longtext: 3JYH-pdb

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HEADER    HYDROLASE                               21-SEP-09   3JYH
TITLE     HUMAN DIPEPTIDYL PEPTIDASE DPP7
COMPND    MOL_ID: 1;
COMPND   2 MOLECULE: DIPEPTIDYL-PEPTIDASE 2;
COMPND   3 CHAIN: A, B, C, D;
COMPND   4 FRAGMENT: PEPTIDASE DOMAIN: UNP RESIDUES 28-492;
COMPND   5 SYNONYM: DIPEPTIDYL-PEPTIDASE II, DPP II, DIPEPTIDYL
COMPND   6 AMINOPEPTIDASE II, QUIESCENT CELL PROLINE DIPEPTIDASE,
COMPND   7 DIPEPTIDYL PEPTIDASE 7;
COMPND   8 EC: 3.4.14.2;
COMPND   9 ENGINEERED: YES
SOURCE    MOL_ID: 1;
SOURCE   2 ORGANISM_SCIENTIFIC: HOMO SAPIENS;
SOURCE   3 ORGANISM_COMMON: HUMAN;
SOURCE   4 ORGANISM_TAXID: 9606;
SOURCE   5 GENE: DPP2, DPP7, QPP;
SOURCE   6 EXPRESSION_SYSTEM: SPODOPTERA FRUGIPERDA;
SOURCE   7 EXPRESSION_SYSTEM_TAXID: 7108;
SOURCE   8 EXPRESSION_SYSTEM_STRAIN: SF9;
SOURCE   9 EXPRESSION_SYSTEM_CELL_LINE: SF9 INSECT CELLS;
SOURCE  10 EXPRESSION_SYSTEM_VECTOR_TYPE: PLASMID;
SOURCE  11 EXPRESSION_SYSTEM_VECTOR: BACULOVIRUS;
SOURCE  12 EXPRESSION_SYSTEM_PLASMID: PFHMSP-LIC-N
KEYWDS    STRUCTURAL GENOMICS, STRUCTURAL GENOMICS CONSORTIUM, SGC,
KEYWDS   2 AMINOPEPTIDASE, CLEAVAGE ON PAIR OF BASIC RESIDUES,
KEYWDS   3 CYTOPLASMIC VESICLE, GLYCOPROTEIN, HYDROLASE, LYSOSOME,
KEYWDS   4 POLYMORPHISM, PROTEASE, SERINE PROTEASE, ZYMOGEN
EXPDTA    X-RAY DIFFRACTION
AUTHOR    E.DOBROVETSKY,A.DONG,A.SEITOVA,L.CROMBETT,S.PAGANON,
AUTHOR   2 D.COSSAR,A.M.EDWARDS,C.H.ARROWSMITH,C.BOUNTRA,J.WEIGELT,
AUTHOR   3 A.HASSEL,L.SHEWCHUK,A.BOCHKAREV,STRUCTURAL GENOMICS
AUTHOR   4 CONSORTIUM (SGC)
REVDAT   1   13-OCT-09 3JYH    0
JRNL        AUTH   E.DOBROVETSKY,A.DONG,A.SEITOVA,L.CROMBETT,
JRNL        AUTH 2 S.PAGANON,D.COSSAR,A.M.EDWARDS,C.H.ARROWSMITH,
JRNL        AUTH 3 C.BOUNTRA,J.WEIGELT,A.HASSEL,L.SHEWCHUK,A.BOCHKAREV
JRNL        TITL   HUMAN DIPEPTIDYL PEPTIDASE DPP7
JRNL        REF    TO BE PUBLISHED
JRNL        REFN
REMARK   1
REMARK   2
REMARK   2 RESOLUTION.    2.19 ANGSTROMS.
REMARK   3
REMARK   3 REFINEMENT.
REMARK   3   PROGRAM     : REFMAC 5.2.0019
REMARK   3   AUTHORS     : MURSHUDOV,VAGIN,DODSON
REMARK   3
REMARK   3    REFINEMENT TARGET : MAXIMUM LIKELIHOOD
REMARK   3
REMARK   3  DATA USED IN REFINEMENT.
REMARK   3   RESOLUTION RANGE HIGH (ANGSTROMS) : 2.19
REMARK   3   RESOLUTION RANGE LOW  (ANGSTROMS) : 100.00
REMARK   3   DATA CUTOFF            (SIGMA(F)) : 0.000
REMARK   3   COMPLETENESS FOR RANGE        (%) : 98.8
REMARK   3   NUMBER OF REFLECTIONS             : 127511
REMARK   3
REMARK   3  FIT TO DATA USED IN REFINEMENT.
REMARK   3   CROSS-VALIDATION METHOD          : THROUGHOUT
REMARK   3   FREE R VALUE TEST SET SELECTION  : RANDOM
REMARK   3   R VALUE     (WORKING + TEST SET) : 0.182
REMARK   3   R VALUE            (WORKING SET) : 0.180
REMARK   3   FREE R VALUE                     : 0.222
REMARK   3   FREE R VALUE TEST SET SIZE   (%) : 5.000
REMARK   3   FREE R VALUE TEST SET COUNT      : 6400
REMARK   3
REMARK   3  FIT IN THE HIGHEST RESOLUTION BIN.
REMARK   3   TOTAL NUMBER OF BINS USED           : 20
REMARK   3   BIN RESOLUTION RANGE HIGH       (A) : 2.19
REMARK   3   BIN RESOLUTION RANGE LOW        (A) : 2.24
REMARK   3   REFLECTION IN BIN     (WORKING SET) : 7870
REMARK   3   BIN COMPLETENESS (WORKING+TEST) (%) : 87.07
REMARK   3   BIN R VALUE           (WORKING SET) : 0.2180
REMARK   3   BIN FREE R VALUE SET COUNT          : 392
REMARK   3   BIN FREE R VALUE                    : 0.2580
REMARK   3
REMARK   3  NUMBER OF NON-HYDROGEN ATOMS USED IN REFINEMENT.
REMARK   3   PROTEIN ATOMS            : 13857
REMARK   3   NUCLEIC ACID ATOMS       : 0
REMARK   3   HETEROGEN ATOMS          : 341
REMARK   3   SOLVENT ATOMS            : 946
REMARK   3
REMARK   3  B VALUES.
REMARK   3   FROM WILSON PLOT           (A**2) : NULL
REMARK   3   MEAN B VALUE      (OVERALL, A**2) : 33.22
REMARK   3   OVERALL ANISOTROPIC B VALUE.
REMARK   3    B11 (A**2) : 0.96000
REMARK   3    B22 (A**2) : -1.36000
REMARK   3    B33 (A**2) : -0.21000
REMARK   3    B12 (A**2) : 0.00000
REMARK   3    B13 (A**2) : -1.43000
REMARK   3    B23 (A**2) : 0.00000
REMARK   3
REMARK   3  ESTIMATED OVERALL COORDINATE ERROR.
REMARK   3   ESU BASED ON R VALUE                            (A): 0.201
REMARK   3   ESU BASED ON FREE R VALUE                       (A): 0.175
REMARK   3   ESU BASED ON MAXIMUM LIKELIHOOD                 (A): 0.122
REMARK   3   ESU FOR B VALUES BASED ON MAXIMUM LIKELIHOOD (A**2): 4.714
REMARK   3
REMARK   3 CORRELATION COEFFICIENTS.
REMARK   3   CORRELATION COEFFICIENT FO-FC      : 0.954
REMARK   3   CORRELATION COEFFICIENT FO-FC FREE : 0.930
REMARK   3
REMARK   3  RMS DEVIATIONS FROM IDEAL VALUES        COUNT    RMS    WEIGHT
REMARK   3   BOND LENGTHS REFINED ATOMS        (A): 14632 ; 0.013 ; 0.021
REMARK   3   BOND LENGTHS OTHERS               (A):  NULL ;  NULL ;  NULL
REMARK   3   BOND ANGLES REFINED ATOMS   (DEGREES): 19969 ; 1.346 ; 1.963
REMARK   3   BOND ANGLES OTHERS          (DEGREES):  NULL ;  NULL ;  NULL
REMARK   3   TORSION ANGLES, PERIOD 1    (DEGREES):  1803 ; 5.860 ; 5.000
REMARK   3   TORSION ANGLES, PERIOD 2    (DEGREES):   679 ;33.572 ;23.108
REMARK   3   TORSION ANGLES, PERIOD 3    (DEGREES):  1998 ;13.188 ;15.000
REMARK   3   TORSION ANGLES, PERIOD 4    (DEGREES):   103 ;18.862 ;15.000
REMARK   3   CHIRAL-CENTER RESTRAINTS       (A**3):  2168 ; 0.089 ; 0.200
REMARK   3   GENERAL PLANES REFINED ATOMS      (A): 11418 ; 0.005 ; 0.020
REMARK   3   GENERAL PLANES OTHERS             (A):  NULL ;  NULL ;  NULL
REMARK   3   NON-BONDED CONTACTS REFINED ATOMS (A):  6821 ; 0.194 ; 0.200
REMARK   3   NON-BONDED CONTACTS OTHERS        (A):  NULL ;  NULL ;  NULL
REMARK   3   NON-BONDED TORSION REFINED ATOMS  (A):  9977 ; 0.310 ; 0.200
REMARK   3   NON-BONDED TORSION OTHERS         (A):  NULL ;  NULL ;  NULL
REMARK   3   H-BOND (X...Y) REFINED ATOMS      (A):  1073 ; 0.147 ; 0.200
REMARK   3   H-BOND (X...Y) OTHERS             (A):  NULL ;  NULL ;  NULL
REMARK   3   POTENTIAL METAL-ION REFINED ATOMS (A):  NULL ;  NULL ;  NULL
REMARK   3   POTENTIAL METAL-ION OTHERS        (A):  NULL ;  NULL ;  NULL
REMARK   3   SYMMETRY VDW REFINED ATOMS        (A):    47 ; 0.167 ; 0.200
REMARK   3   SYMMETRY VDW OTHERS               (A):  NULL ;  NULL ;  NULL
REMARK   3   SYMMETRY H-BOND REFINED ATOMS     (A):     8 ; 0.162 ; 0.200
REMARK   3   SYMMETRY H-BOND OTHERS            (A):  NULL ;  NULL ;  NULL
REMARK   3   SYMMETRY METAL-ION REFINED ATOMS  (A):  NULL ;  NULL ;  NULL
REMARK   3   SYMMETRY METAL-ION OTHERS         (A):  NULL ;  NULL ;  NULL
REMARK   3
REMARK   3  ISOTROPIC THERMAL FACTOR RESTRAINTS.     COUNT   RMS    WEIGHT
REMARK   3   MAIN-CHAIN BOND REFINED ATOMS  (A**2):  9137 ; 0.732 ; 1.500
REMARK   3   MAIN-CHAIN BOND OTHER ATOMS    (A**2):  NULL ;  NULL ;  NULL
REMARK   3   MAIN-CHAIN ANGLE REFINED ATOMS (A**2): 14193 ; 1.271 ; 2.000
REMARK   3   SIDE-CHAIN BOND REFINED ATOMS  (A**2):  6281 ; 1.875 ; 3.000
REMARK   3   SIDE-CHAIN ANGLE REFINED ATOMS (A**2):  5775 ; 2.904 ; 4.500
REMARK   3
REMARK   3 ANISOTROPIC THERMAL FACTOR RESTRAINTS.    COUNT   RMS   WEIGHT
REMARK   3   RIGID-BOND RESTRAINTS          (A**2):  NULL ;  NULL ;  NULL
REMARK   3   SPHERICITY; FREE ATOMS         (A**2):  NULL ;  NULL ;  NULL
REMARK   3   SPHERICITY; BONDED ATOMS       (A**2):  NULL ;  NULL ;  NULL
REMARK   3
REMARK   3  NCS RESTRAINTS STATISTICS
REMARK   3   NUMBER OF DIFFERENT NCS GROUPS : NULL
REMARK   3
REMARK   3  TLS DETAILS
REMARK   3   NUMBER OF TLS GROUPS  : NULL
REMARK   3
REMARK   3  BULK SOLVENT MODELLING.
