longtext: 5fkj-pdb

content
HEADER    HYDROLASE                               16-OCT-15   5FKJ
TITLE     CRYSTAL STRUCTURE OF MOUSE ACETYLCHOLINESTERASE IN COMPLEX WITH
TITLE    2 C-547, AN ALKYL AMMONIUM DERIVATIVE OF 6-METHYL URACIL
COMPND    MOL_ID: 1;
COMPND   2 MOLECULE: ACETYLCHOLINESTERASE;
COMPND   3 CHAIN: A, B, C, D;
COMPND   4 FRAGMENT: UNP RESIDUES 32-574;
COMPND   5 EC: 3.1.1.7;
COMPND   6 ENGINEERED: YES
SOURCE    MOL_ID: 1;
SOURCE   2 ORGANISM_SCIENTIFIC: MUS MUSCULUS;
SOURCE   3 ORGANISM_COMMON: HOUSE MOUSE;
SOURCE   4 ORGANISM_TAXID: 10090;
SOURCE   5 EXPRESSION_SYSTEM: CRICETULUS GRISEUS;
SOURCE   6 EXPRESSION_SYSTEM_COMMON: CHINESE HAMSTER;
SOURCE   7 EXPRESSION_SYSTEM_TAXID: 10029;
SOURCE   8 EXPRESSION_SYSTEM_CELL_LINE: CHO-K1;
SOURCE   9 EXPRESSION_SYSTEM_VECTOR_TYPE: PLASMID;
SOURCE  10 EXPRESSION_SYSTEM_PLASMID: PGS
KEYWDS    HYDROLASE, ACETYLCHOLINESTERASE, C-547
EXPDTA    X-RAY DIFFRACTION
AUTHOR    F.NACHON,M.VILLARD-WANDHAMMER,K.PETROV,P.MASSON
REVDAT   1   16-MAR-16 5FKJ    0
JRNL        AUTH   A.D.KHARLAMOVA,S.V.LUSHCHEKINA,K.A.PETROV,E.D.KOTS,
JRNL        AUTH 2 F.V.NACHON,M.VILLARD-WANDHAMMER,I.V.ZUEVA,E.KREJCI,
JRNL        AUTH 3 V.S.REZNIK,V.V.ZOBOV,E.E.NIKOLSKY,P.MASSON
JRNL        TITL   SLOW-BINDING INHIBITION OF ACETYLCHOLINESTERASE BY A 6-
JRNL        TITL 2 METHYLURACIL ALKYL-AMMONIUM DERIVATIVE: MECHANISM AND
JRNL        TITL 3 ADVANTAGES FOR MYASTHENIA GRAVIS TREATMENT.
JRNL        REF    BIOCHEM.J.                                 2016
JRNL        REFN                   ESSN 1470-8728
JRNL        PMID   26929400
JRNL        DOI    10.1042/BCJ20160084
REMARK   2
REMARK   2 RESOLUTION.    3.13 ANGSTROMS.
REMARK   3
REMARK   3 REFINEMENT.
REMARK   3   PROGRAM     : PHENIX (PHENIX.REFINE)
REMARK   3   AUTHORS     : PAUL ADAMS,PAVEL AFONINE,VICENT CHEN,IAN
REMARK   3               : DAVIS,KRESHNA GOPAL,RALF GROSSE-KUNSTLEVE,
REMARK   3               : LI-WEI HUNG,ROBERT IMMORMINO,TOM IOERGER,
REMARK   3               : AIRLIE MCCOY,ERIK MCKEE,NIGEL MORIARTY,
REMARK   3               : REETAL PAI,RANDY READ,JANE RICHARDSON,
REMARK   3               : DAVID RICHARDSON,TOD ROMO,JIM SACCHETTINI,
REMARK   3               : NICHOLAS SAUTER,JACOB SMITH,LAURENT
REMARK   3               : STORONI,TOM TERWILLIGER,PETER ZWART
REMARK   3
REMARK   3    REFINEMENT TARGET : ML
REMARK   3
REMARK   3  DATA USED IN REFINEMENT.
REMARK   3   RESOLUTION RANGE HIGH (ANGSTROMS) : 3.133
REMARK   3   RESOLUTION RANGE LOW  (ANGSTROMS) : 94.524
REMARK   3   MIN(FOBS/SIGMA_FOBS)              : 1.36
REMARK   3   COMPLETENESS FOR RANGE        (%) : 99.35
REMARK   3   NUMBER OF REFLECTIONS             : 94994
REMARK   3
REMARK   3  FIT TO DATA USED IN REFINEMENT.
REMARK   3   R VALUE     (WORKING + TEST SET) : 0.2078
REMARK   3   R VALUE            (WORKING SET) : 0.2073
REMARK   3   FREE R VALUE                     : 0.2494
REMARK   3   FREE R VALUE TEST SET SIZE   (%) : 1.1
REMARK   3   FREE R VALUE TEST SET COUNT      : 1046
REMARK   3
REMARK   3  FIT TO DATA USED IN REFINEMENT (IN BINS).
REMARK   3   BIN  RESOLUTION RANGE  COMPL.    NWORK NFREE   RWORK  RFREE  CCWORK
REMARK   3     1 94.5674 -  5.9930    1.00    13916   156  0.1849 0.2281   0.917
REMARK   3     2  5.9930 -  4.7568    1.00    13543   150  0.1779 0.2039   0.915
REMARK   3     3  4.7568 -  4.1555    1.00    13409   149  0.1695 0.2159   0.925
REMARK   3     4  4.1555 -  3.7756    1.00    13394   149  0.1960 0.2354   0.906
REMARK   3     5  3.7756 -  3.5049    1.00    13325   149  0.2417 0.2983   0.869
REMARK   3     6  3.5049 -  3.2983    1.00    13343   148  0.2742 0.3317   0.823
REMARK   3     7  3.2983 -  3.1331    0.98    13018   145  0.3357 0.3507   0.732
REMARK   3
REMARK   3  BULK SOLVENT MODELLING.
