROGEN ATOMS USED IN REFINEMENT.
REMARK   3   PROTEIN ATOMS            : 6168
REMARK   3   NUCLEIC ACID ATOMS       : 0
REMARK   3   HETEROGEN ATOMS          : 326
REMARK   3   SOLVENT ATOMS            : 721
REMARK   3
REMARK   3  B VALUES.
REMARK   3   FROM WILSON PLOT           (A**2) : 29.5
REMARK   3   MEAN B VALUE      (OVERALL, A**2) : 41.338
REMARK   3   OVERALL ANISOTROPIC B VALUE.
REMARK   3    B11 (A**2) : 2.673
REMARK   3    B22 (A**2) : -1.710
REMARK   3    B33 (A**2) : -0.963
REMARK   3    B12 (A**2) : 0.000
REMARK   3    B13 (A**2) : 0.000
REMARK   3    B23 (A**2) : 0.000
REMARK   3
REMARK   3  ESTIMATED OVERALL COORDINATE ERROR.
REMARK   3   ESU BASED ON R VALUE                            (A): 0.066
REMARK   3   ESU BASED ON FREE R VALUE                       (A): 0.064
REMARK   3   ESU BASED ON MAXIMUM LIKELIHOOD                 (A): 0.051
REMARK   3   ESU FOR B VALUES BASED ON MAXIMUM LIKELIHOOD (A**2): 3.558
REMARK   3
REMARK   3  CORRELATION COEFFICIENTS.
REMARK   3   CORRELATION COEFFICIENT FO-FC      : 0.981
REMARK   3   CORRELATION COEFFICIENT FO-FC FREE : 0.971
REMARK   3
REMARK   3  RMS DEVIATIONS FROM IDEAL VALUES        COUNT    RMS    WEIGHT
REMARK   3   BOND LENGTHS REFINED ATOMS        (A):  6627 ; 0.035 ; 0.022
REMARK   3   BOND LENGTHS OTHERS               (A):  NULL ;  NULL ;  NULL
REMARK   3   BOND ANGLES REFINED ATOMS   (DEGREES):  8977 ; 2.353 ; 1.982
REMARK   3   BOND ANGLES OTHERS          (DEGREES):  NULL ;  NULL ;  NULL
REMARK   3   TORSION ANGLES, PERIOD 1    (DEGREES):   819 ; 6.661 ; 5.000
REMARK   3   TORSION ANGLES, PERIOD 2    (DEGREES):   305 ;33.738 ;23.738
REMARK   3   TORSION ANGLES, PERIOD 3    (DEGREES):  1084 ;12.490 ;15.000
REMARK   3   TORSION ANGLES, PERIOD 4    (DEGREES):    46 ;15.532 ;15.000
REMARK   3   CHIRAL-CENTER RESTRAINTS       (A**3):   975 ; 0.209 ; 0.200
REMARK   3   GENERAL PLANES REFINED ATOMS      (A):  5027 ; 0.014 ; 0.021
REMARK   3   GENERAL PLANES OTHERS             (A):  NULL ;  NULL ;  NULL
REMARK   3   NON-BONDED CONTACTS REFINED ATOMS (A):  3318 ; 0.222 ; 0.200
REMARK   3   NON-BONDED CONTACTS OTHERS        (A):  NULL ;  NULL ;  NULL
REMARK   3   NON-BONDED TORSION REFINED ATOMS  (A):  4107 ; 0.304 ; 0.200
REMARK   3   NON-BONDED TORSION OTHERS         (A):  NULL ;  NULL ;  NULL
REMARK   3   H-BOND (X...Y) REFINED ATOMS      (A):   704 ; 0.161 ; 0.200
REMARK   3   H-BOND (X...Y) OTHERS             (A):  NULL ;  NULL ;  NULL
REMARK   3   POTENTIAL METAL-ION REFINED ATOMS (A):     1 ; 0.065 ; 0.200
REMARK   3   POTENTIAL METAL-ION OTHERS        (A):  NULL ;  NULL ;  NULL
REMARK   3   SYMMETRY VDW REFINED ATOMS        (A):    91 ; 0.227 ; 0.200
REMARK   3   SYMMETRY VDW OTHERS               (A):  NULL ;  NULL ;  NULL
REMARK   3   SYMMETRY H-BOND REFINED ATOMS     (A):    29 ; 0.215 ; 0.200
REMARK   3   SYMMETRY H-BOND OTHERS            (A):  NULL ;  NULL ;  NULL
REMARK   3   SYMMETRY METAL-ION REFINED ATOMS  (A):  NULL ;  NULL ;  NULL
REMARK   3   SYMMETRY METAL-ION OTHERS         (A):  NULL ;  NULL ;  NULL
REMARK   3
REMARK   3  ISOTROPIC THERMAL FACTOR RESTRAINTS.     COUNT   RMS    WEIGHT
REMARK   3   MAIN-CHAIN BOND REFINED ATOMS  (A**2):  3852 ; 2.833 ; 1.500
REMARK   3   MAIN-CHAIN BOND OTHER ATOMS    (A**2):  NULL ;  NULL ;  NULL
REMARK   3   MAIN-CHAIN ANGLE REFINED ATOMS (A**2):  6311 ; 4.118 ; 2.000
REMARK   3   SIDE-CHAIN BOND REFINED ATOMS  (A**2):  2775 ; 6.794 ; 3.000
REMARK   3   SIDE-CHAIN ANGLE REFINED ATOMS (A**2):  2648 ; 9.512 ; 4.500
REMARK   3
REMARK   3  ANISOTROPIC THERMAL FACTOR RESTRAINTS.   COUNT   RMS    WEIGHT
REMARK   3   RIGID-BOND RESTRAINTS          (A**2):  6627 ; 3.903 ; 3.000
REMARK   3   SPHERICITY; FREE ATOMS         (A**2):  NULL ;  NULL ;  NULL
REMARK   3   SPHERICITY; BONDED ATOMS       (A**2):  NULL ;  NULL ;  NULL
REMARK   3
REMARK   3  NCS RESTRAINTS STATISTICS
REMARK   3   NUMBER OF DIFFERENT NCS GROUPS : NULL
REMARK   3
REMARK   3  TLS DETAILS
REMARK   3   NUMBER OF TLS GROUPS  : NULL
REMARK   3
REMARK   3  BULK SOLVENT MODELLING.
REMARK   3   METHOD USED : BABINET MODEL PLUS MASK
REMARK   3   PARAMETERS FOR MASK CALCULATION
REMARK   3   VDW PROBE RADIUS   : 1.400
REMARK   3   ION PROBE RADIUS   : 0.800
REMARK   3   SHRINKAGE RADIUS   : NULL
REMARK   3
REMARK   3  OTHER REFINEMENT REMARKS: HYDROGENS HAVE BEEN ADDED IN THE
REMARK   3   RIDING POSITIONS. RESIDUES 1-9 AND 731 ARE DISORDERED.
REMARK   4
REMARK   4 2XE4 COMPLIES WITH FORMAT V. 3.20, 01-DEC-08
REMARK 100
REMARK 100 THIS ENTRY HAS BEEN PROCESSED BY PDBE ON 11-MAY-10.
REMARK 100 THE PDBE ID CODE IS EBI-43877.
REMARK 200
REMARK 200 EXPERIMENTAL DETAILS
REMARK 200  EXPERIMENT TYPE                : X-RAY DIFFRACTION
REMARK 200  DATE OF DATA COLLECTION        : 10-JUN-08
REMARK 200  TEMPERATURE           (KELVIN) : 103
REMARK 200  PH                             : 4.2
REMARK 200  NUMBER OF CRYSTALS USED        : 1
REMARK 200
REMARK 200  SYNCHROTRON              (Y/N) : N ; Y
REMARK 200  RADIATION SOURCE               : ROTATING ANODE ; ESRF
REMARK 200  BEAMLINE                       : NULL ; BM14
REMARK 200  X-RAY GENERATOR MODEL          : RIGAKU MICROMAX 007
REMARK 200  MONOCHROMATIC OR LAUE    (M/L) : M ; M
REMARK 200  WAVELENGTH OR RANGE        (A) : 1.541 ; 1.005
REMARK 200  MONOCHROMATOR                  : GRAPHITE ; NULL
REMARK 200  OPTICS                         : MIRRORS  ; NULL
REMARK 200
REMARK 200  DETECTOR TYPE                  : IMAGE PLATE ; CCD
REMARK 200  DETECTOR MANUFACTURER          : MARRESEARCH ; MARRESEARCH
REMARK 200  INTENSITY-INTEGRATION SOFTWARE : DTREK
REMARK 200  DATA SCALING SOFTWARE          : SCALA
REMARK 200
REMARK 200  NUMBER OF UNIQUE REFLECTIONS   : 167772
REMARK 200  RESOLUTION RANGE HIGH      (A) : 1.65
REMARK 200  RESOLUTION RANGE LOW       (A) : 32.00
REMARK 200  REJECTION CRITERIA  (SIGMA(I)) : 1.5
REMARK 200
REMARK 200 OVERALL.