REMARK   3   METHOD USED : MASK
REMARK   3   PARAMETERS FOR MASK CALCULATION
REMARK   3   VDW PROBE RADIUS   : 1.20
REMARK   3   ION PROBE RADIUS   : 0.80
REMARK   3   SHRINKAGE RADIUS   : 0.80
REMARK   3
REMARK   3  OTHER REFINEMENT REMARKS: HYDROGENS HAVE BEEN ADDED IN THE
REMARK   3  RIDING POSITIONS
REMARK   4
REMARK   4 3JYH COMPLIES WITH FORMAT V. 3.20, 01-DEC-08
REMARK 100
REMARK 100 THIS ENTRY HAS BEEN PROCESSED BY RCSB ON 23-SEP-09.
REMARK 100 THE RCSB ID CODE IS RCSB055318.
REMARK 200
REMARK 200 EXPERIMENTAL DETAILS
REMARK 200  EXPERIMENT TYPE                : X-RAY DIFFRACTION
REMARK 200  DATE OF DATA COLLECTION        : 18-MAR-09
REMARK 200  TEMPERATURE           (KELVIN) : 100
REMARK 200  PH                             : 7.5
REMARK 200  NUMBER OF CRYSTALS USED        : 1
REMARK 200
REMARK 200  SYNCHROTRON              (Y/N) : Y
REMARK 200  RADIATION SOURCE               : APS
REMARK 200  BEAMLINE                       : 19-ID
REMARK 200  X-RAY GENERATOR MODEL          : NULL
REMARK 200  MONOCHROMATIC OR LAUE    (M/L) : M
REMARK 200  WAVELENGTH OR RANGE        (A) : 0.9794
REMARK 200  MONOCHROMATOR                  : SI(111)
REMARK 200  OPTICS                         : NULL
REMARK 200
REMARK 200  DETECTOR TYPE                  : CCD
REMARK 200  DETECTOR MANUFACTURER          : ADSC QUANTUM 315
REMARK 200  INTENSITY-INTEGRATION SOFTWARE : DENZO
REMARK 200  DATA SCALING SOFTWARE          : HKL-3000
REMARK 200
REMARK 200  NUMBER OF UNIQUE REFLECTIONS   : 127772
REMARK 200  RESOLUTION RANGE HIGH      (A) : 2.190
REMARK 200  RESOLUTION RANGE LOW       (A) : 100.000
REMARK 200  REJECTION CRITERIA  (SIGMA(I)) : 0.000
REMARK 200
REMARK 200 OVERALL.
REMARK 200  COMPLETENESS FOR RANGE     (%) : 100.0
REMARK 200  DATA REDUNDANCY                : 9.800
REMARK 200  R MERGE                    (I) : NULL
REMARK 200  R SYM                      (I) : 0.11100
REMARK 200   FOR THE DATA SET  : 25.9000
REMARK 200
REMARK 200 IN THE HIGHEST RESOLUTION SHELL.
REMARK 200  HIGHEST RESOLUTION SHELL, RANGE HIGH (A) : 2.19
REMARK 200  HIGHEST RESOLUTION SHELL, RANGE LOW  (A) : 2.22
REMARK 200  COMPLETENESS FOR SHELL     (%) : 99.9
REMARK 200  DATA REDUNDANCY IN SHELL       : NULL
REMARK 200  R MERGE FOR SHELL          (I) : NULL
REMARK 200  R SYM FOR SHELL            (I) : NULL
REMARK 200   FOR SHELL         : NULL
REMARK 200
REMARK 200 DIFFRACTION PROTOCOL: SINGLE WAVELENGTH
REMARK 200 METHOD USED TO DETERMINE THE STRUCTURE: MOLECULAR REPLACEMENT
REMARK 200 SOFTWARE USED: MOLREP
REMARK 200 STARTING MODEL: NULL
REMARK 200
REMARK 200 REMARK: NULL
REMARK 280
REMARK 280 CRYSTAL
REMARK 280 SOLVENT CONTENT, VS   (%): 59.67
REMARK 280 MATTHEWS COEFFICIENT, VM (ANGSTROMS**3/DA): 3.05
REMARK 280
REMARK 280 CRYSTALLIZATION CONDITIONS: 2M AMMONIUM SULFATE, 0.2M SODIUM
REMARK 280  ACETATE, 0.1M HEPES, 5% MPD, PH 7.5, VAPOR DIFFUSION, SITTING
REMARK 280  DROP, TEMPERATURE 300K
REMARK 290
REMARK 290 CRYSTALLOGRAPHIC SYMMETRY
REMARK 290 SYMMETRY OPERATORS FOR SPACE GROUP: P 1 21 1
REMARK 290
REMARK 290      SYMOP   SYMMETRY
REMARK 290     NNNMMM   OPERATOR
REMARK 290       1555   X,Y,Z
REMARK 290       2555   -X,Y+1/2,-Z
REMARK 290
REMARK 290     WHERE NNN -> OPERATOR NUMBER
REMARK 290           MMM -> TRANSLATION VECTOR
REMARK 290
REMARK 290 CRYSTALLOGRAPHIC SYMMETRY TRANSFORMATIONS
REMARK 290 THE FOLLOWING TRANSFORMATIONS OPERATE ON THE ATOM/HETATM
REMARK 290 RECORDS IN THIS ENTRY TO PRODUCE CRYSTALLOGRAPHICALLY
REMARK 290 RELATED MOLECULES.
REMARK 290   SMTRY1   1  1.000000  0.000000  0.000000        0.00000
REMARK 290   SMTRY2   1  0.000000  1.000000  0.000000        0.00000
REMARK 290   SMTRY3   1  0.000000  0.000000  1.000000        0.00000
REMARK 290   SMTRY1   2 -1.000000  0.000000  0.000000        0.00000
REMARK 290   SMTRY2   2  0.000000  1.000000  0.000000       65.10750
REMARK 290   SMTRY3   2  0.000000  0.000000 -1.000000        0.00000
REMARK 290
REMARK 290 REMARK: NULL
REMARK 300
REMARK 300 BIOMOLECULE: 1, 2
REMARK 300 SEE REMARK 350 FOR THE AUTHOR PROVIDED AND/OR PROGRAM
REMARK 300 GENERATED ASSEMBLY INFORMATION FOR THE STRUCTURE IN
REMARK 300 THIS ENTRY. THE REMARK MAY ALSO PROVIDE INFORMATION ON
REMARK 300 BURIED SURFACE AREA.
REMARK 350
REMARK 350 COORDINATES FOR A COMPLETE MULTIMER REPRESENTING THE KNOWN
REMARK 350 BIOLOGICALLY SIGNIFICANT OLIGOMERIZATION STATE OF THE
REMARK 350 MOLECULE CAN BE GENERATED BY APPLYING BIOMT TRANSFORMATIONS
REMARK 350 GIVEN BELOW.  BOTH NON-CRYSTALLOGRAPHIC AND
REMARK 350 CRYSTALLOGRAPHIC OPERATIONS ARE GIVEN.