REMARK   3   METHOD USED        : FLAT BULK SOLVENT MODEL
REMARK   3   SOLVENT RADIUS     : 1.11
REMARK   3   SHRINKAGE RADIUS   : 0.90
REMARK   3   K_SOL              : NULL
REMARK   3   B_SOL              : NULL
REMARK   3
REMARK   3  ERROR ESTIMATES.
REMARK   3   COORDINATE ERROR (MAXIMUM-LIKELIHOOD BASED)     : 0.40
REMARK   3   PHASE ERROR (DEGREES, MAXIMUM-LIKELIHOOD BASED) : 25.98
REMARK   3
REMARK   3  B VALUES.
REMARK   3   FROM WILSON PLOT           (A**2) : 65.96
REMARK   3   MEAN B VALUE      (OVERALL, A**2) : 71.5
REMARK   3   OVERALL ANISOTROPIC B VALUE.
REMARK   3    B11 (A**2) : NULL
REMARK   3    B22 (A**2) : NULL
REMARK   3    B33 (A**2) : NULL
REMARK   3    B12 (A**2) : NULL
REMARK   3    B13 (A**2) : NULL
REMARK   3    B23 (A**2) : NULL
REMARK   3
REMARK   3  TWINNING INFORMATION.
REMARK   3   FRACTION: NULL
REMARK   3   OPERATOR: NULL
REMARK   3
REMARK   3  DEVIATIONS FROM IDEAL VALUES.
REMARK   3                 RMSD          COUNT
REMARK   3   BOND      :  0.004          17565
REMARK   3   ANGLE     :  0.847          24034
REMARK   3   CHIRALITY :  0.056           2561
REMARK   3   PLANARITY :  0.006           3155
REMARK   3   DIHEDRAL  : 16.277          10287
REMARK   3
REMARK   3  TLS DETAILS
REMARK   3   NUMBER OF TLS GROUPS  : 4
REMARK   3   TLS GROUP : 1
REMARK   3    SELECTION: CHAIN A
REMARK   3    ORIGIN FOR THE GROUP (A):   5.5597 -29.1297  85.8149
REMARK   3    T TENSOR
REMARK   3      T11:   0.4995 T22:   0.5212
REMARK   3      T33:   0.5105 T12:  -0.0172
REMARK   3      T13:   0.0470 T23:  -0.0036
REMARK   3    L TENSOR
REMARK   3      L11:   1.0281 L22:   2.7656
REMARK   3      L33:   1.5527 L12:   0.3122
REMARK   3      L13:  -0.0857 L23:  -0.3253
REMARK   3    S TENSOR
REMARK   3      S11:   0.0378 S12:   0.0119 S13:   0.0679
REMARK   3      S21:   0.1413 S22:   0.0234 S23:   0.0915
REMARK   3      S31:  -0.1773 S32:  -0.0083 S33:  -0.0000
REMARK   3   TLS GROUP : 2
REMARK   3    SELECTION: CHAIN B
REMARK   3    ORIGIN FOR THE GROUP (A):  -9.5087  26.9033  66.5270
REMARK   3    T TENSOR
REMARK   3      T11:   1.0833 T22:   0.7677
REMARK   3      T33:   0.7219 T12:   0.4272
REMARK   3      T13:   0.2488 T23:   0.0557
REMARK   3    L TENSOR
REMARK   3      L11:   1.8991 L22:   3.5387
REMARK   3      L33:   3.0336 L12:  -0.7167
REMARK   3      L13:   0.4705 L23:  -1.6586
REMARK   3    S TENSOR
REMARK   3      S11:  -0.1228 S12:  -0.3184 S13:   0.0898
REMARK   3      S21:   1.1332 S22:   0.4511 S23:   0.5077
REMARK   3      S31:  -1.0931 S32:  -0.8028 S33:   0.0741
REMARK   3   TLS GROUP : 3
REMARK   3    SELECTION: CHAIN C
REMARK   3    ORIGIN FOR THE GROUP (A):  24.0097  12.4321  25.5550
REMARK   3    T TENSOR
REMARK   3      T11:   0.5305 T22:   0.4849
REMARK   3      T33:   0.5189 T12:   0.0280
REMARK   3      T13:   0.0634 T23:   0.0412
REMARK   3    L TENSOR
REMARK   3      L11:   1.0169 L22:   1.2441
REMARK   3      L33:   2.1137 L12:   0.0507
REMARK   3      L13:   0.1720 L23:  -0.0790
REMARK   3    S TENSOR
REMARK   3      S11:  -0.0913 S12:   0.0105 S13:  -0.0543
REMARK   3      S21:   0.0512 S22:  -0.0002 S23:  -0.0728
REMARK   3      S31:   0.0818 S32:   0.2665 S33:   0.0000
REMARK   3   TLS GROUP : 4
REMARK   3    SELECTION: CHAIN D
REMARK   3    ORIGIN FOR THE GROUP (A):  47.8884   4.9577  81.3984
REMARK   3    T TENSOR
REMARK   3      T11:   0.4527 T22:   0.6304
REMARK   3      T33:   0.6193 T12:  -0.0030
REMARK   3      T13:  -0.0644 T23:   0.0754
REMARK   3    L TENSOR
REMARK   3      L11:   1.1354 L22:   1.6123
REMARK   3      L33:   3.4087 L12:  -0.1951
REMARK   3      L13:   0.5140 L23:  -0.2662
REMARK   3    S TENSOR
REMARK   3      S11:  -0.0032 S12:   0.1550 S13:   0.1760
REMARK   3      S21:   0.0051 S22:  -0.1115 S23:  -0.2881
REMARK   3      S31:  -0.1581 S32:   0.3452 S33:  -0.0010
REMARK   3
REMARK   3  NCS DETAILS
REMARK   3   NUMBER OF NCS GROUPS : NULL
REMARK   3
REMARK   3  OTHER REFINEMENT REMARKS: NULL
REMARK   4
REMARK   4 5FKJ COMPLIES WITH FORMAT V. 3.30, 13-JUL-11
REMARK 100
REMARK 100 THIS ENTRY HAS BEEN PROCESSED BY PDBE ON 19-OCT-15.