REMARK 200  COMPLETENESS FOR RANGE     (%) : 98.4
REMARK 200  DATA REDUNDANCY                : 3.3
REMARK 200  R MERGE                    (I) : 0.06
REMARK 200  R SYM                      (I) : NULL
REMARK 200   FOR THE DATA SET  : 8.80
REMARK 200
REMARK 200 IN THE HIGHEST RESOLUTION SHELL.
REMARK 200  HIGHEST RESOLUTION SHELL, RANGE HIGH (A) : 1.65
REMARK 200  HIGHEST RESOLUTION SHELL, RANGE LOW  (A) : 1.71
REMARK 200  COMPLETENESS FOR SHELL     (%) : 100.0
REMARK 200  DATA REDUNDANCY IN SHELL       : 3.0
REMARK 200  R MERGE FOR SHELL          (I) : 0.46
REMARK 200  R SYM FOR SHELL            (I) : NULL
REMARK 200   FOR SHELL         : 1.70
REMARK 200
REMARK 200 DIFFRACTION PROTOCOL: SINGLE WAVELENGTH
REMARK 200 METHOD USED TO DETERMINE THE STRUCTURE: SAD
REMARK 200 SOFTWARE USED: AUTOSHARP, SHELXC, SHELXD
REMARK 200 STARTING MODEL: NONE
REMARK 200
REMARK 200 REMARK: NONE
REMARK 280
REMARK 280 CRYSTAL
REMARK 280 SOLVENT CONTENT, VS   (%): 71
REMARK 280 MATTHEWS COEFFICIENT, VM (ANGSTROMS**3/DA): 4.2
REMARK 280
REMARK 280 CRYSTALLIZATION CONDITIONS: PROTEIN WAS DIALYZED INTO 50 MM
REMARK 280  TRIS, PH 8.0 AND INCUBATED WITH 10 MM ANTIPAIN FOR 30
REMARK 280  MINS. THIS WAS MIXED IN A 1:1 RATIO WITH 25% 1,2
REMARK 280  PROPANEDIOL, 10% GLYCEROL, 5 % PEG300 AND 0.1 M PHOSPHATE
REMARK 280  CITRATE, PH 4.2
REMARK 290
REMARK 290 CRYSTALLOGRAPHIC SYMMETRY
REMARK 290 SYMMETRY OPERATORS FOR SPACE GROUP: I 2 2 2
REMARK 290
REMARK 290      SYMOP   SYMMETRY
REMARK 290     NNNMMM   OPERATOR
REMARK 290       1555   X,Y,Z
REMARK 290       2555   -X,-Y,Z
REMARK 290       3555   -X,Y,-Z
REMARK 290       4555   X,-Y,-Z
REMARK 290       5555   X+1/2,Y+1/2,Z+1/2
REMARK 290       6555   -X+1/2,-Y+1/2,Z+1/2
REMARK 290       7555   -X+1/2,Y+1/2,-Z+1/2
REMARK 290       8555   X+1/2,-Y+1/2,-Z+1/2
REMARK 290
REMARK 290     WHERE NNN -> OPERATOR NUMBER
REMARK 290           MMM -> TRANSLATION VECTOR
REMARK 290
REMARK 290 CRYSTALLOGRAPHIC SYMMETRY TRANSFORMATIONS
REMARK 290 THE FOLLOWING TRANSFORMATIONS OPERATE ON THE ATOM/HETATM
REMARK 290 RECORDS IN THIS ENTRY TO PRODUCE CRYSTALLOGRAPHICALLY
REMARK 290 RELATED MOLECULES.
REMARK 290   SMTRY1   1  1.000000  0.000000  0.000000        0.00000
REMARK 290   SMTRY2   1  0.000000  1.000000  0.000000        0.00000
REMARK 290   SMTRY3   1  0.000000  0.000000  1.000000        0.00000
REMARK 290   SMTRY1   2 -1.000000  0.000000  0.000000        0.00000
REMARK 290   SMTRY2   2  0.000000 -1.000000  0.000000        0.00000
REMARK 290   SMTRY3   2  0.000000  0.000000  1.000000        0.00000
REMARK 290   SMTRY1   3 -1.000000  0.000000  0.000000        0.00000
REMARK 290   SMTRY2   3  0.000000  1.000000  0.000000        0.00000
REMARK 290   SMTRY3   3  0.000000  0.000000 -1.000000        0.00000
REMARK 290   SMTRY1   4  1.000000  0.000000  0.000000        0.00000
REMARK 290   SMTRY2   4  0.000000 -1.000000  0.000000        0.00000
REMARK 290   SMTRY3   4  0.000000  0.000000 -1.000000        0.00000
REMARK 290   SMTRY1   5  1.000000  0.000000  0.000000       47.73900
REMARK 290   SMTRY2   5  0.000000  1.000000  0.000000       71.38800
REMARK 290   SMTRY3   5  0.000000  0.000000  1.000000      104.45950
REMARK 290   SMTRY1   6 -1.000000  0.000000  0.000000       47.73900
REMARK 290   SMTRY2   6  0.000000 -1.000000  0.000000       71.38800
REMARK 290   SMTRY3   6  0.000000  0.000000  1.000000      104.45950
REMARK 290   SMTRY1   7 -1.000000  0.000000  0.000000       47.73900
REMARK 290   SMTRY2   7  0.000000  1.000000  0.000000       71.38800
REMARK 290   SMTRY3   7  0.000000  0.000000 -1.000000      104.45950
REMARK 290   SMTRY1   8  1.000000  0.000000  0.000000       47.73900
REMARK 290   SMTRY2   8  0.000000 -1.000000  0.000000       71.38800
REMARK 290   SMTRY3   8  0.000000  0.000000 -1.000000      104.45950
REMARK 290
REMARK 290 REMARK: NULL
REMARK 300
REMARK 300 BIOMOLECULE: 1
REMARK 300 SEE REMARK 350 FOR THE AUTHOR PROVIDED AND/OR PROGRAM
REMARK 300 GENERATED ASSEMBLY INFORMATION FOR THE STRUCTURE IN
REMARK 300 THIS ENTRY. THE REMARK MAY ALSO PROVIDE INFORMATION ON
REMARK 300 BURIED SURFACE AREA.
REMARK 350
REMARK 350 COORDINATES FOR A COMPLETE MULTIMER REPRESENTING THE KNOWN
REMARK 350 BIOLOGICALLY SIGNIFICANT OLIGOMERIZATION STATE OF THE
REMARK 350 MOLECULE CAN BE GENERATED BY APPLYING BIOMT TRANSFORMATIONS
REMARK 350 GIVEN BELOW.  BOTH NON-CRYSTALLOGRAPHIC AND
REMARK 350 CRYSTALLOGRAPHIC OPERATIONS ARE GIVEN.
REMARK 350
REMARK 350 BIOMOLECULE: 1
REMARK 350 AUTHOR DETERMINED BIOLOGICAL UNIT: DIMERIC
REMARK 350 SOFTWARE DETERMINED QUATERNARY STRUCTURE: DIMERIC
REMARK 350 SOFTWARE USED: PISA
REMARK 350 APPLY THE FOLLOWING TO CHAINS: A, B
REMARK 350   BIOMT1   1  1.000000  0.000000  0.000000        0.00000
REMARK 350   BIOMT2   1  0.000000  1.000000  0.000000        0.00000
REMARK 350   BIOMT3   1  0.000000  0.000000  1.000000        0.00000
REMARK 400
REMARK 400 COMPOUND
REMARK 400 ENGINEERED RESIDUE IN CHAIN A, PHE  25 TO LEU
REMARK 465
REMARK 465 MISSING RESIDUES
REMARK 465 THE FOLLOWING RESIDUES WERE NOT LOCATED IN THE
REMARK 465 EXPERIMENT. (M=MODEL NUMBER; RES=RESIDUE NAME; C=CHAIN
REMARK 465 IDENTIFIER; SSSEQ=SEQUENCE NUMBER; I=INSERTION CODE.)