REMARK 350
REMARK 350 BIOMOLECULE: 1
REMARK 350 SOFTWARE DETERMINED QUATERNARY STRUCTURE: DIMERIC
REMARK 350 SOFTWARE USED: PISA
REMARK 350 TOTAL BURIED SURFACE AREA: 4160 ANGSTROM**2
REMARK 350 SURFACE AREA OF THE COMPLEX: 31530 ANGSTROM**2
REMARK 350 CHANGE IN SOLVENT FREE ENERGY: -10.0 KCAL/MOL
REMARK 350 APPLY THE FOLLOWING TO CHAINS: A, B
REMARK 350   BIOMT1   1  1.000000  0.000000  0.000000        0.00000
REMARK 350   BIOMT2   1  0.000000  1.000000  0.000000        0.00000
REMARK 350   BIOMT3   1  0.000000  0.000000  1.000000        0.00000
REMARK 350
REMARK 350 BIOMOLECULE: 2
REMARK 350 SOFTWARE DETERMINED QUATERNARY STRUCTURE: DIMERIC
REMARK 350 SOFTWARE USED: PISA
REMARK 350 TOTAL BURIED SURFACE AREA: 4200 ANGSTROM**2
REMARK 350 SURFACE AREA OF THE COMPLEX: 31160 ANGSTROM**2
REMARK 350 CHANGE IN SOLVENT FREE ENERGY: -9.9 KCAL/MOL
REMARK 350 APPLY THE FOLLOWING TO CHAINS: C, D
REMARK 350   BIOMT1   1  1.000000  0.000000  0.000000        0.00000
REMARK 350   BIOMT2   1  0.000000  1.000000  0.000000        0.00000
REMARK 350   BIOMT3   1  0.000000  0.000000  1.000000        0.00000
REMARK 465
REMARK 465 MISSING RESIDUES
REMARK 465 THE FOLLOWING RESIDUES WERE NOT LOCATED IN THE
REMARK 465 EXPERIMENT. (M=MODEL NUMBER; RES=RESIDUE NAME; C=CHAIN
REMARK 465 IDENTIFIER; SSSEQ=SEQUENCE NUMBER; I=INSERTION CODE.)
REMARK 465
REMARK 465   M RES C SSSEQI
REMARK 465     GLY A    24
REMARK 465     ALA A    25
REMARK 465     MET A    26
REMARK 465     ASP A    27
REMARK 465     GLN A   480
REMARK 465     GLN A   481
REMARK 465     PRO A   482
REMARK 465     ALA A   483
REMARK 465     LEU A   484
REMARK 465     ARG A   485
REMARK 465     GLY A   486
REMARK 465     GLY A   487
REMARK 465     PRO A   488
REMARK 465     ARG A   489
REMARK 465     LEU A   490
REMARK 465     SER A   491
REMARK 465     LEU A   492
REMARK 465     GLY B    24
REMARK 465     ALA B    25
REMARK 465     MET B    26
REMARK 465     ASP B    27
REMARK 465     GLN B   480
REMARK 465     GLN B   481
REMARK 465     PRO B   482
REMARK 465     ALA B   483
REMARK 465     LEU B   484
REMARK 465     ARG B   485
REMARK 465     GLY B   486
REMARK 465     GLY B   487
REMARK 465     PRO B   488
REMARK 465     ARG B   489
REMARK 465     LEU B   490
REMARK 465     SER B   491
REMARK 465     LEU B   492
REMARK 465     GLY C    24
REMARK 465     ALA C    25
REMARK 465     MET C    26
REMARK 465     ASP C    27
REMARK 465     GLU C   479
REMARK 465     GLN C   480
REMARK 465     GLN C   481
REMARK 465     PRO C   482
REMARK 465     ALA C   483
REMARK 465     LEU C   484
REMARK 465     ARG C   485
REMARK 465     GLY C   486
REMARK 465     GLY C   487
REMARK 465     PRO C   488
REMARK 465     ARG C   489
REMARK 465     LEU C   490
REMARK 465     SER C   491
REMARK 465     LEU C   492
REMARK 465     GLY D    24
REMARK 465     ALA D    25
REMARK 465     MET D    26
REMARK 465     ASP D    27
REMARK 465     ARG D   478
REMARK 465     GLU D   479
REMARK 465     GLN D   480
REMARK 465     GLN D   481
REMARK 465     PRO D   482
REMARK 465     ALA D   483
REMARK 465     LEU D   484
REMARK 465     ARG D   485
REMARK 465     GLY D   486
REMARK 465     GLY D   487
REMARK 465     PRO D   488
REMARK 465     ARG D   489
REMARK 465     LEU D   490
REMARK 465     SER D   491
REMARK 465     LEU D   492
REMARK 470
REMARK 470 MISSING ATOM
REMARK 470 THE FOLLOWING RESIDUES HAVE MISSING ATOMS(M=MODEL NUMBER;
REMARK 470 RES=RESIDUE NAME; C=CHAIN IDENTIFIER; SSEQ=SEQUENCE NUMBER;
REMARK 470 I=INSERTION CODE):
REMARK 470   M RES CSSEQI  ATOMS
REMARK 470     ASP A  28    CG   OD1  OD2
REMARK 470     ARG A  34    NH1  NH2
REMARK 470     ARG A  47    CG   CD   NE   CZ   NH1  NH2
REMARK 470     ARG A  62    CZ   NH1  NH2
REMARK 470     ARG A  66    CZ   NH1  NH2
REMARK 470     GLU A  68    CG   CD   OE1  OE2
REMARK 470     ALA A  89    CB
REMARK 470     GLN A 119    CG   CD   OE1  NE2
REMARK 470     ARG A 203    NE   CZ   NH1  NH2
REMARK 470     GLN A 212    CG   CD   OE1  NE2
REMARK 470     LYS A 215    CE   NZ
REMARK 470     GLN A 218    CG   CD   OE1  NE2
REMARK 470     GLU A 252    CG   CD   OE1  OE2
REMARK 470     LYS A 253    CE   NZ
REMARK 470     ARG A 327    NE   CZ   NH1  NH2
REMARK 470     ARG A 380    CZ   NH1  NH2
REMARK 470     ARG A 427    CG   CD   NE   CZ   NH1  NH2
REMARK 470     GLN A 439    CD   OE1  NE2
REMARK 470     LYS A 463    CD   CE   NZ
REMARK 470     GLU A 471    CD   OE1  OE2
REMARK 470     LYS A 474    CG   CD   CE   NZ
REMARK 470     ARG A 477    CZ   NH1  NH2
REMARK 470     ARG A 478    CG   CD   NE   CZ   NH1  NH2
REMARK 470     GLU A 479    CG   CD   OE1  OE2
REMARK 470     ASP B  28    CG   OD1  OD2
REMARK 470     GLN B  32    CD   OE1  NE2
REMARK 470     ARG B  47    CZ   NH1  NH2
REMARK 470     ARG B  62    NE   CZ   NH1  NH2
REMARK 470     ARG B  66    CG   CD   NE   CZ   NH1  NH2
REMARK 470     GLU B  68    CG   CD   OE1  OE2
REMARK 470     ALA B  89    CB
REMARK 470     GLU B  97    CD   OE1  OE2
REMARK 470     ARG B  98    CD   NE   CZ   NH1  NH2
REMARK 470     GLN B 119    CG   CD   OE1  NE2
REMARK 470     LYS B 215    CE   NZ
REMARK 470     ARG B 221    CZ   NH1  NH2
REMARK 470     GLU B 252    CG   CD   OE1  OE2
REMARK 470     LYS B 253    NZ
REMARK 470     ARG B 327    NE   CZ   NH1  NH2
REMARK 470     GLU B 376    CG   CD   OE1  OE2
REMARK 470     ARG B 380    CG   CD   NE   CZ   NH1  NH2
REMARK 470     LYS B 463    CD   CE   NZ
REMARK 470     GLU B 471    CG   CD   OE1  OE2
REMARK 470     LYS B 474    CG   CD   CE   NZ
REMARK 470     ARG B 478    CG   CD   NE   CZ   NH1  NH2
REMARK 470     GLU B 479    CG   CD   OE1  OE2
REMARK 470     ASP C  28    CG   OD1  OD2
REMARK 470     ARG C  47    CZ   NH1  NH2
REMARK 470     ARG C  66    NE   CZ   NH1  NH2
REMARK 470     GLU C  68    CG   CD   OE1  OE2
REMARK 470     ALA C  89    CB
REMARK 470     GLU C  97    CG   CD   OE1  OE2
REMARK 470     ASP C 153    CG   OD1  OD2
REMARK 470     ASP C 197    CG   OD1  OD2
REMARK 470     ASN C 199    CG   OD1  ND2
REMARK 470     LYS C 215    CG   CD   CE   NZ
REMARK 470     GLN C 218    CG   CD   OE1  NE2
REMARK 470     GLU C 252    CG   CD   OE1  OE2
REMARK 470     LYS C 253    CE   NZ
REMARK 470     LYS C 290    CD   CE   NZ
REMARK 470     ARG C 327    CG   CD   NE   CZ   NH1  NH2
REMARK 470     ARG C 427    CG   CD   NE   CZ   NH1  NH2
REMARK 470     GLU C 471    CD   OE1  OE2
REMARK 470     LYS C 474    CG   CD   CE   NZ
REMARK 470     ARG C 477    CG   CD   NE   CZ   NH1  NH2
REMARK 470     ARG C 478    CG   CD   NE   CZ   NH1  NH2
REMARK 470     ASP D  28    CG   OD1  OD2
REMARK 470     ARG D  47    NE   CZ   NH1  NH2
REMARK 470     ARG D  62    CG   CD   NE   CZ   NH1  NH2
REMARK 470     ARG D  66    CG   CD   NE   CZ   NH1  NH2
REMARK 470     GLU D  68    CG   CD   OE1  OE2
REMARK 470     ALA D  89    CB
REMARK 470     GLU D  97    CG   CD   OE1  OE2
REMARK 470     LYS D 112    CD   CE   NZ
REMARK 470     GLN D 119    CG   CD   OE1  NE2
REMARK 470     LYS D 215    CE   NZ
REMARK 470     GLN D 218    CG   CD   OE1  NE2
REMARK 470     GLU D 222    CG   CD   OE1  OE2
REMARK 470     LEU D 232    CG   CD1  CD2
REMARK 470     GLU D 252    CG   CD   OE1  OE2
REMARK 470     LYS D 253    CG   CD   CE   NZ
REMARK 470     ARG D 327    CG   CD   NE   CZ   NH1  NH2
REMARK 470     GLU D 376    CG   CD   OE1  OE2
REMARK 470     ARG D 380    CG   CD   NE   CZ   NH1  NH2
REMARK 470     ASP D 384    CG   OD1  OD2
REMARK 470     LYS D 463    CG   CD   CE   NZ
REMARK 470     GLU D 471    CG   CD   OE1  OE2
REMARK 470     LYS D 474    CE   NZ
REMARK 500
REMARK 500 GEOMETRY AND STEREOCHEMISTRY
REMARK 500 SUBTOPIC: CLOSE CONTACTS IN SAME ASYMMETRIC UNIT
REMARK 500
REMARK 500 THE FOLLOWING ATOMS ARE IN CLOSE CONTACT.