REMARK 100 THE PDBE ID CODE IS EBI-65320.
REMARK 200
REMARK 200 EXPERIMENTAL DETAILS
REMARK 200  EXPERIMENT TYPE                : X-RAY DIFFRACTION
REMARK 200  DATE OF DATA COLLECTION        : NULL
REMARK 200  TEMPERATURE           (KELVIN) : 100
REMARK 200  PH                             : 7.4
REMARK 200  NUMBER OF CRYSTALS USED        : 1
REMARK 200
REMARK 200  SYNCHROTRON              (Y/N) : Y
REMARK 200  RADIATION SOURCE               : ESRF
REMARK 200  BEAMLINE                       : ID14-1
REMARK 200  X-RAY GENERATOR MODEL          : NULL
REMARK 200  MONOCHROMATIC OR LAUE    (M/L) : M
REMARK 200  WAVELENGTH OR RANGE        (A) : 0.9334
REMARK 200  MONOCHROMATOR                  : NULL
REMARK 200  OPTICS                         : NULL
REMARK 200
REMARK 200  DETECTOR TYPE                  : CCD (QUANTUM Q210)
REMARK 200  DETECTOR MANUFACTURER          : ADSC
REMARK 200  INTENSITY-INTEGRATION SOFTWARE : XDS
REMARK 200  DATA SCALING SOFTWARE          : XSCALE
REMARK 200
REMARK 200  NUMBER OF UNIQUE REFLECTIONS   : 95147
REMARK 200  RESOLUTION RANGE HIGH      (A) : 3.13
REMARK 200  RESOLUTION RANGE LOW       (A) : 87.72
REMARK 200  REJECTION CRITERIA  (SIGMA(I)) : 1.5
REMARK 200
REMARK 200 OVERALL.
REMARK 200  COMPLETENESS FOR RANGE     (%) : 99.0
REMARK 200  DATA REDUNDANCY                : 3.7
REMARK 200  R MERGE                    (I) : 0.14
REMARK 200  R SYM                      (I) : NULL
REMARK 200   FOR THE DATA SET  : 10.69
REMARK 200
REMARK 200 IN THE HIGHEST RESOLUTION SHELL.
REMARK 200  HIGHEST RESOLUTION SHELL, RANGE HIGH (A) : 3.13
REMARK 200  HIGHEST RESOLUTION SHELL, RANGE LOW  (A) : 3.24
REMARK 200  COMPLETENESS FOR SHELL     (%) : 97.0
REMARK 200  DATA REDUNDANCY IN SHELL       : 3.7
REMARK 200  R MERGE FOR SHELL          (I) : 0.84
REMARK 200  R SYM FOR SHELL            (I) : NULL
REMARK 200   FOR SHELL         : 1.57
REMARK 200
REMARK 200 DIFFRACTION PROTOCOL: SINGLE WAVELENGTH
REMARK 200 METHOD USED TO DETERMINE THE STRUCTURE: MOLECULAR REPLACEMENT
REMARK 200 SOFTWARE USED: MOLREP
REMARK 200 STARTING MODEL: PDB ENTRY 4A16
REMARK 200
REMARK 200 REMARK: NONE
REMARK 280
REMARK 280 CRYSTAL
REMARK 280 SOLVENT CONTENT, VS   (%): 75
REMARK 280 MATTHEWS COEFFICIENT, VM (ANGSTROMS**3/DA): 4.9
REMARK 280
REMARK 280 CRYSTALLIZATION CONDITIONS: 0.1 M BICINE BUFFER PH 9, 1.6 M
REMARK 280  AMMONIUM SULFATE
REMARK 290
REMARK 290 CRYSTALLOGRAPHIC SYMMETRY
REMARK 290 SYMMETRY OPERATORS FOR SPACE GROUP: P 21 21 21
REMARK 290
REMARK 290      SYMOP   SYMMETRY
REMARK 290     NNNMMM   OPERATOR
REMARK 290       1555   X,Y,Z
REMARK 290       2555   -X+1/2,-Y,Z+1/2
REMARK 290       3555   -X,Y+1/2,-Z+1/2
REMARK 290       4555   X+1/2,-Y+1/2,-Z
REMARK 290
REMARK 290     WHERE NNN -> OPERATOR NUMBER
REMARK 290           MMM -> TRANSLATION VECTOR
REMARK 290
REMARK 290 CRYSTALLOGRAPHIC SYMMETRY TRANSFORMATIONS
REMARK 290 THE FOLLOWING TRANSFORMATIONS OPERATE ON THE ATOM/HETATM
REMARK 290 RECORDS IN THIS ENTRY TO PRODUCE CRYSTALLOGRAPHICALLY
REMARK 290 RELATED MOLECULES.