REMARK 465
REMARK 465   M RES C SSSEQI
REMARK 465     MET A   -19
REMARK 465     GLY A   -18
REMARK 465     SER A   -17
REMARK 465     SER A   -16
REMARK 465     HIS A   -15
REMARK 465     HIS A   -14
REMARK 465     HIS A   -13
REMARK 465     HIS A   -12
REMARK 465     HIS A   -11
REMARK 465     HIS A   -10
REMARK 465     SER A    -9
REMARK 465     SER A    -8
REMARK 465     GLY A    -7
REMARK 465     LEU A    -6
REMARK 465     VAL A    -5
REMARK 465     PRO A    -4
REMARK 465     ARG A    -3
REMARK 465     GLY A    -2
REMARK 465     SER A    -1
REMARK 465     HIS A     0
REMARK 465     MET A     1
REMARK 465     SER A     2
REMARK 465     SER A     3
REMARK 465     ASP A     4
REMARK 465     SER A     5
REMARK 465     SER A     6
REMARK 465     VAL A     7
REMARK 465     ALA A     8
REMARK 465     ALA A     9
REMARK 465     ARG A   731
REMARK 500
REMARK 500 GEOMETRY AND STEREOCHEMISTRY
REMARK 500 SUBTOPIC: CLOSE CONTACTS IN SAME ASYMMETRIC UNIT
REMARK 500
REMARK 500 THE FOLLOWING ATOMS ARE IN CLOSE CONTACT.
REMARK 500
REMARK 500  ATM1  RES C  SSEQI   ATM2  RES C  SSEQI           DISTANCE
REMARK 500   O2   PGR A  1784     O    HOH A  2712              2.09
REMARK 500   O    HOH A  2219     O    HOH A  2654              2.10
REMARK 500   O    HOH A  2110     O    HOH A  2643              2.13
REMARK 500   O    HOH A  2123     O    HOH A  2128              2.19
REMARK 500
REMARK 500 REMARK: NULL
REMARK 500
REMARK 500 GEOMETRY AND STEREOCHEMISTRY
REMARK 500 SUBTOPIC: COVALENT BOND LENGTHS
REMARK 500
REMARK 500 THE STEREOCHEMICAL PARAMETERS OF THE FOLLOWING RESIDUES
REMARK 500 HAVE VALUES WHICH DEVIATE FROM EXPECTED VALUES BY MORE
REMARK 500 THAN 6*RMSD (M=MODEL NUMBER; RES=RESIDUE NAME; C=CHAIN
REMARK 500 IDENTIFIER; SSEQ=SEQUENCE NUMBER; I=INSERTION CODE).
REMARK 500
REMARK 500 STANDARD TABLE:
REMARK 500 FORMAT: (10X,I3,1X,2(A3,1X,A1,I4,A1,1X,A4,3X),1X,F6.3)
REMARK 500
REMARK 500 EXPECTED VALUES PROTEIN: ENGH AND HUBER, 1999
REMARK 500 EXPECTED VALUES NUCLEIC ACID: CLOWNEY ET AL 1996
REMARK 500
REMARK 500  M RES CSSEQI ATM1   RES CSSEQI ATM2   DEVIATION
REMARK 500    TYR A  71   CG    TYR A  71   CD1     0.082
REMARK 500    TYR A 110   CE1   TYR A 110   CZ      0.106
REMARK 500    GLU A 205   CD    GLU A 205   OE2    -0.072
REMARK 500    TYR A 217   CG    TYR A 217   CD1     0.089
REMARK 500    ARG A 332   CZ    ARG A 332   NH2     0.086
REMARK 500    TRP A 338   CG    TRP A 338   CD1     0.099
REMARK 500    SER A 346   CB    SER A 346   OG     -0.083
REMARK 500    PHE A 350   CG    PHE A 350   CD1     0.094
REMARK 500    GLU A 352   CB    GLU A 352   CG     -0.169
REMARK 500    GLU A 352   CG    GLU A 352   CD      0.156
REMARK 500    ALA A 368   CA    ALA A 368   CB      0.139
REMARK 500    TYR A 494   CZ    TYR A 494   CE2     0.092
REMARK 500    TYR A 499   CE1   TYR A 499   CZ      0.081
REMARK 500    TYR A 514   CG    TYR A 514   CD1     0.079
REMARK 500    TYR A 514   CZ    TYR A 514   CE2     0.108
REMARK 500    TRP A 536   CZ3   TRP A 536   CH2     0.106
REMARK 500    TYR A 537   CG    TYR A 537   CD1     0.089
REMARK 500    TYR A 537   CZ    TYR A 537   CE2     0.087
REMARK 500    GLU A 538   CB    GLU A 538   CG     -0.156
REMARK 500    PHE A 553   CE1   PHE A 553   CZ      0.121
REMARK 500    GLU A 624   CG    GLU A 624   CD      0.102
REMARK 500    GLU A 624   CD    GLU A 624   OE1     0.071
REMARK 500    GLU A 624   CD    GLU A 624   OE2     0.073
REMARK 500    TRP A 625   CG    TRP A 625   CD1     0.089
REMARK 500    TRP A 625   CZ3   TRP A 625   CH2     0.106
REMARK 500    TYR A 633   CZ    TYR A 633   CE2     0.088
REMARK 500    TYR A 667   CG    TYR A 667   CD1     0.092
REMARK 500    TYR A 667   CZ    TYR A 667   CE2     0.085
REMARK 500    TRP A 673   CE3   TRP A 673   CZ3     0.106
REMARK 500    PHE A 698   CZ    PHE A 698   CE2     0.142
REMARK 500    PHE A 706   CE1   PHE A 706   CZ      0.117
REMARK 500    TRP A 707   CE3   TRP A 707   CZ3     0.104
REMARK 500    ARG B   2   CD    ARG B   2   NE      0.135
REMARK 500    ARG B   2   NE    ARG B   2   CZ      0.116
REMARK 500    ARG B   2   CZ    ARG B   2   NH1     0.188
REMARK 500
REMARK 500 REMARK: NULL
REMARK 500
REMARK 500 GEOMETRY AND STEREOCHEMISTRY
REMARK 500 SUBTOPIC: COVALENT BOND ANGLES
REMARK 500
REMARK 500 THE STEREOCHEMICAL PARAMETERS OF THE FOLLOWING RESIDUES
REMARK 500 HAVE VALUES WHICH DEVIATE FROM EXPECTED VALUES BY MORE
REMARK 500 THAN 6*RMSD (M=MODEL NUMBER; RES=RESIDUE NAME; C=CHAIN
REMARK 500 IDENTIFIER; SSEQ=SEQUENCE NUMBER; I=INSERTION CODE).
REMARK 500
REMARK 500 STANDARD TABLE:
REMARK 500 FORMAT: (10X,I3,1X,A3,1X,A1,I4,A1,3(1X,A4,2X),12X,F5.1)
REMARK 500
REMARK 500 EXPECTED VALUES PROTEIN: ENGH AND HUBER, 1999
REMARK 500 EXPECTED VALUES NUCLEIC ACID: CLOWNEY ET AL 1996
REMARK 500
REMARK 500  M RES CSSEQI ATM1   ATM2   ATM3
REMARK 500    ARG A  33   NE  -  CZ  -  NH2 ANGL. DEV. =  -3.5 DEGREES
REMARK 500    ARG A  56   NE  -  CZ  -  NH1 ANGL. DEV. =  -3.2 DEGREES
REMARK 500    ARG A 113   NE  -  CZ  -  NH1 ANGL. DEV. =  -3.6 DEGREES
REMARK 500    ASP A 129   CB  -  CG  -  OD1 ANGL. DEV. =   7.3 DEGREES
REMARK 500    ASP A 211   CB  -  CG  -  OD1 ANGL. DEV. =   6.9 DEGREES
REMARK 500    ASP A 281   CB  -  CG  -  OD1 ANGL. DEV. =   5.6 DEGREES
REMARK 500    ARG A 283   NE  -  CZ  -  NH1 ANGL. DEV. =  -3.1 DEGREES
REMARK 500    ARG A 295   NE  -  CZ  -  NH1 ANGL. DEV. =  -3.6 DEGREES
REMARK 500    ARG A 295   NE  -  CZ  -  NH2 ANGL. DEV. =   3.1 DEGREES
REMARK 500    ASP A 344   CB  -  CG  -  OD1 ANGL. DEV. =   7.5 DEGREES
REMARK 500    ASP A 344   CB  -  CG  -  OD2 ANGL. DEV. =  -5.8 DEGREES
REMARK 500    ARG A 462   NE  -  CZ  -  NH2 ANGL. DEV. =  -3.8 DEGREES
REMARK 500    ARG A 527   NE  -  CZ  -  NH1 ANGL. DEV. =  -3.1 DEGREES
REMARK 500    ARG A 576   NE  -  CZ  -  NH2 ANGL. DEV. =  -4.4 DEGREES
REMARK 500    ARG A 590   NE  -  CZ  -  NH2 ANGL. DEV. =  -3.1 DEGREES
REMARK 500    ILE A 712   CG1 -  CB  -  CG2 ANGL. DEV. = -15.5 DEGREES
REMARK 500    ARG A 726   NE  -  CZ  -  NH1 ANGL. DEV. =   3.6 DEGREES
REMARK 500    ARG A 726   NE  -  CZ  -  NH2 ANGL. DEV. =  -3.1 DEGREES
REMARK 500    ARG B   2   CD  -  NE  -  CZ  ANGL. DEV. =  27.3 DEGREES
REMARK 500    ARG B   2   NE  -  CZ  -  NH1 ANGL. DEV. =  15.6 DEGREES
REMARK 500    ARG B   2   NE  -  CZ  -  NH2 ANGL. DEV. = -17.0 DEGREES
REMARK 500
REMARK 500 REMARK: NULL
REMARK 500
REMARK 500 GEOMETRY AND STEREOCHEMISTRY
REMARK 500 SUBTOPIC: TORSION ANGLES
REMARK 500
REMARK 500 TORSION ANGLES OUTSIDE THE EXPECTED RAMACHANDRAN REGIONS:
REMARK 500 (M=MODEL NUMBER; RES=RESIDUE NAME; C=CHAIN IDENTIFIER;
REMARK 500 SSEQ=SEQUENCE NUMBER; I=INSERTION CODE).