REMARK 500
REMARK 500  ATM1  RES C  SSEQI   ATM2  RES C  SSEQI           DISTANCE
REMARK 500   O    HOH A   653     O    HOH A  1230              2.12
REMARK 500   O    HOH B   628     O    HOH B   667              2.12
REMARK 500   NE2  GLN D   247     OD1  ASP D   324              2.18
REMARK 500
REMARK 500 REMARK: NULL
REMARK 500
REMARK 500 GEOMETRY AND STEREOCHEMISTRY
REMARK 500 SUBTOPIC: TORSION ANGLES
REMARK 500
REMARK 500 TORSION ANGLES OUTSIDE THE EXPECTED RAMACHANDRAN REGIONS:
REMARK 500 (M=MODEL NUMBER; RES=RESIDUE NAME; C=CHAIN IDENTIFIER;
REMARK 500 SSEQ=SEQUENCE NUMBER; I=INSERTION CODE).
REMARK 500
REMARK 500 STANDARD TABLE:
REMARK 500 FORMAT:(10X,I3,1X,A3,1X,A1,I4,A1,4X,F7.2,3X,F7.2)
REMARK 500
REMARK 500 EXPECTED VALUES: GJ KLEYWEGT AND TA JONES (1996). PHI/PSI-
REMARK 500 CHOLOGY: RAMACHANDRAN REVISITED. STRUCTURE 4, 1395 - 1400
REMARK 500
REMARK 500  M RES CSSEQI        PSI       PHI
REMARK 500    ARG A  66      -10.40    -49.15
REMARK 500    ASN A  77     -142.92   -107.92
REMARK 500    TYR A 109       -1.40     77.11
REMARK 500    SER A 113       73.54   -104.42
REMARK 500    ALA A 151       48.11   -149.54
REMARK 500    SER A 162     -136.41     66.62
REMARK 500    SER A 213      108.73   -164.00
REMARK 500    SER A 250      -23.87   -156.86
REMARK 500    PHE A 280      -76.57    -92.17
REMARK 500    ASN A 315       45.51   -146.69
REMARK 500    THR A 353      -66.69   -128.93
REMARK 500    VAL A 364      -58.00   -120.76
REMARK 500    TRP A 400       -8.11     85.61
REMARK 500    ALA A 442     -133.95    -95.00
REMARK 500    HIS A 444       53.39     33.24
REMARK 500    ASN B  77     -146.86   -106.36
REMARK 500    TYR B 109       -0.72     76.27
REMARK 500    SER B 162     -138.33     71.72
REMARK 500    SER B 213      115.38   -166.63
REMARK 500    SER B 250      -32.17   -149.79
REMARK 500    ASP B 279       64.68   -152.91
REMARK 500    PHE B 280      -75.29    -95.33
REMARK 500    ASN B 315       40.47   -142.52
REMARK 500    THR B 353      -68.44   -134.19
REMARK 500    TRP B 400       -1.86     87.04
REMARK 500    ALA B 442     -134.46    -92.05
REMARK 500    HIS B 444       53.33     36.15
REMARK 500    ARG C  66       -4.99    -54.73
REMARK 500    ASN C  77     -141.85   -110.11
REMARK 500    GLU C  78       45.01    -84.48
REMARK 500    SER C  88       50.19   -101.31
REMARK 500    TYR C 109       -1.52     80.45
REMARK 500    SER C 113       75.31   -104.48
REMARK 500    ALA C 151       56.14    -69.84
REMARK 500    SER C 162     -132.10     70.42
REMARK 500    SER C 250      -39.21   -145.04
REMARK 500    ASP C 279       63.78   -151.66
REMARK 500    PHE C 280      -72.86    -90.15
REMARK 500    ASN C 315       45.31   -144.37
REMARK 500    THR C 353      -65.33   -127.94
REMARK 500    TRP C 400       -8.90     81.13
REMARK 500    ALA C 442     -137.22    -92.48
REMARK 500    HIS C 444       60.39     28.84
REMARK 500    ARG D  62      -39.92    -35.64
REMARK 500    ARG D  66       -1.14    -48.08
REMARK 500    ASN D  77     -147.77   -116.81
REMARK 500    GLU D  78       46.84    -73.37
REMARK 500    SER D  88       53.36   -112.05
REMARK 500    TYR D 109       -3.08     74.61
REMARK 500    SER D 162     -135.61     68.47
REMARK 500    ALA D 235       55.85    -94.04
REMARK 500    MET D 272       35.98    -93.41
REMARK 500    PHE D 280      -66.32    -92.89
REMARK 500    ASN D 315       47.43   -151.35
REMARK 500    THR D 353      -67.23   -129.62
REMARK 500    VAL D 364      -53.01   -120.66
REMARK 500    TRP D 400       -9.15     84.46
REMARK 500    ALA D 442     -138.62    -80.44
REMARK 500    HIS D 444       68.33     22.93
REMARK 500
REMARK 500 REMARK: NULL
REMARK 525
REMARK 525 SOLVENT
REMARK 525
REMARK 525 THE SOLVENT MOLECULES HAVE CHAIN IDENTIFIERS THAT
REMARK 525 INDICATE THE POLYMER CHAIN WITH WHICH THEY ARE MOST
REMARK 525 CLOSELY ASSOCIATED. THE REMARK LISTS ALL THE SOLVENT
REMARK 525 MOLECULES WHICH ARE MORE THAN 5A AWAY FROM THE
REMARK 525 NEAREST POLYMER CHAIN (M = MODEL NUMBER;
REMARK 525 RES=RESIDUE NAME; C=CHAIN IDENTIFIER; SSEQ=SEQUENCE
REMARK 525 NUMBER; I=INSERTION CODE):
REMARK 525
REMARK 525  M RES CSSEQI
REMARK 525    HOH D1140        DISTANCE =  5.66 ANGSTROMS
REMARK 525    HOH D1204        DISTANCE =  5.34 ANGSTROMS
REMARK 525    HOH B 953        DISTANCE =  6.93 ANGSTROMS
REMARK 525    HOH B1018        DISTANCE =  6.23 ANGSTROMS
REMARK 525    HOH B1058        DISTANCE =  5.40 ANGSTROMS
REMARK 525    HOH B1212        DISTANCE =  7.11 ANGSTROMS
REMARK 800
REMARK 800 SITE
REMARK 800 SITE_IDENTIFIER: AC1
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE NAG A 1
REMARK 800 SITE_IDENTIFIER: AC2
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE BMA A 493
REMARK 800 SITE_IDENTIFIER: AC3
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE NAG A 494
REMARK 800 SITE_IDENTIFIER: AC4
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE NAG A 498
REMARK 800 SITE_IDENTIFIER: AC5
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE NAG A 495
REMARK 800 SITE_IDENTIFIER: AC6
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE NAG A 496
REMARK 800 SITE_IDENTIFIER: AC7
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE NAG A 497
REMARK 800 SITE_IDENTIFIER: AC8
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE NAG B 1
REMARK 800 SITE_IDENTIFIER: AC9
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE BMA B 493
REMARK 800 SITE_IDENTIFIER: BC1
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE NAG B 494
REMARK 800 SITE_IDENTIFIER: BC2
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE NAG B 497
REMARK 800 SITE_IDENTIFIER: BC3
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE NAG B 495
REMARK 800 SITE_IDENTIFIER: BC4
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE NAG B 496
REMARK 800 SITE_IDENTIFIER: BC5
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE BMA C 1
REMARK 800 SITE_IDENTIFIER: BC6
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE NAG C 493
REMARK 800 SITE_IDENTIFIER: BC7
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE NAG C 498
REMARK 800 SITE_IDENTIFIER: BC8
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE NAG C 494
REMARK 800 SITE_IDENTIFIER: BC9
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE NAG C 495
REMARK 800 SITE_IDENTIFIER: CC1
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE NAG C 496
REMARK 800 SITE_IDENTIFIER: CC2
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE NAG C 497
REMARK 800 SITE_IDENTIFIER: CC3
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE NAG D 1
REMARK 800 SITE_IDENTIFIER: CC4
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE NAG D 493
REMARK 800 SITE_IDENTIFIER: CC5
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE NAG D 494
REMARK 800 SITE_IDENTIFIER: CC6
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE NAG D 495
REMARK 800 SITE_IDENTIFIER: CC7