REMARK 290   SMTRY1   1  1.000000  0.000000  0.000000        0.00000
REMARK 290   SMTRY2   1  0.000000  1.000000  0.000000        0.00000
REMARK 290   SMTRY3   1  0.000000  0.000000  1.000000        0.00000
REMARK 290   SMTRY1   2 -1.000000  0.000000  0.000000       68.57500
REMARK 290   SMTRY2   2  0.000000 -1.000000  0.000000        0.00000
REMARK 290   SMTRY3   2  0.000000  0.000000  1.000000      112.20000
REMARK 290   SMTRY1   3 -1.000000  0.000000  0.000000        0.00000
REMARK 290   SMTRY2   3  0.000000  1.000000  0.000000       87.72500
REMARK 290   SMTRY3   3  0.000000  0.000000 -1.000000      112.20000
REMARK 290   SMTRY1   4  1.000000  0.000000  0.000000       68.57500
REMARK 290   SMTRY2   4  0.000000 -1.000000  0.000000       87.72500
REMARK 290   SMTRY3   4  0.000000  0.000000 -1.000000        0.00000
REMARK 290
REMARK 290 REMARK: NULL
REMARK 300
REMARK 300 BIOMOLECULE: 1, 2
REMARK 300 SEE REMARK 350 FOR THE AUTHOR PROVIDED AND/OR PROGRAM
REMARK 300 GENERATED ASSEMBLY INFORMATION FOR THE STRUCTURE IN
REMARK 300 THIS ENTRY. THE REMARK MAY ALSO PROVIDE INFORMATION ON
REMARK 300 BURIED SURFACE AREA.
REMARK 350
REMARK 350 COORDINATES FOR A COMPLETE MULTIMER REPRESENTING THE KNOWN
REMARK 350 BIOLOGICALLY SIGNIFICANT OLIGOMERIZATION STATE OF THE
REMARK 350 MOLECULE CAN BE GENERATED BY APPLYING BIOMT TRANSFORMATIONS
REMARK 350 GIVEN BELOW.  BOTH NON-CRYSTALLOGRAPHIC AND
REMARK 350 CRYSTALLOGRAPHIC OPERATIONS ARE GIVEN.
REMARK 350
REMARK 350 BIOMOLECULE: 1
REMARK 350 AUTHOR DETERMINED BIOLOGICAL UNIT: DIMERIC
REMARK 350 SOFTWARE DETERMINED QUATERNARY STRUCTURE: DIMERIC
REMARK 350 SOFTWARE USED: PISA
REMARK 350 TOTAL BURIED SURFACE AREA: 6910 ANGSTROM**2
REMARK 350 SURFACE AREA OF THE COMPLEX: 38330 ANGSTROM**2
REMARK 350 CHANGE IN SOLVENT FREE ENERGY: -151.7 KCAL/MOL
REMARK 350 APPLY THE FOLLOWING TO CHAINS: C, D
REMARK 350   BIOMT1   1  1.000000  0.000000  0.000000        0.00000
REMARK 350   BIOMT2   1  0.000000  1.000000  0.000000        0.00000
REMARK 350   BIOMT3   1  0.000000  0.000000  1.000000        0.00000
REMARK 350
REMARK 350 BIOMOLECULE: 2
REMARK 350 AUTHOR DETERMINED BIOLOGICAL UNIT: DIMERIC
REMARK 350 SOFTWARE DETERMINED QUATERNARY STRUCTURE: DIMERIC
REMARK 350 SOFTWARE USED: PISA
REMARK 350 TOTAL BURIED SURFACE AREA: 6670 ANGSTROM**2
REMARK 350 SURFACE AREA OF THE COMPLEX: 39060 ANGSTROM**2
REMARK 350 CHANGE IN SOLVENT FREE ENERGY: -135.2 KCAL/MOL
REMARK 350 APPLY THE FOLLOWING TO CHAINS: A, B
REMARK 350   BIOMT1   1  1.000000  0.000000  0.000000        0.00000
REMARK 350   BIOMT2   1  0.000000  1.000000  0.000000        0.00000
REMARK 350   BIOMT3   1  0.000000  0.000000  1.000000        0.00000
REMARK 465
REMARK 465 MISSING RESIDUES
REMARK 465 THE FOLLOWING RESIDUES WERE NOT LOCATED IN THE
REMARK 465 EXPERIMENT. (M=MODEL NUMBER; RES=RESIDUE NAME; C=CHAIN
REMARK 465 IDENTIFIER; SSSEQ=SEQUENCE NUMBER; I=INSERTION CODE.)
REMARK 465
REMARK 465   M RES C SSSEQI
REMARK 465     GLU A     1
REMARK 465     GLY A     2
REMARK 465     GLU B     1
REMARK 465     GLY B     2
REMARK 465     ARG B     3
REMARK 465     ALA B   542
REMARK 465     THR B   543
REMARK 465     GLU C     1
REMARK 465     GLY C     2
REMARK 465     ARG C     3
REMARK 465     LEU C   540
REMARK 465     SER C   541
REMARK 465     ALA C   542
REMARK 465     THR C   543
REMARK 465     GLU D     1
REMARK 465     GLY D     2
REMARK 465     ARG D     3
REMARK 465     LEU D   540
REMARK 465     SER D   541
REMARK 465     ALA D   542
REMARK 465     THR D   543
REMARK 500
REMARK 500 GEOMETRY AND STEREOCHEMISTRY
REMARK 500 SUBTOPIC: CLOSE CONTACTS IN SAME ASYMMETRIC UNIT
REMARK 500
REMARK 500 THE FOLLOWING ATOMS ARE IN CLOSE CONTACT.