REMARK 500
REMARK 500 STANDARD TABLE:
REMARK 500 FORMAT:(10X,I3,1X,A3,1X,A1,I4,A1,4X,F7.2,3X,F7.2)
REMARK 500
REMARK 500 EXPECTED VALUES: GJ KLEYWEGT AND TA JONES (1996). PHI/PSI-
REMARK 500 CHOLOGY: RAMACHANDRAN REVISITED. STRUCTURE 4, 1395 - 1400
REMARK 500
REMARK 500  M RES CSSEQI        PSI       PHI
REMARK 500    ASN A  36       61.45   -152.15
REMARK 500    VAL A 294      -70.39    -81.65
REMARK 500    HIS A 325      153.19     88.92
REMARK 500    VAL A 406       74.08   -104.24
REMARK 500    TYR A 496      -81.43   -131.34
REMARK 500    TYR A 537      -61.39    -97.11
REMARK 500    ALA A 541       84.63   -163.91
REMARK 500    TYR A 543     -123.68     43.68
REMARK 500    SER A 577     -116.99     61.97
REMARK 500    VAL A 601       57.47     32.62
REMARK 500    ASP A 605       59.11    -94.31
REMARK 500    LEU A 617      -19.76     82.90
REMARK 500    GLU A 624      -69.84   -108.48
REMARK 500    SER A 699     -157.10     57.83
REMARK 500
REMARK 500 REMARK: NULL
REMARK 600
REMARK 600 HETEROGEN
REMARK 600 CHLORINE ION (CL): NA
REMARK 620
REMARK 620 METAL COORDINATION
REMARK 620 (M=MODEL NUMBER; RES=RESIDUE NAME; C=CHAIN IDENTIFIER;
REMARK 620 SSEQ=SEQUENCE NUMBER; I=INSERTION CODE):
REMARK 620
REMARK 620 COORDINATION ANGLES FOR:  M RES CSSEQI METAL
REMARK 620                              NA A1795  NA
REMARK 620 N RES CSSEQI ATOM
REMARK 620 1 ILE A  94   O
REMARK 620 2 ILE A  91   O    77.9
REMARK 620 3 HOH A2132   O    86.8 107.8
REMARK 620 4 HOH A2138   O    85.8 155.6  89.0
REMARK 620 5 HOH A2131   O   170.3  99.9 102.8  93.2
REMARK 620 N                    1     2     3     4
REMARK 620
REMARK 620 COORDINATION ANGLES FOR:  M RES CSSEQI METAL
REMARK 620                              NA A1797  NA
REMARK 620 N RES CSSEQI ATOM
REMARK 620 1 ASP A 174   OD1
REMARK 620 2 ASN A 178   OD1  91.9
REMARK 620 3 VAL A 180   O    90.9  90.9
REMARK 620 4 SER A 176   OG   73.5  68.7 153.3
REMARK 620 5 HOH A2226   O   150.3 113.6  74.5 128.7
REMARK 620 6 HOH A2216   O    92.5 169.6  98.4 103.6  65.1
REMARK 620 N                    1     2     3     4     5
REMARK 800
REMARK 800 SITE
REMARK 800 SITE_IDENTIFIER: AC1
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE GOL A1732
REMARK 800
REMARK 800 SITE_IDENTIFIER: AC2
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE GOL A1733
REMARK 800
REMARK 800 SITE_IDENTIFIER: AC3
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE GOL A1734
REMARK 800
REMARK 800 SITE_IDENTIFIER: AC4
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE GOL A1735
REMARK 800
REMARK 800 SITE_IDENTIFIER: AC5
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE GOL A1736
REMARK 800
REMARK 800 SITE_IDENTIFIER: AC6
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE GOL A1737
REMARK 800
REMARK 800 SITE_IDENTIFIER: AC7
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE GOL A1738
REMARK 800
REMARK 800 SITE_IDENTIFIER: AC8
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE GOL A1739
REMARK 800
REMARK 800 SITE_IDENTIFIER: AC9
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE GOL A1740
REMARK 800
REMARK 800 SITE_IDENTIFIER: BC1
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE GOL A1741
REMARK 800
REMARK 800 SITE_IDENTIFIER: BC2
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE PGR A1742
REMARK 800
REMARK 800 SITE_IDENTIFIER: BC3
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE PGO A1743
REMARK 800
REMARK 800 SITE_IDENTIFIER: BC4
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE PGR A1744
REMARK 800
REMARK 800 SITE_IDENTIFIER: BC5
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE PGR A1745
REMARK 800
REMARK 800 SITE_IDENTIFIER: BC6
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE PGR A1746
REMARK 800
REMARK 800 SITE_IDENTIFIER: BC7
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE PGR A1747
REMARK 800
REMARK 800 SITE_IDENTIFIER: BC8
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE PGR A1748
REMARK 800
REMARK 800 SITE_IDENTIFIER: BC9
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE PGR A1749
REMARK 800
REMARK 800 SITE_IDENTIFIER: CC1
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE PGR A1750
REMARK 800
REMARK 800 SITE_IDENTIFIER: CC2
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE PGR A1751
REMARK 800
REMARK 800 SITE_IDENTIFIER: CC3
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE PGR A1752
REMARK 800
REMARK 800 SITE_IDENTIFIER: CC4
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE PGR A1753
REMARK 800
REMARK 800 SITE_IDENTIFIER: CC5
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE PGR A1754
REMARK 800
REMARK 800 SITE_IDENTIFIER: CC6
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE PGR A1755
REMARK 800
REMARK 800 SITE_IDENTIFIER: CC7
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE PGR A1756
REMARK 800
REMARK 800 SITE_IDENTIFIER: CC8
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE PGR A1757
REMARK 800
REMARK 800 SITE_IDENTIFIER: CC9
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE PGR A1758
REMARK 800
REMARK 800 SITE_IDENTIFIER: DC1
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE PGR A1759
REMARK 800
REMARK 800 SITE_IDENTIFIER: DC2
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE PGR A1760
REMARK 800
REMARK 800 SITE_IDENTIFIER: DC3
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE PGR A1761
REMARK 800
REMARK 800 SITE_IDENTIFIER: DC4
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE PGR A1762
REMARK 800
REMARK 800 SITE_IDENTIFIER: DC5
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE PGR A1763
REMARK 800
REMARK 800 SITE_IDENTIFIER: DC6
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE PGR A1764
REMARK 800
REMARK 800 SITE_IDENTIFIER: DC7
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE PGR A1765
REMARK 800
REMARK 800 SITE_IDENTIFIER: DC8
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE PGR A1766
REMARK 800
REMARK 800 SITE_IDENTIFIER: DC9
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE PGR A1767
REMARK 800