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE NAG D 496
DBREF  3JYH A   28   492  UNP    Q9UHL4   DPP2_HUMAN      28    492
DBREF  3JYH B   28   492  UNP    Q9UHL4   DPP2_HUMAN      28    492
DBREF  3JYH C   28   492  UNP    Q9UHL4   DPP2_HUMAN      28    492
DBREF  3JYH D   28   492  UNP    Q9UHL4   DPP2_HUMAN      28    492
SEQADV 3JYH GLY A   24  UNP  Q9UHL4              EXPRESSION TAG
SEQADV 3JYH ALA A   25  UNP  Q9UHL4              EXPRESSION TAG
SEQADV 3JYH MET A   26  UNP  Q9UHL4              EXPRESSION TAG
SEQADV 3JYH ASP A   27  UNP  Q9UHL4              EXPRESSION TAG
SEQADV 3JYH GLY B   24  UNP  Q9UHL4              EXPRESSION TAG
SEQADV 3JYH ALA B   25  UNP  Q9UHL4              EXPRESSION TAG
SEQADV 3JYH MET B   26  UNP  Q9UHL4              EXPRESSION TAG
SEQADV 3JYH ASP B   27  UNP  Q9UHL4              EXPRESSION TAG
SEQADV 3JYH GLY C   24  UNP  Q9UHL4              EXPRESSION TAG
SEQADV 3JYH ALA C   25  UNP  Q9UHL4              EXPRESSION TAG
SEQADV 3JYH MET C   26  UNP  Q9UHL4              EXPRESSION TAG
SEQADV 3JYH ASP C   27  UNP  Q9UHL4              EXPRESSION TAG
SEQADV 3JYH GLY D   24  UNP  Q9UHL4              EXPRESSION TAG
SEQADV 3JYH ALA D   25  UNP  Q9UHL4              EXPRESSION TAG
SEQADV 3JYH MET D   26  UNP  Q9UHL4              EXPRESSION TAG
SEQADV 3JYH ASP D   27  UNP  Q9UHL4              EXPRESSION TAG
SEQRES   1 A  469  GLY ALA MET ASP ASP PRO GLY PHE GLN GLU ARG PHE PHE
SEQRES   2 A  469  GLN GLN ARG LEU ASP HIS PHE ASN PHE GLU ARG PHE GLY
SEQRES   3 A  469  ASN LYS THR PHE PRO GLN ARG PHE LEU VAL SER ASP ARG
SEQRES   4 A  469  PHE TRP VAL ARG GLY GLU GLY PRO ILE PHE PHE TYR THR
SEQRES   5 A  469  GLY ASN GLU GLY ASP VAL TRP ALA PHE ALA ASN ASN SER
SEQRES   6 A  469  ALA PHE VAL ALA GLU LEU ALA ALA GLU ARG GLY ALA LEU
SEQRES   7 A  469  LEU VAL PHE ALA GLU HIS ARG TYR TYR GLY LYS SER LEU
SEQRES   8 A  469  PRO PHE GLY ALA GLN SER THR GLN ARG GLY HIS THR GLU
SEQRES   9 A  469  LEU LEU THR VAL GLU GLN ALA LEU ALA ASP PHE ALA GLU
SEQRES  10 A  469  LEU LEU ARG ALA LEU ARG ARG ASP LEU GLY ALA GLN ASP
SEQRES  11 A  469  ALA PRO ALA ILE ALA PHE GLY GLY SER TYR GLY GLY MET
SEQRES  12 A  469  LEU SER ALA TYR LEU ARG MET LYS TYR PRO HIS LEU VAL
SEQRES  13 A  469  ALA GLY ALA LEU ALA ALA SER ALA PRO VAL LEU ALA VAL
SEQRES  14 A  469  ALA GLY LEU GLY ASP SER ASN GLN PHE PHE ARG ASP VAL
SEQRES  15 A  469  THR ALA ASP PHE GLU GLY GLN SER PRO LYS CYS THR GLN
SEQRES  16 A  469  GLY VAL ARG GLU ALA PHE ARG GLN ILE LYS ASP LEU PHE
SEQRES  17 A  469  LEU GLN GLY ALA TYR ASP THR VAL ARG TRP GLU PHE GLY
SEQRES  18 A  469  THR CYS GLN PRO LEU SER ASP GLU LYS ASP LEU THR GLN
SEQRES  19 A  469  LEU PHE MET PHE ALA ARG ASN ALA PHE THR VAL LEU ALA
SEQRES  20 A  469  MET MET ASP TYR PRO TYR PRO THR ASP PHE LEU GLY PRO
SEQRES  21 A  469  LEU PRO ALA ASN PRO VAL LYS VAL GLY CYS ASP ARG LEU
SEQRES  22 A  469  LEU SER GLU ALA GLN ARG ILE THR GLY LEU ARG ALA LEU
SEQRES  23 A  469  ALA GLY LEU VAL TYR ASN ALA SER GLY SER GLU HIS CYS
SEQRES  24 A  469  TYR ASP ILE TYR ARG LEU TYR HIS SER CYS ALA ASP PRO
SEQRES  25 A  469  THR GLY CYS GLY THR GLY PRO ASP ALA ARG ALA TRP ASP
SEQRES  26 A  469  TYR GLN ALA CYS THR GLU ILE ASN LEU THR PHE ALA SER
SEQRES  27 A  469  ASN ASN VAL THR ASP MET PHE PRO ASP LEU PRO PHE THR
SEQRES  28 A  469  ASP GLU LEU ARG GLN ARG TYR CYS LEU ASP THR TRP GLY
SEQRES  29 A  469  VAL TRP PRO ARG PRO ASP TRP LEU LEU THR SER PHE TRP
SEQRES  30 A  469  GLY GLY ASP LEU ARG ALA ALA SER ASN ILE ILE PHE SER
SEQRES  31 A  469  ASN GLY ASN LEU ASP PRO TRP ALA GLY GLY GLY ILE ARG
SEQRES  32 A  469  ARG ASN LEU SER ALA SER VAL ILE ALA VAL THR ILE GLN
SEQRES  33 A  469  GLY GLY ALA HIS HIS LEU ASP LEU ARG ALA SER HIS PRO
SEQRES  34 A  469  GLU ASP PRO ALA SER VAL VAL GLU ALA ARG LYS LEU GLU
SEQRES  35 A  469  ALA THR ILE ILE GLY GLU TRP VAL LYS ALA ALA ARG ARG
SEQRES  36 A  469  GLU GLN GLN PRO ALA LEU ARG GLY GLY PRO ARG LEU SER
SEQRES  37 A  469  LEU
SEQRES   1 B  469  GLY ALA MET ASP ASP PRO GLY PHE GLN GLU ARG PHE PHE
SEQRES   2 B  469  GLN GLN ARG LEU ASP HIS PHE ASN PHE GLU ARG PHE GLY
SEQRES   3 B  469  ASN LYS THR PHE PRO GLN ARG PHE LEU VAL SER ASP ARG
SEQRES   4 B  469  PHE TRP VAL ARG GLY GLU GLY PRO ILE PHE PHE TYR THR
SEQRES   5 B  469  GLY ASN GLU GLY ASP VAL TRP ALA PHE ALA ASN ASN SER
SEQRES   6 B  469  ALA PHE VAL ALA GLU LEU ALA ALA GLU ARG GLY ALA LEU
SEQRES   7 B  469  LEU VAL PHE ALA GLU HIS ARG TYR TYR GLY LYS SER LEU
SEQRES   8 B  469  PRO PHE GLY ALA GLN SER THR GLN ARG GLY HIS THR GLU
SEQRES   9 B  469  LEU LEU THR VAL GLU GLN ALA LEU ALA ASP PHE ALA GLU
SEQRES  10 B  469  LEU LEU ARG ALA LEU ARG ARG ASP LEU GLY ALA GLN ASP
SEQRES  11 B  469  ALA PRO ALA ILE ALA PHE GLY GLY SER TYR GLY GLY MET
SEQRES  12 B  469  LEU SER ALA TYR LEU ARG MET LYS TYR PRO HIS LEU VAL
SEQRES  13 B  469  ALA GLY ALA LEU ALA ALA SER ALA PRO VAL LEU ALA VAL
SEQRES  14 B  469  ALA GLY LEU GLY ASP SER ASN GLN PHE PHE ARG ASP VAL
SEQRES  15 B  469  THR ALA ASP PHE GLU GLY GLN SER PRO LYS CYS THR GLN
SEQRES  16 B  469  GLY VAL ARG GLU ALA PHE ARG GLN ILE LYS ASP LEU PHE
SEQRES  17 B  469  LEU GLN GLY ALA TYR ASP THR VAL ARG TRP GLU PHE GLY
SEQRES  18 B  469  THR CYS GLN PRO LEU SER ASP GLU LYS ASP LEU THR GLN
SEQRES  19 B  469  LEU PHE MET PHE ALA ARG ASN ALA PHE THR VAL LEU ALA
SEQRES  20 B  469  MET MET ASP TYR PRO TYR PRO THR ASP PHE LEU GLY PRO
SEQRES  21 B  469  LEU PRO ALA ASN PRO VAL LYS VAL GLY CYS ASP ARG LEU
SEQRES  22 B  469  LEU SER GLU ALA GLN ARG ILE THR GLY LEU ARG ALA LEU
SEQRES  23 B  469  ALA GLY LEU VAL TYR ASN ALA SER GLY SER GLU HIS CYS
SEQRES  24 B  469  TYR ASP ILE TYR ARG LEU TYR HIS SER CYS ALA ASP PRO
SEQRES  25 B  469  THR GLY CYS GLY THR GLY PRO ASP ALA ARG ALA TRP ASP
SEQRES  26 B  469  TYR GLN ALA CYS THR GLU ILE ASN LEU THR PHE ALA SER
SEQRES  27 B  469  ASN ASN VAL THR ASP MET PHE PRO ASP LEU PRO PHE THR
SEQRES  28 B  469  ASP GLU LEU ARG GLN ARG TYR CYS LEU ASP THR TRP GLY
SEQRES  29 B  469  VAL TRP PRO ARG PRO ASP TRP LEU LEU THR SER PHE TRP
SEQRES  30 B  469  GLY GLY ASP LEU ARG ALA ALA SER ASN ILE ILE PHE SER
SEQRES  31 B  469  ASN GLY ASN LEU ASP PRO TRP ALA GLY GLY GLY ILE ARG
SEQRES  32 B  469  ARG ASN LEU SER ALA SER VAL ILE ALA VAL THR ILE GLN
SEQRES  33 B  469  GLY GLY ALA HIS HIS LEU ASP LEU ARG ALA SER HIS PRO
SEQRES  34 B  469  GLU ASP PRO ALA SER VAL VAL GLU ALA ARG LYS LEU GLU
SEQRES  35 B  469  ALA THR ILE ILE GLY GLU TRP VAL LYS ALA ALA ARG ARG
SEQRES  36 B  469  GLU GLN GLN PRO ALA LEU ARG GLY GLY PRO ARG LEU SER
SEQRES  37 B  469  LEU
SEQRES   1 C  469  GLY ALA MET ASP ASP PRO GLY PHE GLN GLU ARG PHE PHE
SEQRES   2 C  469  GLN GLN ARG LEU ASP HIS PHE ASN PHE GLU ARG PHE GLY
SEQRES   3 C  469  ASN LYS THR PHE PRO GLN ARG PHE LEU VAL SER ASP ARG
SEQRES   4 C  469  PHE TRP VAL ARG GLY GLU GLY PRO ILE PHE PHE TYR THR
SEQRES   5 C  469  GLY ASN GLU GLY ASP VAL TRP ALA PHE ALA ASN ASN SER