REMARK 500
REMARK 500  ATM1  RES C  SSEQI   ATM2  RES C  SSEQI           DISTANCE
REMARK 500   O    VAL A   300     O    HOH A  2047              2.18
REMARK 500   O    HOH A  2047     O    HOH A  2048              2.13
REMARK 500   O    HOH A  2048     O    HOH A  2078              2.15
REMARK 500
REMARK 500 REMARK: NULL
REMARK 500
REMARK 500 GEOMETRY AND STEREOCHEMISTRY
REMARK 500 SUBTOPIC: COVALENT BOND ANGLES
REMARK 500
REMARK 500 THE STEREOCHEMICAL PARAMETERS OF THE FOLLOWING RESIDUES
REMARK 500 HAVE VALUES WHICH DEVIATE FROM EXPECTED VALUES BY MORE
REMARK 500 THAN 6*RMSD (M=MODEL NUMBER; RES=RESIDUE NAME; C=CHAIN
REMARK 500 IDENTIFIER; SSEQ=SEQUENCE NUMBER; I=INSERTION CODE).
REMARK 500
REMARK 500 STANDARD TABLE:
REMARK 500 FORMAT: (10X,I3,1X,A3,1X,A1,I4,A1,3(1X,A4,2X),12X,F5.1)
REMARK 500
REMARK 500 EXPECTED VALUES PROTEIN: ENGH AND HUBER, 1999
REMARK 500 EXPECTED VALUES NUCLEIC ACID: CLOWNEY ET AL 1996
REMARK 500
REMARK 500  M RES CSSEQI ATM1   ATM2   ATM3
REMARK 500    CYS A 257   CA  -  CB  -  SG  ANGL. DEV. =   9.4 DEGREES
REMARK 500    CYS C 257   CA  -  CB  -  SG  ANGL. DEV. =  10.9 DEGREES
REMARK 500
REMARK 500 REMARK: NULL
REMARK 500
REMARK 500 GEOMETRY AND STEREOCHEMISTRY
REMARK 500 SUBTOPIC: TORSION ANGLES
REMARK 500
REMARK 500 TORSION ANGLES OUTSIDE THE EXPECTED RAMACHANDRAN REGIONS:
REMARK 500 (M=MODEL NUMBER; RES=RESIDUE NAME; C=CHAIN IDENTIFIER;
REMARK 500 SSEQ=SEQUENCE NUMBER; I=INSERTION CODE).
REMARK 500
REMARK 500 STANDARD TABLE:
REMARK 500 FORMAT:(10X,I3,1X,A3,1X,A1,I4,A1,4X,F7.2,3X,F7.2)
REMARK 500
REMARK 500 EXPECTED VALUES: GJ KLEYWEGT AND TA JONES (1996). PHI/PSI-
REMARK 500 CHOLOGY: RAMACHANDRAN REVISITED. STRUCTURE 4, 1395 - 1400
REMARK 500
REMARK 500  M RES CSSEQI        PSI       PHI
REMARK 500    PHE A  47       -9.24     70.79
REMARK 500    PHE A 123       12.20     58.54
REMARK 500    SER A 203     -129.12     55.55
REMARK 500    HIS A 223      -56.42   -128.89
REMARK 500    ALA A 262      -24.74     56.41
REMARK 500    ASP A 306      -75.50   -123.16
REMARK 500    VAL A 407      -61.11   -126.72
REMARK 500    LYS A 496       -9.13     86.11
REMARK 500    ARG A 525       63.85     33.30
REMARK 500    LEU A 540     -143.99     50.43
REMARK 500    PHE B  47       -3.82     75.95
REMARK 500    PRO B 108       49.87    -75.44
REMARK 500    ALA B 109     -116.92     51.56
REMARK 500    PHE B 123       15.06     58.10
REMARK 500    SER B 203     -133.88     58.27
REMARK 500    HIS B 223      -59.44   -120.98
REMARK 500    PRO B 259       46.58    -89.11
REMARK 500    ASP B 306      -71.08   -129.63
REMARK 500    SER B 336      -70.68    -55.51
REMARK 500    VAL B 367       72.68   -119.17
REMARK 500    VAL B 407      -65.28   -130.45
REMARK 500    ASP B 494     -144.67     54.42
REMARK 500    SER B 497      176.41     73.16
REMARK 500    GLN B 499     -157.43     58.26
REMARK 500    TRP B 500       83.58   -157.52
REMARK 500    LEU B 515     -105.76     49.88
REMARK 500    PHE B 535      -62.63    -91.05
REMARK 500    PHE C  47       -9.17     71.21
REMARK 500    PHE C 123       13.79     58.09
REMARK 500    SER C 203     -128.12     51.61
REMARK 500    ALA C 262      -65.89   -143.56
REMARK 500    ASP C 306      -72.47   -126.46
REMARK 500    VAL C 367       71.67   -118.24
REMARK 500    VAL C 407      -64.12   -129.49
REMARK 500    ASP C 494      160.45    175.76
REMARK 500    ARG C 534      -61.39    -97.38
REMARK 500    PHE D  47       -5.60     73.78
REMARK 500    PHE D 123       13.13     58.69
REMARK 500    SER D 203     -130.12     57.05
REMARK 500    HIS D 223      -57.84   -120.65
REMARK 500    ALA D 262     -118.34     57.34
REMARK 500    ASP D 306      -77.31   -121.76
REMARK 500    VAL D 407      -64.73   -130.65
REMARK 500    ARG D 493     -115.31     56.54
REMARK 500    ASP D 494     -111.16     60.30
REMARK 500    SER D 495     -157.18     60.40
REMARK 500    LYS D 496       -9.83     56.60
REMARK 500    ARG D 525       63.40     32.15
REMARK 500
REMARK 500 REMARK: NULL
REMARK 500
REMARK 500 GEOMETRY AND STEREOCHEMISTRY
REMARK 500 SUBTOPIC: NON-CIS, NON-TRANS
REMARK 500
REMARK 500 THE FOLLOWING PEPTIDE BONDS DEVIATE SIGNIFICANTLY FROM BOTH
REMARK 500 CIS AND TRANS CONFORMATION.  CIS BONDS, IF ANY, ARE LISTED
REMARK 500 ON CISPEP RECORDS.  TRANS IS DEFINED AS 180 +/- 30 AND
REMARK 500 CIS IS DEFINED AS 0 +/- 30 DEGREES.