REMARK 800 SITE_IDENTIFIER: EC1
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE PGR A1768
REMARK 800
REMARK 800 SITE_IDENTIFIER: EC2
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE PGR A1769
REMARK 800
REMARK 800 SITE_IDENTIFIER: EC3
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE PGR A1770
REMARK 800
REMARK 800 SITE_IDENTIFIER: EC4
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE PGR A1771
REMARK 800
REMARK 800 SITE_IDENTIFIER: EC5
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE PGR A1772
REMARK 800
REMARK 800 SITE_IDENTIFIER: EC6
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE PGR A1773
REMARK 800
REMARK 800 SITE_IDENTIFIER: EC7
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE PGR A1774
REMARK 800
REMARK 800 SITE_IDENTIFIER: EC8
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE PGR A1775
REMARK 800
REMARK 800 SITE_IDENTIFIER: EC9
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE PGR A1776
REMARK 800
REMARK 800 SITE_IDENTIFIER: FC1
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE PGR A1777
REMARK 800
REMARK 800 SITE_IDENTIFIER: FC2
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE PGR A1778
REMARK 800
REMARK 800 SITE_IDENTIFIER: FC3
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE PGR A1779
REMARK 800
REMARK 800 SITE_IDENTIFIER: FC4
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE PGR A1780
REMARK 800
REMARK 800 SITE_IDENTIFIER: FC5
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE PGR A1781
REMARK 800
REMARK 800 SITE_IDENTIFIER: FC6
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE PGR A1782
REMARK 800
REMARK 800 SITE_IDENTIFIER: FC7
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE PGR A1783
REMARK 800
REMARK 800 SITE_IDENTIFIER: FC8
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE PGR A1784
REMARK 800
REMARK 800 SITE_IDENTIFIER: FC9
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE PGR A1785
REMARK 800
REMARK 800 SITE_IDENTIFIER: GC1
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE PGR A1786
REMARK 800
REMARK 800 SITE_IDENTIFIER: GC2
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE PGR A1787
REMARK 800
REMARK 800 SITE_IDENTIFIER: GC3
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE PGR A1788
REMARK 800
REMARK 800 SITE_IDENTIFIER: GC4
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE PGR A1789
REMARK 800
REMARK 800 SITE_IDENTIFIER: GC5
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE PGR A1790
REMARK 800
REMARK 800 SITE_IDENTIFIER: GC6
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE PO4 A1791
REMARK 800
REMARK 800 SITE_IDENTIFIER: GC7
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE PO4 A1792
REMARK 800
REMARK 800 SITE_IDENTIFIER: GC8
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE PO4 A1793
REMARK 800
REMARK 800 SITE_IDENTIFIER: GC9
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE  CL A1794
REMARK 800
REMARK 800 SITE_IDENTIFIER: HC1
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE  NA A1795
REMARK 800
REMARK 800 SITE_IDENTIFIER: HC2
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE  CL A1796
REMARK 800
REMARK 800 SITE_IDENTIFIER: HC3
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE  NA A1797
REMARK 800
REMARK 800 SITE_IDENTIFIER: HC4
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE  CL A1798
REMARK 800
REMARK 800 SITE_IDENTIFIER: HC5
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE  CL A1799
REMARK 800
REMARK 800 SITE_IDENTIFIER: HC6
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR CHAIN B OF
REMARK 800     RESIDUES    1 TO    4
DBREF  2XE4 A    1   731  UNP    Q4QHU7   Q4QHU7_LEIMA     1    731
DBREF  2XE4 B    1     4  NORINE NOR00664 NOR00664         1      4
SEQADV 2XE4 MET A  -19  UNP  Q4QHU7              EXPRESSION TAG
SEQADV 2XE4 GLY A  -18  UNP  Q4QHU7              EXPRESSION TAG
SEQADV 2XE4 SER A  -17  UNP  Q4QHU7              EXPRESSION TAG
SEQADV 2XE4 SER A  -16  UNP  Q4QHU7              EXPRESSION TAG
SEQADV 2XE4 HIS A  -15  UNP  Q4QHU7              EXPRESSION TAG
SEQADV 2XE4 HIS A  -14  UNP  Q4QHU7              EXPRESSION TAG
SEQADV 2XE4 HIS A  -13  UNP  Q4QHU7              EXPRESSION TAG
SEQADV 2XE4 HIS A  -12  UNP  Q4QHU7              EXPRESSION TAG
SEQADV 2XE4 HIS A  -11  UNP  Q4QHU7              EXPRESSION TAG
SEQADV 2XE4 HIS A  -10  UNP  Q4QHU7              EXPRESSION TAG
SEQADV 2XE4 SER A   -9  UNP  Q4QHU7              EXPRESSION TAG
SEQADV 2XE4 SER A   -8  UNP  Q4QHU7              EXPRESSION TAG
SEQADV 2XE4 GLY A   -7  UNP  Q4QHU7              EXPRESSION TAG
SEQADV 2XE4 LEU A   -6  UNP  Q4QHU7              EXPRESSION TAG
SEQADV 2XE4 VAL A   -5  UNP  Q4QHU7              EXPRESSION TAG
SEQADV 2XE4 PRO A   -4  UNP  Q4QHU7              EXPRESSION TAG
SEQADV 2XE4 ARG A   -3  UNP  Q4QHU7              EXPRESSION TAG
SEQADV 2XE4 GLY A   -2  UNP  Q4QHU7              EXPRESSION TAG
SEQADV 2XE4 SER A   -1  UNP  Q4QHU7              EXPRESSION TAG
SEQADV 2XE4 HIS A    0  UNP  Q4QHU7              EXPRESSION TAG
SEQADV 2XE4 LEU A   25  UNP  Q4QHU7    PHE    25 ENGINEERED MUTATION
SEQRES   1 A  751  MET GLY SER SER HIS HIS HIS HIS HIS HIS SER SER GLY
SEQRES   2 A  751  LEU VAL PRO ARG GLY SER HIS MET SER SER ASP SER SER
SEQRES   3 A  751  VAL ALA ALA SER ALA GLN PRO PRO ILE ALA ALA LYS LYS
SEQRES   4 A  751  PRO HIS ARG VAL THR LEU GLY TYR VAL GLU GLY GLU ASP
SEQRES   5 A  751  ARG GLY PRO ASN PRO MET ASN PRO PRO ARG TYR ARG GLU
SEQRES   6 A  751  ASP PRO TYR PHE TRP MET ARG ASP ASP ASP ARG LYS ASP
SEQRES   7 A  751  PRO ALA VAL ILE GLU HIS LEU ASN LYS GLU LYS VAL TYR
SEQRES   8 A  751  PHE GLN ALA ARG SER ALA ASP ILE ALA GLN LEU ARG ASP
SEQRES   9 A  751  ASP ILE TYR ALA GLU HIS ILE SER HIS ILE ASN GLU ASP
SEQRES  10 A  751  ASP MET SER ALA PRO TYR VAL TYR GLY LYS TYR ARG TYR
SEQRES  11 A  751  TYR THR ARG GLU VAL LYS GLY LYS PRO TYR LYS ILE TYR
SEQRES  12 A  751  CYS ARG VAL PHE THR ASP LYS GLU PRO GLY ASP VAL ALA
SEQRES  13 A  751  ALA GLU GLU VAL ILE ILE ASP VAL ASN GLN VAL ALA GLU