SEQRES   6 C  469  ALA PHE VAL ALA GLU LEU ALA ALA GLU ARG GLY ALA LEU
SEQRES   7 C  469  LEU VAL PHE ALA GLU HIS ARG TYR TYR GLY LYS SER LEU
SEQRES   8 C  469  PRO PHE GLY ALA GLN SER THR GLN ARG GLY HIS THR GLU
SEQRES   9 C  469  LEU LEU THR VAL GLU GLN ALA LEU ALA ASP PHE ALA GLU
SEQRES  10 C  469  LEU LEU ARG ALA LEU ARG ARG ASP LEU GLY ALA GLN ASP
SEQRES  11 C  469  ALA PRO ALA ILE ALA PHE GLY GLY SER TYR GLY GLY MET
SEQRES  12 C  469  LEU SER ALA TYR LEU ARG MET LYS TYR PRO HIS LEU VAL
SEQRES  13 C  469  ALA GLY ALA LEU ALA ALA SER ALA PRO VAL LEU ALA VAL
SEQRES  14 C  469  ALA GLY LEU GLY ASP SER ASN GLN PHE PHE ARG ASP VAL
SEQRES  15 C  469  THR ALA ASP PHE GLU GLY GLN SER PRO LYS CYS THR GLN
SEQRES  16 C  469  GLY VAL ARG GLU ALA PHE ARG GLN ILE LYS ASP LEU PHE
SEQRES  17 C  469  LEU GLN GLY ALA TYR ASP THR VAL ARG TRP GLU PHE GLY
SEQRES  18 C  469  THR CYS GLN PRO LEU SER ASP GLU LYS ASP LEU THR GLN
SEQRES  19 C  469  LEU PHE MET PHE ALA ARG ASN ALA PHE THR VAL LEU ALA
SEQRES  20 C  469  MET MET ASP TYR PRO TYR PRO THR ASP PHE LEU GLY PRO
SEQRES  21 C  469  LEU PRO ALA ASN PRO VAL LYS VAL GLY CYS ASP ARG LEU
SEQRES  22 C  469  LEU SER GLU ALA GLN ARG ILE THR GLY LEU ARG ALA LEU
SEQRES  23 C  469  ALA GLY LEU VAL TYR ASN ALA SER GLY SER GLU HIS CYS
SEQRES  24 C  469  TYR ASP ILE TYR ARG LEU TYR HIS SER CYS ALA ASP PRO
SEQRES  25 C  469  THR GLY CYS GLY THR GLY PRO ASP ALA ARG ALA TRP ASP
SEQRES  26 C  469  TYR GLN ALA CYS THR GLU ILE ASN LEU THR PHE ALA SER
SEQRES  27 C  469  ASN ASN VAL THR ASP MET PHE PRO ASP LEU PRO PHE THR
SEQRES  28 C  469  ASP GLU LEU ARG GLN ARG TYR CYS LEU ASP THR TRP GLY
SEQRES  29 C  469  VAL TRP PRO ARG PRO ASP TRP LEU LEU THR SER PHE TRP
SEQRES  30 C  469  GLY GLY ASP LEU ARG ALA ALA SER ASN ILE ILE PHE SER
SEQRES  31 C  469  ASN GLY ASN LEU ASP PRO TRP ALA GLY GLY GLY ILE ARG
SEQRES  32 C  469  ARG ASN LEU SER ALA SER VAL ILE ALA VAL THR ILE GLN
SEQRES  33 C  469  GLY GLY ALA HIS HIS LEU ASP LEU ARG ALA SER HIS PRO
SEQRES  34 C  469  GLU ASP PRO ALA SER VAL VAL GLU ALA ARG LYS LEU GLU
SEQRES  35 C  469  ALA THR ILE ILE GLY GLU TRP VAL LYS ALA ALA ARG ARG
SEQRES  36 C  469  GLU GLN GLN PRO ALA LEU ARG GLY GLY PRO ARG LEU SER
SEQRES  37 C  469  LEU
SEQRES   1 D  469  GLY ALA MET ASP ASP PRO GLY PHE GLN GLU ARG PHE PHE
SEQRES   2 D  469  GLN GLN ARG LEU ASP HIS PHE ASN PHE GLU ARG PHE GLY
SEQRES   3 D  469  ASN LYS THR PHE PRO GLN ARG PHE LEU VAL SER ASP ARG
SEQRES   4 D  469  PHE TRP VAL ARG GLY GLU GLY PRO ILE PHE PHE TYR THR
SEQRES   5 D  469  GLY ASN GLU GLY ASP VAL TRP ALA PHE ALA ASN ASN SER
SEQRES   6 D  469  ALA PHE VAL ALA GLU LEU ALA ALA GLU ARG GLY ALA LEU
SEQRES   7 D  469  LEU VAL PHE ALA GLU HIS ARG TYR TYR GLY LYS SER LEU
SEQRES   8 D  469  PRO PHE GLY ALA GLN SER THR GLN ARG GLY HIS THR GLU
SEQRES   9 D  469  LEU LEU THR VAL GLU GLN ALA LEU ALA ASP PHE ALA GLU
SEQRES  10 D  469  LEU LEU ARG ALA LEU ARG ARG ASP LEU GLY ALA GLN ASP
SEQRES  11 D  469  ALA PRO ALA ILE ALA PHE GLY GLY SER TYR GLY GLY MET
SEQRES  12 D  469  LEU SER ALA TYR LEU ARG MET LYS TYR PRO HIS LEU VAL
SEQRES  13 D  469  ALA GLY ALA LEU ALA ALA SER ALA PRO VAL LEU ALA VAL
SEQRES  14 D  469  ALA GLY LEU GLY ASP SER ASN GLN PHE PHE ARG ASP VAL
SEQRES  15 D  469  THR ALA ASP PHE GLU GLY GLN SER PRO LYS CYS THR GLN
SEQRES  16 D  469  GLY VAL ARG GLU ALA PHE ARG GLN ILE LYS ASP LEU PHE
SEQRES  17 D  469  LEU GLN GLY ALA TYR ASP THR VAL ARG TRP GLU PHE GLY
SEQRES  18 D  469  THR CYS GLN PRO LEU SER ASP GLU LYS ASP LEU THR GLN
SEQRES  19 D  469  LEU PHE MET PHE ALA ARG ASN ALA PHE THR VAL LEU ALA
SEQRES  20 D  469  MET MET ASP TYR PRO TYR PRO THR ASP PHE LEU GLY PRO
SEQRES  21 D  469  LEU PRO ALA ASN PRO VAL LYS VAL GLY CYS ASP ARG LEU
SEQRES  22 D  469  LEU SER GLU ALA GLN ARG ILE THR GLY LEU ARG ALA LEU
SEQRES  23 D  469  ALA GLY LEU VAL TYR ASN ALA SER GLY SER GLU HIS CYS
SEQRES  24 D  469  TYR ASP ILE TYR ARG LEU TYR HIS SER CYS ALA ASP PRO
SEQRES  25 D  469  THR GLY CYS GLY THR GLY PRO ASP ALA ARG ALA TRP ASP
SEQRES  26 D  469  TYR GLN ALA CYS THR GLU ILE ASN LEU THR PHE ALA SER
SEQRES  27 D  469  ASN ASN VAL THR ASP MET PHE PRO ASP LEU PRO PHE THR
SEQRES  28 D  469  ASP GLU LEU ARG GLN ARG TYR CYS LEU ASP THR TRP GLY
SEQRES  29 D  469  VAL TRP PRO ARG PRO ASP TRP LEU LEU THR SER PHE TRP
SEQRES  30 D  469  GLY GLY ASP LEU ARG ALA ALA SER ASN ILE ILE PHE SER
SEQRES  31 D  469  ASN GLY ASN LEU ASP PRO TRP ALA GLY GLY GLY ILE ARG
SEQRES  32 D  469  ARG ASN LEU SER ALA SER VAL ILE ALA VAL THR ILE GLN
SEQRES  33 D  469  GLY GLY ALA HIS HIS LEU ASP LEU ARG ALA SER HIS PRO
SEQRES  34 D  469  GLU ASP PRO ALA SER VAL VAL GLU ALA ARG LYS LEU GLU
SEQRES  35 D  469  ALA THR ILE ILE GLY GLU TRP VAL LYS ALA ALA ARG ARG
SEQRES  36 D  469  GLU GLN GLN PRO ALA LEU ARG GLY GLY PRO ARG LEU SER
SEQRES  37 D  469  LEU
MODRES 3JYH ASN A   50  ASN  GLYCOSYLATION SITE
MODRES 3JYH ASN A   86  ASN  GLYCOSYLATION SITE
MODRES 3JYH ASN A  315  ASN  GLYCOSYLATION SITE
MODRES 3JYH ASN A  363  ASN  GLYCOSYLATION SITE
MODRES 3JYH ASN B   86  ASN  GLYCOSYLATION SITE
MODRES 3JYH ASN B  315  ASN  GLYCOSYLATION SITE
MODRES 3JYH ASN B  363  ASN  GLYCOSYLATION SITE
MODRES 3JYH ASN C   50  ASN  GLYCOSYLATION SITE
MODRES 3JYH ASN C   86  ASN  GLYCOSYLATION SITE
MODRES 3JYH ASN C  315  ASN  GLYCOSYLATION SITE
MODRES 3JYH ASN C  363  ASN  GLYCOSYLATION SITE
MODRES 3JYH ASN D   86  ASN  GLYCOSYLATION SITE
MODRES 3JYH ASN D  315  ASN  GLYCOSYLATION SITE
MODRES 3JYH ASN D  363  ASN  GLYCOSYLATION SITE
HET    NAG  A   1      14
HET    BMA  A 493      11
HET    NAG  A 494      14
HET    NAG  A 498      14
HET    NAG  A 495      14
HET    NAG  A 496      14
HET    NAG  A 497      14
HET    NAG  B   1      14
HET    BMA  B 493      11
HET    NAG  B 494      14
HET    NAG  B 497      14
HET    NAG  B 495      14
HET    NAG  B 496      14
HET    BMA  C   1      11
HET    NAG  C 493      14
HET    NAG  C 498      14
HET    NAG  C 494      14
HET    NAG  C 495      14
HET    NAG  C 496      14
HET    NAG  C 497      14
HET    NAG  D   1      14
HET    NAG  D 493      14
HET    NAG  D 494      14
HET    NAG  D 495      14
HET    NAG  D 496      14
HETNAM     NAG N-ACETYL-D-GLUCOSAMINE
HETNAM     BMA BETA-D-MANNOSE
HETSYN     NAG NAG
FORMUL   5  NAG    22(C8 H15 N O6)
FORMUL   6  BMA    3(C6 H12 O6)
FORMUL  19  HOH   *946(H2 O)
HELIX    1   1 ASP A   80  SER A   88  1                                   9
HELIX    2   2 SER A   88  GLY A   99  1                                  12
HELIX    3   3 PHE A  116  GLN A  122  5                                   7
HELIX    4   4 THR A  130  LEU A  149  1                                  20
HELIX    5   5 SER A  162  TYR A  175  1                                  14
HELIX    6   6 LEU A  190  GLY A  194  5                                   5
HELIX    7   7 ASN A  199  SER A  213  1                                  15