REMARK 500                                 MODEL     OMEGA
REMARK 500 GLY A  260     GLY A  261                  134.01
REMARK 500 LYS A  496     SER A  497                  149.13
REMARK 500 LEU A  540     SER A  541                  141.52
REMARK 500 GLY B  260     GLY B  261                 -149.49
REMARK 500 SER B  497     PRO B  498                 -141.28
REMARK 500 ALA C  262     GLY C  263                 -124.16
REMARK 500
REMARK 500 REMARK: NULL
REMARK 525
REMARK 525 SOLVENT
REMARK 525
REMARK 525 THE SOLVENT MOLECULES HAVE CHAIN IDENTIFIERS THAT
REMARK 525 INDICATE THE POLYMER CHAIN WITH WHICH THEY ARE MOST
REMARK 525 CLOSELY ASSOCIATED. THE REMARK LISTS ALL THE SOLVENT
REMARK 525 MOLECULES WHICH ARE MORE THAN 5A AWAY FROM THE
REMARK 525 NEAREST POLYMER CHAIN (M = MODEL NUMBER;
REMARK 525 RES=RESIDUE NAME; C=CHAIN IDENTIFIER; SSEQ=SEQUENCE
REMARK 525 NUMBER; I=INSERTION CODE):
REMARK 525
REMARK 525  M RES CSSEQI
REMARK 525    HOH D2029        DISTANCE =  5.07 ANGSTROMS
REMARK 525    HOH D2099        DISTANCE =  9.07 ANGSTROMS
REMARK 525    HOH D2100        DISTANCE =  5.64 ANGSTROMS
REMARK 525    HOH D2101        DISTANCE =  8.21 ANGSTROMS
REMARK 525    HOH D2102        DISTANCE =  5.68 ANGSTROMS
REMARK 610
REMARK 610 MISSING HETEROATOM
REMARK 610 THE FOLLOWING RESIDUES HAVE MISSING ATOMS (M=MODEL NUMBER;
REMARK 610 RES=RESIDUE NAME; C=CHAIN IDENTIFIER; SSEQ=SEQUENCE NUMBER;
REMARK 610 I=INSERTION CODE):
REMARK 610   M RES C SSEQI
REMARK 610     G0W B  550
REMARK 610     G0W D  550
REMARK 800
REMARK 800 SITE
REMARK 800 SITE_IDENTIFIER: AC1
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE G0W A 550
REMARK 800
REMARK 800 SITE_IDENTIFIER: AC2
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE G0W B 550
REMARK 800
REMARK 800 SITE_IDENTIFIER: AC3
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE G0W C 550
REMARK 800
REMARK 800 SITE_IDENTIFIER: AC4
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE G0W D 550
REMARK 800
REMARK 800 SITE_IDENTIFIER: AC5
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE SO4 D1540
REMARK 800
REMARK 800 SITE_IDENTIFIER: AC6
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE SO4 B1542
REMARK 800
REMARK 800 SITE_IDENTIFIER: AC7
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE SO4 C1541
REMARK 800
REMARK 800 SITE_IDENTIFIER: AC8
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE  CL A 601
REMARK 800
REMARK 800 SITE_IDENTIFIER: AC9
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE  CL A 605
REMARK 800
REMARK 800 SITE_IDENTIFIER: BC1
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE  CL A 606
REMARK 800
REMARK 800 SITE_IDENTIFIER: BC2
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE  CL A 607
REMARK 800
REMARK 800 SITE_IDENTIFIER: BC3
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE  CL A 608
REMARK 800
REMARK 800 SITE_IDENTIFIER: BC4
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE  CL A 610
REMARK 800
REMARK 800 SITE_IDENTIFIER: BC5
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE  CL B 605
REMARK 800
REMARK 800 SITE_IDENTIFIER: BC6
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE  CL B 606
REMARK 800
REMARK 800 SITE_IDENTIFIER: BC7
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE  CL B 607
REMARK 800
REMARK 800 SITE_IDENTIFIER: BC8
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE  CL B 608
REMARK 800
REMARK 800 SITE_IDENTIFIER: BC9
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE  CL C 603
REMARK 800
REMARK 800 SITE_IDENTIFIER: CC1
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE  CL C 605
REMARK 800
REMARK 800 SITE_IDENTIFIER: CC2
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE  CL C 606