SEQRES  14 A  751  GLY LYS ALA PHE CYS ASP VAL MET GLU VAL LYS PRO ALA
SEQRES  15 A  751  PRO PRO GLU HIS ASP LEU VAL ALA PHE SER VAL ASP MET
SEQRES  16 A  751  SER GLY ASN GLU VAL TYR THR ILE GLU PHE LYS ARG ILE
SEQRES  17 A  751  SER ASP PRO SER GLN THR ILE ALA ASP LYS VAL SER GLY
SEQRES  18 A  751  THR ASN GLY GLU ILE VAL TRP GLY PRO ASP HIS THR SER
SEQRES  19 A  751  LEU PHE TYR VAL THR LYS ASP GLU THR LEU ARG GLU ASN
SEQRES  20 A  751  LYS VAL TRP ARG HIS VAL MET GLY LYS LEU GLN SER GLU
SEQRES  21 A  751  ASP VAL CYS LEU TYR GLU GLU HIS ASN PRO LEU PHE SER
SEQRES  22 A  751  ALA PHE MET TYR LYS ALA ALA ASP THR ASN THR LEU CYS
SEQRES  23 A  751  ILE GLY SER GLN SER PRO GLU THR ALA GLU VAL HIS LEU
SEQRES  24 A  751  LEU ASP LEU ARG LYS GLY ASN ALA HIS ASN THR LEU GLU
SEQRES  25 A  751  ILE VAL ARG PRO ARG GLU LYS GLY VAL ARG TYR ASP VAL
SEQRES  26 A  751  GLN MET HIS GLY THR SER HIS LEU VAL ILE LEU THR ASN
SEQRES  27 A  751  GLU GLY GLY ALA VAL ASN HIS LYS LEU LEU ILE ALA PRO
SEQRES  28 A  751  ARG GLY GLN PRO SER ASP TRP SER HIS VAL LEU VAL ASP
SEQRES  29 A  751  HIS SER GLU ASP VAL PHE MET GLU SER ILE ALA VAL ARG
SEQRES  30 A  751  SER ASN TYR LEU VAL VAL ALA GLY ARG ARG ALA GLY LEU
SEQRES  31 A  751  THR ARG ILE TRP THR MET MET ALA ASP SER GLN ASP GLY
SEQRES  32 A  751  VAL PHE LYS ALA GLY THR GLY LEU ARG GLU VAL VAL MET
SEQRES  33 A  751  GLU GLU PRO ILE PHE THR VAL HIS LEU VAL GLU SER GLN
SEQRES  34 A  751  MET LEU GLU TYR GLU GLU PRO THR PHE ARG MET GLU TYR
SEQRES  35 A  751  SER SER LEU ALA THR PRO ASN THR TRP PHE ASP VAL SER
SEQRES  36 A  751  PRO GLN ASP HIS SER ARG THR ALA VAL LYS VAL ARG GLU
SEQRES  37 A  751  VAL GLY GLY GLY PHE ASP ALA ALA ASN TYR LYS VAL GLU
SEQRES  38 A  751  ARG ARG PHE ALA THR ALA PRO ASP GLN THR LYS ILE PRO
SEQRES  39 A  751  LEU SER VAL VAL TYR HIS LYS ASP LEU ASP MET SER GLN
SEQRES  40 A  751  PRO GLN PRO CYS MET LEU TYR GLY TYR GLY SER TYR GLY
SEQRES  41 A  751  LEU SER MET ASP PRO GLN PHE SER ILE GLN HIS LEU PRO
SEQRES  42 A  751  TYR CYS ASP ARG GLY MET ILE PHE ALA ILE ALA HIS ILE
SEQRES  43 A  751  ARG GLY GLY SER GLU LEU GLY ARG ALA TRP TYR GLU ILE
SEQRES  44 A  751  GLY ALA LYS TYR LEU THR LYS ARG ASN THR PHE SER ASP
SEQRES  45 A  751  PHE ILE ALA ALA ALA GLU PHE LEU VAL ASN ALA LYS LEU
SEQRES  46 A  751  THR THR PRO SER GLN LEU ALA CYS GLU GLY ARG SER ALA
SEQRES  47 A  751  GLY GLY LEU LEU MET GLY ALA VAL LEU ASN MET ARG PRO
SEQRES  48 A  751  ASP LEU PHE LYS VAL ALA LEU ALA GLY VAL PRO PHE VAL
SEQRES  49 A  751  ASP VAL MET THR THR MET CYS ASP PRO SER ILE PRO LEU
SEQRES  50 A  751  THR THR GLY GLU TRP GLU GLU TRP GLY ASN PRO ASN GLU
SEQRES  51 A  751  TYR LYS TYR TYR ASP TYR MET LEU SER TYR SER PRO MET
SEQRES  52 A  751  ASP ASN VAL ARG ALA GLN GLU TYR PRO ASN ILE MET VAL
SEQRES  53 A  751  GLN CYS GLY LEU HIS ASP PRO ARG VAL ALA TYR TRP GLU
SEQRES  54 A  751  PRO ALA LYS TRP VAL SER LYS LEU ARG GLU CYS LYS THR
SEQRES  55 A  751  ASP ASN ASN GLU ILE LEU LEU ASN ILE ASP MET GLU SER
SEQRES  56 A  751  GLY HIS PHE SER ALA LYS ASP ARG TYR LYS PHE TRP LYS
SEQRES  57 A  751  GLU SER ALA ILE GLN GLN ALA PHE VAL CYS LYS HIS LEU
SEQRES  58 A  751  LYS SER THR VAL ARG LEU LEU VAL ARG ARG
SEQRES   1 B    4  FC0 ARG VAL RGL
HET    FC0  B   1      14
HET    RGL  B   4      11
HET    GOL  A1732       6
HET    GOL  A1733       6
HET    GOL  A1734       6
HET    GOL  A1735       6
HET    GOL  A1736       6
HET    GOL  A1737       6
HET    GOL  A1738       6
HET    GOL  A1739       6
HET    GOL  A1740       6
HET    GOL  A1741       6
HET    PGR  A1742       5
HET    PGO  A1743       5
HET    PGR  A1744       5
HET    PGR  A1745       5
HET    PGR  A1746       5
HET    PGR  A1747       5
HET    PGR  A1748       5
HET    PGR  A1749       5
HET    PGR  A1750       5
HET    PGR  A1751       5
HET    PGR  A1752       5
HET    PGR  A1753       5
HET    PGR  A1754       5
HET    PGR  A1755       5
HET    PGR  A1756       5
HET    PGR  A1757       5
HET    PGR  A1758       5
HET    PGR  A1759       5
HET    PGR  A1760       5
HET    PGR  A1761       5
HET    PGR  A1762       5
HET    PGR  A1763       5
HET    PGR  A1764       5
HET    PGR  A1765       5
HET    PGR  A1766       5
HET    PGR  A1767       5
HET    PGR  A1768       5
HET    PGR  A1769       5
HET    PGR  A1770       5
HET    PGR  A1771       5
HET    PGR  A1772       5
HET    PGR  A1773       5
HET    PGR  A1774       5
HET    PGR  A1775       5
HET    PGR  A1776       5
HET    PGR  A1777       5
HET    PGR  A1778       5
HET    PGR  A1779       5
HET    PGR  A1780       5
HET    PGR  A1781       5
HET    PGR  A1782       5
HET    PGR  A1783       5
HET    PGR  A1784       5
HET    PGR  A1785       5
HET    PGR  A1786       5
HET    PGR  A1787       5
HET    PGR  A1788       5
HET    PGR  A1789       5
HET    PGR  A1790       5
HET    PO4  A1791       5
HET    PO4  A1792       5
HET    PO4  A1793       5
HET     CL  A1794       1
HET     NA  A1795       1
HET     CL  A1796       1
HET     NA  A1797       1
HET     CL  A1798       1
HET     CL  A1799       1
HETNAM     RGL ARGINAL
HETNAM     FC0 N-CARBOXY-L-PHENYLALANINE
HETNAM     PO4 PHOSPHATE ION
HETNAM      NA SODIUM ION
HETNAM      CL CHLORIDE ION
HETNAM     PGR R-1,2-PROPANEDIOL
HETNAM     PGO S-1,2-PROPANEDIOL
HETNAM     GOL GLYCEROL
FORMUL   2  FC0    C10 H11 N O4
FORMUL   3  RGL    C6 H14 N4 O
FORMUL   4  PO4    3(O4 P 3-)
FORMUL   5   NA    2(NA 1+)
FORMUL   6   CL    4(CL 1-)
FORMUL   7  PGR    48(C3 H8 O2)
FORMUL   8  PGO    C3 H8 O2
FORMUL   9  GOL    10(C3 H8 O3)
FORMUL  10  HOH   *721(H2 O)
HELIX    1   1 TYR A   48  ARG A   52  5                                   5
HELIX    2   2 ASP A   58  ALA A   77  1                                  20
HELIX    3   3 ILE A   79  HIS A   93  1                                  15
HELIX    4   4 VAL A  144  ALA A  148  1                                   5
HELIX    5   5 LEU A  237  ASP A  241  5                                   5
HELIX    6   6 GLU A  407  MET A  410  5                                   4