HELIX    8   8 SER A  213  GLN A  233  1                                  21
HELIX    9   9 ALA A  235  GLY A  244  1                                  10
HELIX   10  10 ASP A  251  MET A  272  1                                  22
HELIX   11  11 ASN A  287  SER A  298  1                                  12
HELIX   12  12 GLN A  301  ASN A  315  1                                  15
HELIX   13  13 ASP A  324  TYR A  329  1                                   6
HELIX   14  14 GLY A  341  CYS A  352  1                                  12
HELIX   15  15 THR A  374  GLY A  387  1                                  14
HELIX   16  16 ASP A  393  TRP A  400  1                                   8
HELIX   17  17 ASP A  418  GLY A  424  5                                   7
HELIX   18  18 HIS A  444  ARG A  448  5                                   5
HELIX   19  19 PRO A  455  GLU A  479  1                                  25
HELIX   20  20 ASP B   80  SER B   88  1                                   9
HELIX   21  21 SER B   88  GLY B   99  1                                  12
HELIX   22  22 PHE B  116  GLN B  122  5                                   7
HELIX   23  23 THR B  130  LEU B  149  1                                  20
HELIX   24  24 SER B  162  TYR B  175  1                                  14
HELIX   25  25 LEU B  190  GLY B  194  5                                   5
HELIX   26  26 ASN B  199  SER B  213  1                                  15
HELIX   27  27 SER B  213  GLN B  233  1                                  21
HELIX   28  28 ALA B  235  GLY B  244  1                                  10
HELIX   29  29 ASP B  251  MET B  272  1                                  22
HELIX   30  30 ASN B  287  SER B  298  1                                  12
HELIX   31  31 GLN B  301  ASN B  315  1                                  15
HELIX   32  32 ASP B  324  TYR B  329  1                                   6
HELIX   33  33 GLY B  341  CYS B  352  1                                  12
HELIX   34  34 THR B  374  GLY B  387  1                                  14
HELIX   35  35 ASP B  393  TRP B  400  1                                   8
HELIX   36  36 TRP B  420  GLY B  424  5                                   5
HELIX   37  37 HIS B  444  ARG B  448  5                                   5
HELIX   38  38 PRO B  455  GLU B  479  1                                  25
HELIX   39  39 ASP C   80  SER C   88  1                                   9
HELIX   40  40 SER C   88  GLY C   99  1                                  12
HELIX   41  41 PHE C  116  GLN C  122  5                                   7
HELIX   42  42 HIS C  125  LEU C  129  5                                   5
HELIX   43  43 THR C  130  LEU C  149  1                                  20
HELIX   44  44 SER C  162  TYR C  175  1                                  14
HELIX   45  45 LEU C  190  GLY C  194  5                                   5
HELIX   46  46 ASN C  199  SER C  213  1                                  15
HELIX   47  47 SER C  213  GLN C  233  1                                  21
HELIX   48  48 ALA C  235  GLY C  244  1                                  10
HELIX   49  49 ASP C  251  MET C  272  1                                  22
HELIX   50  50 ASN C  287  LEU C  297  1                                  11
HELIX   51  51 GLN C  301  ASN C  315  1                                  15
HELIX   52  52 GLY C  341  CYS C  352  1                                  12
HELIX   53  53 THR C  374  GLY C  387  1                                  14
HELIX   54  54 ASP C  393  TRP C  400  1                                   8
HELIX   55  55 TRP C  420  GLY C  424  5                                   5
HELIX   56  56 HIS C  444  ARG C  448  5                                   5
HELIX   57  57 PRO C  455  ARG C  477  1                                  23
HELIX   58  58 ASP D   80  SER D   88  1                                   9
HELIX   59  59 SER D   88  GLY D   99  1                                  12
HELIX   60  60 PHE D  116  GLN D  122  5                                   7
HELIX   61  61 THR D  130  GLY D  150  1                                  21
HELIX   62  62 SER D  162  TYR D  175  1                                  14
HELIX   63  63 PRO D  188  ALA D  193  1                                   6
HELIX   64  64 ASN D  199  SER D  213  1                                  15
HELIX   65  65 SER D  213  GLN D  233  1                                  21
HELIX   66  66 ALA D  235  GLY D  244  1                                  10
HELIX   67  67 ASP D  251  MET D  272  1                                  22
HELIX   68  68 ASN D  287  SER D  298  1                                  12
HELIX   69  69 GLN D  301  ASN D  315  1                                  15
HELIX   70  70 ASP D  324  TYR D  329  1                                   6
HELIX   71  71 GLY D  341  CYS D  352  1                                  12
HELIX   72  72 THR D  374  GLY D  387  1                                  14
HELIX   73  73 ASP D  393  TRP D  400  1                                   8
HELIX   74  74 ASP D  418  GLY D  424  5                                   7
HELIX   75  75 HIS D  444  ARG D  448  5                                   5
HELIX   76  76 PRO D  455  ARG D  477  1                                  23
SHEET    1   A 8 GLN A  32  ARG A  39  0
SHEET    2   A 8 THR A  52  SER A  60 -1  O  PHE A  53   N  GLN A  38
SHEET    3   A 8 LEU A 101  ALA A 105 -1  O  PHE A 104   N  LEU A  58
SHEET    4   A 8 ILE A  71  THR A  75  1  N  PHE A  72   O  LEU A 101
SHEET    5   A 8 ALA A 156  GLY A 161  1  O  ILE A 157   N  PHE A  73
SHEET    6   A 8 GLY A 181  ALA A 185  1  O  ALA A 185   N  GLY A 160
SHEET    7   A 8 ILE A 410  GLY A 415  1  O  ILE A 411   N  ALA A 184
SHEET    8   A 8 VAL A 433  ILE A 438  1  O  ILE A 434   N  PHE A 412
SHEET    1   B 2 THR A 278  ASP A 279  0
SHEET    2   B 2 PRO A 283  LEU A 284 -1  O  LEU A 284   N  THR A 278
SHEET    1   C 8 GLN B  32  ARG B  39  0
SHEET    2   C 8 THR B  52  SER B  60 -1  O  PHE B  53   N  GLN B  38
SHEET    3   C 8 LEU B 101  ALA B 105 -1  O  PHE B 104   N  LEU B  58
SHEET    4   C 8 ILE B  71  THR B  75  1  N  PHE B  72   O  LEU B 101
SHEET    5   C 8 ALA B 156  GLY B 161  1  O  ILE B 157   N  PHE B  73
SHEET    6   C 8 GLY B 181  ALA B 185  1  O  LEU B 183   N  ALA B 158
SHEET    7   C 8 ILE B 410  GLY B 415  1  O  ILE B 411   N  ALA B 184
SHEET    8   C 8 VAL B 433  ILE B 438  1  O  ILE B 434   N  PHE B 412
SHEET    1   D 2 THR B 278  ASP B 279  0
SHEET    2   D 2 PRO B 283  LEU B 284 -1  O  LEU B 284   N  THR B 278
SHEET    1   E 8 GLN C  32  ARG C  39  0
SHEET    2   E 8 THR C  52  SER C  60 -1  O  GLN C  55   N  PHE C  36
SHEET    3   E 8 LEU C 101  ALA C 105 -1  O  PHE C 104   N  LEU C  58
SHEET    4   E 8 ILE C  71  THR C  75  1  N  PHE C  72   O  LEU C 101