REMARK 800
REMARK 800 SITE_IDENTIFIER: CC3
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE  CL C 607
REMARK 800
REMARK 800 SITE_IDENTIFIER: CC4
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE  CL C 608
REMARK 800
REMARK 800 SITE_IDENTIFIER: CC5
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE  CL C 612
REMARK 800
REMARK 800 SITE_IDENTIFIER: CC6
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE  CL D 606
REMARK 800
REMARK 800 SITE_IDENTIFIER: CC7
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE  CL D 607
REMARK 800
REMARK 800 SITE_IDENTIFIER: CC8
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE  CL D 609
REMARK 800
REMARK 800 SITE_IDENTIFIER: CC9
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR RESIDUE  CL D 610
REMARK 800
REMARK 800 SITE_IDENTIFIER: DC1
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR MONO-SACCHARIDE
REMARK 800  NAG A 560  BOUND TO ASN A 265
REMARK 800
REMARK 800 SITE_IDENTIFIER: DC2
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR MONO-SACCHARIDE
REMARK 800  NAG B 560  BOUND TO ASN B 265
REMARK 800
REMARK 800 SITE_IDENTIFIER: DC3
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR MONO-SACCHARIDE
REMARK 800  NAG B 561  BOUND TO ASN B 350
REMARK 800
REMARK 800 SITE_IDENTIFIER: DC4
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR MONO-SACCHARIDE
REMARK 800  NAG C 560  BOUND TO ASN C 265
REMARK 800
REMARK 800 SITE_IDENTIFIER: DC5
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR MONO-SACCHARIDE
REMARK 800  NAG D 560  BOUND TO ASN D 265
REMARK 800
REMARK 800 SITE_IDENTIFIER: DC6
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: BINDING SITE FOR MONO-SACCHARIDE
REMARK 800  NAG D 561  BOUND TO ASN D 350
REMARK 999
REMARK 999 SEQUENCE
REMARK 999 CONTAINS MUTATION D544STOP TO PRODUCE TRUNCATION
DBREF  5FKJ A    1   543  UNP    P21836   ACES_MOUSE      32    574
DBREF  5FKJ B    1   543  UNP    P21836   ACES_MOUSE      32    574
DBREF  5FKJ C    1   543  UNP    P21836   ACES_MOUSE      32    574
DBREF  5FKJ D    1   543  UNP    P21836   ACES_MOUSE      32    574
SEQRES   1 A  543  GLU GLY ARG GLU ASP PRO GLN LEU LEU VAL ARG VAL ARG
SEQRES   2 A  543  GLY GLY GLN LEU ARG GLY ILE ARG LEU LYS ALA PRO GLY
SEQRES   3 A  543  GLY PRO VAL SER ALA PHE LEU GLY ILE PRO PHE ALA GLU
SEQRES   4 A  543  PRO PRO VAL GLY SER ARG ARG PHE MET PRO PRO GLU PRO
SEQRES   5 A  543  LYS ARG PRO TRP SER GLY VAL LEU ASP ALA THR THR PHE
SEQRES   6 A  543  GLN ASN VAL CYS TYR GLN TYR VAL ASP THR LEU TYR PRO
SEQRES   7 A  543  GLY PHE GLU GLY THR GLU MET TRP ASN PRO ASN ARG GLU
SEQRES   8 A  543  LEU SER GLU ASP CYS LEU TYR LEU ASN VAL TRP THR PRO
SEQRES   9 A  543  TYR PRO ARG PRO ALA SER PRO THR PRO VAL LEU ILE TRP
SEQRES  10 A  543  ILE TYR GLY GLY GLY PHE TYR SER GLY ALA ALA SER LEU
SEQRES  11 A  543  ASP VAL TYR ASP GLY ARG PHE LEU ALA GLN VAL GLU GLY
SEQRES  12 A  543  ALA VAL LEU VAL SER MET ASN TYR ARG VAL GLY THR PHE
SEQRES  13 A  543  GLY PHE LEU ALA LEU PRO GLY SER ARG GLU ALA PRO GLY
SEQRES  14 A  543  ASN VAL GLY LEU LEU ASP GLN ARG LEU ALA LEU GLN TRP
SEQRES  15 A  543  VAL GLN GLU ASN ILE ALA ALA PHE GLY GLY ASP PRO MET
SEQRES  16 A  543  SER VAL THR LEU PHE GLY GLU SER ALA GLY ALA ALA SER
SEQRES  17 A  543  VAL GLY MET HIS ILE LEU SER LEU PRO SER ARG SER LEU
SEQRES  18 A  543  PHE HIS ARG ALA VAL LEU GLN SER GLY THR PRO ASN GLY
SEQRES  19 A  543  PRO TRP ALA THR VAL SER ALA GLY GLU ALA ARG ARG ARG
SEQRES  20 A  543  ALA THR LEU LEU ALA ARG LEU VAL GLY CYS PRO PRO GLY
SEQRES  21 A  543  GLY ALA GLY GLY ASN ASP THR GLU LEU ILE ALA CYS LEU
SEQRES  22 A  543  ARG THR ARG PRO ALA GLN ASP LEU VAL ASP HIS GLU TRP