HELIX    7   7 ASP A  454  ALA A  456  5                                   3
HELIX    8   8 SER A  508  GLN A  510  5                                   3
HELIX    9   9 HIS A  511  ASP A  516  1                                   6
HELIX   10  10 ARG A  534  ILE A  539  1                                   6
HELIX   11  11 LYS A  542  LYS A  546  5                                   5
HELIX   12  12 ARG A  547  ALA A  563  1                                  17
HELIX   13  13 THR A  567  SER A  569  5                                   3
HELIX   14  14 SER A  577  ARG A  590  1                                  14
HELIX   15  15 PRO A  591  PHE A  594  5                                   4
HELIX   16  16 ASP A  605  CYS A  611  1                                   7
HELIX   17  17 LEU A  617  TRP A  622  1                                   6
HELIX   18  18 GLU A  630  SER A  641  1                                  12
HELIX   19  19 PRO A  642  VAL A  646  5                                   5
HELIX   20  20 TYR A  667  LYS A  681  1                                  15
HELIX   21  21 ASP A  702  LEU A  721  1                                  20
HELIX   22  22 ARG A  726  ARG A  730  5                                   5
SHEET    1  AA 2 ARG A  22  LEU A  25  0
SHEET    2  AA 2 ARG A  42  GLU A  45 -1  O  ARG A  42   N  LEU A  25
SHEET    1  AB 2 ASP A  98  MET A  99  0
SHEET    2  AB 2 TYR A 108  GLU A 114 -1  O  GLU A 114   N  ASP A  98
SHEET    1  AC 2 TYR A 103  TYR A 105  0
SHEET    2  AC 2 TYR A 108  GLU A 114 -1  O  TYR A 108   N  TYR A 105
SHEET    1  AD 4 GLU A 139  ASP A 143  0
SHEET    2  AD 4 ILE A 122  PHE A 127 -1  O  TYR A 123   N  ILE A 141
SHEET    3  AD 4 TYR A 108  GLU A 114 -1  O  ARG A 109   N  VAL A 126
SHEET    4  AD 4 TYR A 103  TYR A 105 -1  O  TYR A 103   N  TYR A 110
SHEET    1  AE 4 GLU A 139  ASP A 143  0
SHEET    2  AE 4 ILE A 122  PHE A 127 -1  O  TYR A 123   N  ILE A 141
SHEET    3  AE 4 TYR A 108  GLU A 114 -1  O  ARG A 109   N  VAL A 126
SHEET    4  AE 4 ASP A  98  MET A  99 -1  O  ASP A  98   N  GLU A 114
SHEET    1  AF 4 ASP A 155  PRO A 161  0
SHEET    2  AF 4 LEU A 168  ASP A 174 -1  O  ALA A 170   N  LYS A 160
SHEET    3  AF 4 TYR A 181  ARG A 187 -1  O  THR A 182   N  VAL A 173
SHEET    4  AF 4 VAL A 199  THR A 202 -1  O  VAL A 199   N  ILE A 183
SHEET    1  AG 4 VAL A 207  TRP A 208  0
SHEET    2  AG 4 SER A 214  LYS A 220 -1  O  PHE A 216   N  VAL A 207
SHEET    3  AG 4 GLU A 226  VAL A 233 -1  N  ASN A 227   O  THR A 219
SHEET    4  AG 4 VAL A 242  GLU A 246 -1  O  VAL A 242   N  ARG A 231
SHEET    1  AH 4 SER A 253  LYS A 258  0
SHEET    2  AH 4 THR A 264  GLN A 270 -1  O  CYS A 266   N  TYR A 257
SHEET    3  AH 4 ALA A 275  ASP A 281 -1  O  GLU A 276   N  SER A 269
SHEET    4  AH 4 GLU A 292  ILE A 293 -1  O  GLU A 292   N  LEU A 279
SHEET    1  AI 4 TYR A 303  HIS A 308  0
SHEET    2  AI 4 HIS A 312  THR A 317 -1  O  HIS A 312   N  HIS A 308
SHEET    3  AI 4 LYS A 326  PRO A 331 -1  O  LYS A 326   N  THR A 317
SHEET    4  AI 4 VAL A 341  VAL A 343 -1  N  LEU A 342   O  LEU A 327
SHEET    1  AJ 4 VAL A 349  VAL A 356  0
SHEET    2  AJ 4 TYR A 360  ARG A 367 -1  O  VAL A 362   N  ALA A 355
SHEET    3  AJ 4 LEU A 370  MET A 377 -1  O  LEU A 370   N  ARG A 367
SHEET    4  AJ 4 ARG A 392  GLU A 393 -1  O  ARG A 392   N  THR A 375
SHEET    1  AK 4 THR A 402  LEU A 405  0
SHEET    2  AK 4 PHE A 418  SER A 424 -1  O  GLU A 421   N  HIS A 404
SHEET    3  AK 4 THR A 427  VAL A 434 -1  O  THR A 427   N  SER A 424
SHEET    4  AK 4 ARG A 441  VAL A 446 -1  O  THR A 442   N  ASP A 433
SHEET    1  AL 8 TYR A 458  THR A 466  0
SHEET    2  AL 8 LYS A 472  HIS A 480 -1  O  ILE A 473   N  ALA A 465
SHEET    3  AL 8 ILE A 520  ALA A 524 -1  O  PHE A 521   N  VAL A 478
SHEET    4  AL 8 CYS A 491  TYR A 494  1  O  MET A 492   N  ALA A 522
SHEET    5  AL 8 LEU A 571  ARG A 576  1  O  ALA A 572   N  LEU A 493
SHEET    6  AL 8 VAL A 596  GLY A 600  1  O  VAL A 596   N  CYS A 573
SHEET    7  AL 8 ASN A 653  GLY A 659  1  O  ASN A 653   N  ALA A 597
SHEET    8  AL 8 ILE A 687  ASP A 692  1  O  LEU A 688   N  VAL A 656
LINK        NA    NA A1795                 O   ILE A  94     1555   1555  2.50
LINK        NA    NA A1795                 O   ILE A  91     1555   1555  2.43
LINK        NA    NA A1795                 O   HOH A2132     1555   1555  2.50
LINK        NA    NA A1795                 O   HOH A2138     1555   1555  2.55
LINK        NA    NA A1795                 O   HOH A2131     1555   1555  2.35
LINK        NA    NA A1797                 OG  SER A 176     1555   1555  3.08
LINK        NA    NA A1797                 O   VAL A 180     1555   1555  2.59
LINK        NA    NA A1797                 OD1 ASN A 178     1555   1555  2.57
LINK        NA    NA A1797                 OD1 ASP A 174     1555   1555  2.46
LINK        NA    NA A1797                 O   HOH A2216     1555   1555  2.65
LINK        NA    NA A1797                 O   HOH A2226     1555   1555  2.99
LINK         C1  FC0 B   1                 N   ARG B   2     1555   1555  1.38
LINK         C   VAL B   3                 N   RGL B   4     1555   1555  1.34
LINK         C   RGL B   4                 OG  SER A 577     1555   1555  1.51
CISPEP   1 ASN A   39    PRO A   40          0         3.63
CISPEP   2 PRO A  163    PRO A  164          0         2.57
SITE     1 AC1  9 PRO A 591  ASP A 592  PHE A 594  GLU A 650
SITE     2 AC1  9 TYR A 651  PRO A 652  PGR A1766  HOH A2610
SITE     3 AC1  9 HOH A2710
SITE     1 AC2  6 HIS A 340  VAL A 341  PHE A 385  LYS A 386
SITE     2 AC2  6 ALA A 387  PGR A1759
SITE     1 AC3  8 GLY A 452  HIS A 480  ASP A 516  ARG A 726
SITE     2 AC3  8 LEU A 727  LEU A 728  HOH A2479  HOH A2682
SITE     1 AC4  5 LYS A 595  ASN A 653  ASN A 685  HIS A 720
SITE     2 AC4  5 PGR A1767
SITE     1 AC5  2 PHE A 698  HOH A2720
SITE     1 AC6  3 GLN A 437  HIS A 439  HOH A2683
SITE     1 AC7  8 SER A 311  VAL A 446  ARG A 447  GLU A 448
SITE     2 AC7  8 VAL A 449  HOH A2362  HOH A2684  HOH A2685