SHEET    5   E 8 ALA C 156  GLY C 161  1  O  PHE C 159   N  THR C  75
SHEET    6   E 8 GLY C 181  ALA C 185  1  O  LEU C 183   N  ALA C 158
SHEET    7   E 8 ILE C 410  GLY C 415  1  O  ILE C 411   N  ALA C 184
SHEET    8   E 8 VAL C 433  ILE C 438  1  O  ILE C 434   N  PHE C 412
SHEET    1   F 2 THR C 278  ASP C 279  0
SHEET    2   F 2 PRO C 283  LEU C 284 -1  O  LEU C 284   N  THR C 278
SHEET    1   G 8 GLN D  32  ARG D  39  0
SHEET    2   G 8 THR D  52  SER D  60 -1  O  PHE D  53   N  GLN D  38
SHEET    3   G 8 LEU D 101  ALA D 105 -1  O  PHE D 104   N  LEU D  58
SHEET    4   G 8 ILE D  71  THR D  75  1  N  PHE D  72   O  LEU D 101
SHEET    5   G 8 ALA D 156  GLY D 161  1  O  PHE D 159   N  PHE D  73
SHEET    6   G 8 GLY D 181  ALA D 185  1  O  ALA D 185   N  GLY D 160
SHEET    7   G 8 ILE D 410  GLY D 415  1  O  ILE D 411   N  ALA D 184
SHEET    8   G 8 VAL D 433  ILE D 438  1  O  ILE D 434   N  PHE D 412
SHEET    1   H 2 THR D 278  ASP D 279  0
SHEET    2   H 2 PRO D 283  LEU D 284 -1  O  LEU D 284   N  THR D 278
SSBOND   1 CYS A  216    CYS A  293                          1555   1555  2.09
SSBOND   2 CYS A  246    CYS A  322                          1555   1555  2.08
SSBOND   3 CYS A  332    CYS A  338                          1555   1555  2.05
SSBOND   4 CYS A  352    CYS A  382                          1555   1555  2.04
SSBOND   5 CYS B  216    CYS B  293                          1555   1555  2.07
SSBOND   6 CYS B  246    CYS B  322                          1555   1555  2.06
SSBOND   7 CYS B  332    CYS B  338                          1555   1555  2.03
SSBOND   8 CYS B  352    CYS B  382                          1555   1555  2.04
SSBOND   9 CYS C  216    CYS C  293                          1555   1555  2.08
SSBOND  10 CYS C  246    CYS C  322                          1555   1555  2.07
SSBOND  11 CYS C  332    CYS C  338                          1555   1555  2.06
SSBOND  12 CYS C  352    CYS C  382                          1555   1555  2.08
SSBOND  13 CYS D  216    CYS D  293                          1555   1555  2.04
SSBOND  14 CYS D  246    CYS D  322                          1555   1555  2.10
SSBOND  15 CYS D  332    CYS D  338                          1555   1555  2.02
SSBOND  16 CYS D  352    CYS D  382                          1555   1555  2.04
LINK         ND2 ASN A  50                 C1  NAG A 495     1555   1555  1.45
LINK         ND2 ASN A  86                 C1  NAG A   1     1555   1555  1.45
LINK         ND2 ASN A 315                 C1  NAG A 496     1555   1555  1.44
LINK         ND2 ASN A 363                 C1  NAG A 498     1555   1555  1.45
LINK         ND2 ASN B  86                 C1  NAG B   1     1555   1555  1.45
LINK         ND2 ASN B 315                 C1  NAG B 495     1555   1555  1.45
LINK         ND2 ASN B 363                 C1  NAG B 497     1555   1555  1.44
LINK         ND2 ASN C  50                 C1  NAG C 494     1555   1555  1.45
LINK         ND2 ASN C  86                 C1  NAG C 495     1555   1555  1.44
LINK         ND2 ASN C 315                 C1  NAG C 496     1555   1555  1.43
LINK         ND2 ASN C 363                 C1  NAG C 498     1555   1555  1.46
LINK         ND2 ASN D  86                 C1  NAG D   1     1555   1555  1.45
LINK         ND2 ASN D 315                 C1  NAG D 495     1555   1555  1.45
LINK         ND2 ASN D 363                 C1  NAG D 493     1555   1555  1.44
LINK         C1  BMA C   1                 O4  NAG C 493     1555   1555  1.48
LINK         C1  NAG C 493                 O4  NAG C 498     1555   1555  1.46
LINK         C1  BMA A 493                 O4  NAG A 494     1555   1555  1.45
LINK         C1  NAG A 494                 O4  NAG A 498     1555   1555  1.45
LINK         C1  BMA B 493                 O4  NAG B 494     1555   1555  1.46
LINK         C1  NAG B 494                 O4  NAG B 497     1555   1555  1.46
LINK         O4  NAG B 495                 C1  NAG B 496     1555   1555  1.45
LINK         O4  NAG A 496                 C1  NAG A 497     1555   1555  1.47
LINK         O4  NAG C 496                 C1  NAG C 497     1555   1555  1.46
LINK         O4  NAG D 493                 C1  NAG D 494     1555   1555  1.44
LINK         O4  NAG D 495                 C1  NAG D 496     1555   1555  1.45
CISPEP   1 ASP D   28    PRO D   29          0        27.57
SITE     1 AC1  3 TRP A  82  ALA A  83  ASN A  86
SITE     1 AC2  1 NAG A 494
SITE     1 AC3  5 ARG A 225  ASP A 229  BMA A 493  NAG A 498
SITE     2 AC3  5 HOH A 676
SITE     1 AC4  6 LYS A 228  ASN A 363  NAG A 494  HOH A 548
SITE     2 AC4  6 HOH A 584  HOH A 608
SITE     1 AC5  4 ASN A  50  HOH A 877  LEU B 383  TRP B 389
SITE     1 AC6  8 ARG A 307  ASN A 315  GLY A 318  GLU A 320
SITE     2 AC6  8 TYR A 323  NAG A 497  HOH A 581  HOH A1246
SITE     1 AC7  3 NAG A 496  HOH A 581  HOH A1119
SITE     1 AC8  3 TRP B  82  ALA B  83  ASN B  86
SITE     1 AC9  1 NAG B 494
SITE     1 BC1  6 ARG B 225  LYS B 228  ASP B 229  BMA B 493
SITE     2 BC1  6 NAG B 497  HOH B 563
SITE     1 BC2  6 ARG B 225  LYS B 228  ASN B 363  NAG B 494
SITE     2 BC2  6 HOH B 557  HOH B 582
SITE     1 BC3 10 ARG B 307  ASN B 315  GLY B 318  GLU B 320
SITE     2 BC3 10 CYS B 322  TYR B 323  NAG B 496  HOH B 516
SITE     3 BC3 10 HOH B 663  HOH B 922
SITE     1 BC4  2 NAG B 495  HOH B 663
SITE     1 BC5  2 ARG C 225  NAG C 493
SITE     1 BC6  6 BMA C   1  ARG C 225  LYS C 228  ASP C 229
SITE     2 BC6  6 NAG C 498  HOH C 586
SITE     1 BC7  7 PHE C 224  ARG C 225  LYS C 228  ASN C 363
SITE     2 BC7  7 NAG C 493  HOH C 540  HOH C 545
SITE     1 BC8  2 ASN C  50  TRP D 389
SITE     1 BC9  5 ASP C  80  TRP C  82  ALA C  83  ASN C  86
SITE     2 BC9  5 HOH C1252
SITE     1 CC1  9 ARG C 307  ASN C 315  GLY C 318  GLU C 320
SITE     2 CC1  9 HIS C 321  CYS C 322  TYR C 323  NAG C 497
SITE     3 CC1  9 HOH C 892
SITE     1 CC2  3 NAG C 496  HOH C 892  HOH C1201
SITE     1 CC3  3 TRP D  82  ASN D  86  HOH D1266
SITE     1 CC4  8 ARG D 221  PHE D 224  ARG D 225  LYS D 228
SITE     2 CC4  8 ASN D 363  NAG D 494  HOH D 497  HOH D 539
SITE     1 CC5  4 ARG D 225  ASP D 229  NAG D 493  HOH D 985
SITE     1 CC6  8 ARG D 307  ASN D 315  GLY D 318  GLU D 320
SITE     2 CC6  8 HIS D 321  CYS D 322  TYR D 323  NAG D 496
SITE     1 CC7  1 NAG D 495
CRYST1   80.216  130.215  124.436  90.00 102.36  90.00 P 1 21 1      8
ORIGX1      1.000000  0.000000  0.000000        0.00000
ORIGX2      0.000000  1.000000  0.000000        0.00000
ORIGX3      0.000000  0.000000  1.000000        0.00000
SCALE1      0.012466  0.000000  0.002732        0.00000
SCALE2      0.000000  0.007680  0.000000        0.00000
SCALE3      0.000000  0.000000  0.008227        0.00000
TER    3473      GLU A 479
TER    6945      GLU B 479
TER   10413      ARG C 478
TER   13861      ARG D 477
MASTER      592    0   25   76   40    0   39    615144    4  387  148
END