SITE     1 AC8  3 THR A 466  ALA A 555  GLU A 558
SITE     1 AC9  8 ARG A 547  SER A 551  MET A 589  ASP A 635
SITE     2 AC9  8 TYR A 636  HOH A2546  HOH A2590  HOH A2591
SITE     1 BC1  8 LYS A 299  TYR A 543  TRP A 622  ASN A 627
SITE     2 BC1  8 TYR A 633  HOH A2587  HOH A2686  HOH A2687
SITE     1 BC2  7 GLU A 574  GLY A 575  GLY A 600  GLN A 713
SITE     2 BC2  7 PGO A1743  HOH A2688  HOH A2706
SITE     1 BC3  7 GLN A 510  TYR A 514  GLU A 574  LEU A 598
SITE     2 BC3  7 SER A 710  PGR A1742  PGR A1777
SITE     1 BC4  6 HIS A 308  GLY A 309  SER A 311  HIS A 312
SITE     2 BC4  6 ASP A 454  HOH A2441
SITE     1 BC5  6 ALA A 700  LYS A 701  ARG A 703  PHE A 706
SITE     2 BC5  6 HOH A2162  HOH A2656
SITE     1 BC6  8 TRP A  50  ARG A  52  ASP A  53  PGR A1775
SITE     2 BC6  8 PGR A1780  HOH A2091  HOH A2691  HOH A2700
SITE     1 BC7  5 ARG A 527  ALA A 535  GLY A 540  HOH A2491
SITE     2 BC7  5 HOH A2692
SITE     1 BC8  6 ASP A 155  MET A 157  PHE A 698  LYS A 701
SITE     2 BC8  6 HOH A2195  HOH A2693
SITE     1 BC9  6 GLY A 369  ARG A 462  PRO A 474  SER A 476
SITE     2 BC9  6 HIS A 525  HOH A2716
SITE     1 CC1  5 ALA A  88  GLU A  89  SER A  92  GLY A 451
SITE     2 CC1  5 HOH A2674
SITE     1 CC2  4 TYR A 103  TYR A 110  VAL A 159  LEU A 411
SITE     1 CC3  4 ILE A 142  ASP A 143  LYS A 186  HOH A2694
SITE     1 CC4  5 ALA A 259  LEU A 411  HOH A2152  HOH A2204
SITE     2 CC4  5 HOH A2437
SITE     1 CC5  3 THR A 262  ASN A 263  LEU A 282
SITE     1 CC6  6 GLY A 300  VAL A 301  ASN A 318  GLY A 320
SITE     2 CC6  6 GLY A 321  HOH A2357
SITE     1 CC7  5 ARG A 302  ASP A 304  LEU A 316  HIS A 325
SITE     2 CC7  5 HOH A2385
SITE     1 CC8  7 ASP A 261  ASP A 454  ASN A 457  LYS A 481
SITE     2 CC8  7 HOH A2311  HOH A2442  HOH A2695
SITE     1 CC9  5 ASP A 281  ARG A 283  ARG A 332  THR A 427
SITE     2 CC9  5 HOH A2696
SITE     1 DC1  6 HIS A 312  ILE A 329  HIS A 340  GLU A 448
SITE     2 DC1  6 GOL A1733  HOH A2697
SITE     1 DC2  3 ALA A 378  SER A 380  THR A 389
SITE     1 DC3  5 TYR A 105  THR A 262  LEU A 411  GLU A 412
SITE     2 DC3  5 TYR A 413
SITE     1 DC4  4 ASP A 433  SER A 440  ARG A 441  THR A 442
SITE     1 DC5  3 THR A 290  SER A 440  ARG A 441
SITE     1 DC6  7 MET A 503  ASP A 504  GLN A 506  ILE A 523
SITE     2 DC6  7 PGR A1779  HOH A2516  HOH A2699
SITE     1 DC7  5 ARG A 447  SER A 508  ILE A 509  PGR A1779
SITE     2 DC7  5 HOH A2193
SITE     1 DC8  6 PRO A 568  SER A 569  PHE A 594  LYS A 595
SITE     2 DC8  6 GOL A1732  HOH A2567
SITE     1 DC9  7 ARG A  75  ASN A 653  ASN A 684  ASN A 685
SITE     2 DC9  7 GLU A 686  HIS A 720  GOL A1735
SITE     1 EC1  2 VAL A 104  GLU A 415
SITE     1 EC2  3 ASP A 304  GLN A 306  HOH A2393
SITE     1 EC3  6 TYR A 103  SER A 408  GLN A 409  HOH A2146
SITE     2 EC3  6 HOH A2159  HOH A2433
SITE     1 EC4  7 ALA A  17  LYS A  19  TRP A  50  HOH A2700
SITE     2 EC4  7 HOH A2701  HOH A2702  HOH A2703
SITE     1 EC5  5 ARG A  56  ILE A  62  MET A 693  HOH A2088
SITE     2 EC5  5 HOH A2650
SITE     1 EC6  2 ARG A 295  GLU A 319
SITE     1 EC7  4 ARG A 463  PHE A 464  PHE A 559  HOH A2704
SITE     1 EC8  4 ARG A  52  ASP A  54  PGR A1746  PGR A1780
SITE     1 EC9  6 GLY A 333  GLN A 334  LYS A 445  VAL A 446
SITE     2 EC9  6 GLU A 448  HOH A2705
SITE     1 FC1  8 GLN A 657  SER A 699  GLU A 709  SER A 710
SITE     2 FC1  8 GLN A 713  PGO A1743  HOH A2614  HOH A2706
SITE     1 FC2  6 ASP A  32  GLY A  34  PRO A  35  ASN A 249
SITE     2 FC2  6 TRP A 622  HOH A2707
SITE     1 FC3  5 GLN A 506  SER A 508  PGR A1764  PGR A1765
SITE     2 FC3  5 PO4 A1793
SITE     1 FC4  4 ASP A  53  ASP A  55  PGR A1746  PGR A1775
SITE     1 FC5  4 LYS A 284  GLU A 397  PHE A 432  ARG A 441
SITE     1 FC6  5 GLU A 650  ASP A 683  ASN A 684  ASN A 685
SITE     2 FC6  5 HOH A2710
SITE     1 FC7  5 ASP A  54  ARG A  56  GLU A 222  PRO A 616
SITE     2 FC7  5 TRP A 668
SITE     1 FC8  6 LEU A 638  ASN A 645  VAL A 646  ARG A 647
SITE     2 FC8  6 HOH A2711  HOH A2712
SITE     1 FC9  3 ASN A  66  LYS A  69  GLN A  73
SITE     1 GC1  3 LEU A 342  ASP A 344  ALA A 387
SITE     1 GC2  4 ASP A 281  LYS A 284  HIS A 288  GLU A 292
SITE     1 GC3  4 ARG A 283  LYS A 459  VAL A 460  HOH A2713
SITE     1 GC4  3 GLU A 246  HOH A2714  HOH A2715
SITE     1 GC5  4 ALA A 368  LEU A 532  HOH A2716  HOH A2717
SITE     1 GC6 10 TYR A 496  ARG A 576  SER A 577  HIS A 697
SITE     2 GC6 10 PHE A 698  PO4 A1793  HOH A2719  HOH A2720
SITE     3 GC6 10 VAL B   3  RGL B   4
SITE     1 GC7  5 GLY A 201  LYS A 220  ASP A 221  LEU A 224
SITE     2 GC7  5 HOH A2250
SITE     1 GC8  7 TYR A 494  TYR A 496  LEU A 501  MET A 503
SITE     2 GC8  7 ARG A 576  PGR A1779  PO4 A1791
SITE     1 GC9  3 TRP A 208  HOH A2204  HOH A2309
SITE     1 HC1  5 ILE A  91  ILE A  94  HOH A2131  HOH A2132
SITE     2 HC1  5 HOH A2138
SITE     1 HC2  3 LYS A 121  HOH A2173  HOH A2194
SITE     1 HC3  6 ASP A 174  SER A 176  ASN A 178  VAL A 180
SITE     2 HC3  6 HOH A2216  HOH A2226
SITE     1 HC4  3 HIS A 308  HIS A 312  PHE A 385
SITE     1 HC5  4 GLU A  63  ASN A  66  HOH A2093  HOH A2094
SITE     1 HC6 25 GLU A 226  SER A 253  TYR A 496  TYR A 499
SITE     2 HC6 25 LEU A 501  SER A 577  ALA A 578  PHE A 603
SITE     3 HC6 25 MET A 610  LEU A 617  GLU A 621  ARG A 664
SITE     4 HC6 25 VAL A 665  HIS A 697  PO4 A1791  HOH A2266
SITE     5 HC6 25 HOH A2267  HOH A2302  HOH A2303  HOH A2580
SITE     6 HC6 25 HOH A2622  HOH A2678  HOH A2679  HOH A2680
SITE     7 HC6 25 HOH A2681
CRYST1   95.478  142.776  208.919  90.00  90.00  90.00 I 2 2 2       8
ORIGX1      1.000000  0.000000  0.000000        0.00000
ORIGX2      0.000000  1.000000  0.000000        0.00000
ORIGX3      0.000000  0.000000  1.000000        0.00000
SCALE1      0.010474  0.000000  0.000000        0.00000
SCALE2      0.000000  0.007004  0.000000        0.00000
SCALE3      0.000000  0.000000  0.004787        0.00000
TER    6126      ARG A 730
TER    6170      RGL B   4
MASTER      731    0   70   22   46    0  119    6 7215    2  363   59
END