SEQRES  23 A  543  HIS VAL LEU PRO GLN GLU SER ILE PHE ARG PHE SER PHE
SEQRES  24 A  543  VAL PRO VAL VAL ASP GLY ASP PHE LEU SER ASP THR PRO
SEQRES  25 A  543  GLU ALA LEU ILE ASN THR GLY ASP PHE GLN ASP LEU GLN
SEQRES  26 A  543  VAL LEU VAL GLY VAL VAL LYS ASP GLU GLY SER TYR PHE
SEQRES  27 A  543  LEU VAL TYR GLY VAL PRO GLY PHE SER LYS ASP ASN GLU
SEQRES  28 A  543  SER LEU ILE SER ARG ALA GLN PHE LEU ALA GLY VAL ARG
SEQRES  29 A  543  ILE GLY VAL PRO GLN ALA SER ASP LEU ALA ALA GLU ALA
SEQRES  30 A  543  VAL VAL LEU HIS TYR THR ASP TRP LEU HIS PRO GLU ASP
SEQRES  31 A  543  PRO THR HIS LEU ARG ASP ALA MET SER ALA VAL VAL GLY
SEQRES  32 A  543  ASP HIS ASN VAL VAL CYS PRO VAL ALA GLN LEU ALA GLY
SEQRES  33 A  543  ARG LEU ALA ALA GLN GLY ALA ARG VAL TYR ALA TYR ILE
SEQRES  34 A  543  PHE GLU HIS ARG ALA SER THR LEU THR TRP PRO LEU TRP
SEQRES  35 A  543  MET GLY VAL PRO HIS GLY TYR GLU ILE GLU PHE ILE PHE
SEQRES  36 A  543  GLY LEU PRO LEU ASP PRO SER LEU ASN TYR THR THR GLU
SEQRES  37 A  543  GLU ARG ILE PHE ALA GLN ARG LEU MET LYS TYR TRP THR
SEQRES  38 A  543  ASN PHE ALA ARG THR GLY ASP PRO ASN ASP PRO ARG ASP
SEQRES  39 A  543  SER LYS SER PRO GLN TRP PRO PRO TYR THR THR ALA ALA
SEQRES  40 A  543  GLN GLN TYR VAL SER LEU ASN LEU LYS PRO LEU GLU VAL
SEQRES  41 A  543  ARG ARG GLY LEU ARG ALA GLN THR CYS ALA PHE TRP ASN
SEQRES  42 A  543  ARG PHE LEU PRO LYS LEU LEU SER ALA THR
SEQRES   1 B  543  GLU GLY ARG GLU ASP PRO GLN LEU LEU VAL ARG VAL ARG
SEQRES   2 B  543  GLY GLY GLN LEU ARG GLY ILE ARG LEU LYS ALA PRO GLY
SEQRES   3 B  543  GLY PRO VAL SER ALA PHE LEU GLY ILE PRO PHE ALA GLU
SEQRES   4 B  543  PRO PRO VAL GLY SER ARG ARG PHE MET PRO PRO GLU PRO
SEQRES   5 B  543  LYS ARG PRO TRP SER GLY VAL LEU ASP ALA THR THR PHE
SEQRES   6 B  543  GLN ASN VAL CYS TYR GLN TYR VAL ASP THR LEU TYR PRO
SEQRES   7 B  543  GLY PHE GLU GLY THR GLU MET TRP ASN PRO ASN ARG GLU
SEQRES   8 B  543  LEU SER GLU ASP CYS LEU TYR LEU ASN VAL TRP THR PRO
SEQRES   9 B  543  TYR PRO ARG PRO ALA SER PRO THR PRO VAL LEU ILE TRP
SEQRES  10 B  543  ILE TYR GLY GLY GLY PHE TYR SER GLY ALA ALA SER LEU
SEQRES  11 B  543  ASP VAL TYR ASP GLY ARG PHE LEU ALA GLN VAL GLU GLY
SEQRES  12 B  543  ALA VAL LEU VAL SER MET ASN TYR ARG VAL GLY THR PHE
SEQRES  13 B  543  GLY PHE LEU ALA LEU PRO GLY SER ARG GLU ALA PRO GLY
SEQRES  14 B  543  ASN VAL GLY LEU LEU ASP GLN ARG LEU ALA LEU GLN TRP
SEQRES  15 B  543  VAL GLN GLU ASN ILE ALA ALA PHE GLY GLY ASP PRO MET
SEQRES  16 B  543  SER VAL THR LEU PHE GLY GLU SER ALA GLY ALA ALA SER
SEQRES  17 B  543  VAL GLY MET HIS ILE LEU SER LEU PRO SER ARG SER LEU
SEQRES  18 B  543  PHE HIS ARG ALA VAL LEU GLN SER GLY THR PRO ASN GLY
SEQRES  19 B  543  PRO TRP ALA THR VAL SER ALA GLY GLU ALA ARG ARG ARG
SEQRES  20 B  543  ALA THR LEU LEU ALA ARG LEU VAL GLY CYS PRO PRO GLY
SEQRES  21 B  543  GLY ALA GLY GLY ASN ASP THR GLU LEU ILE ALA CYS LEU
SEQRES  22 B  543  ARG THR ARG PRO ALA GLN ASP LEU VAL ASP HIS GLU TRP
SEQRES  23 B  543  HIS VAL LEU PRO GLN GLU SER ILE PHE ARG PHE SER PHE
SEQRES  24 B  543  VAL PRO VAL VAL ASP GLY ASP PHE LEU SER ASP THR PRO
SEQRES  25 B  543  GLU ALA LEU ILE ASN THR GLY ASP PHE GLN ASP LEU GLN
SEQRES  26 B  543  VAL LEU VAL GLY VAL VAL LYS ASP GLU GLY SER TYR PHE
SEQRES  27 B  543  LEU VAL TYR GLY VAL PRO GLY PHE SER LYS ASP ASN GLU
SEQRES  28 B  543  SER LEU ILE SER ARG ALA GLN PHE LEU ALA GLY VAL ARG
SEQRES  29 B  543  ILE GLY VAL PRO GLN ALA SER ASP LEU ALA ALA GLU ALA
SEQRES  30 B  543  VAL VAL LEU HIS TYR THR ASP TRP LEU HIS PRO GLU ASP
SEQRES  31 B  543  PRO THR HIS LEU ARG ASP ALA MET SER ALA VAL VAL GLY
SEQRES  32 B  543  ASP HIS ASN VAL VAL CYS PRO VAL ALA GLN LEU ALA GLY
SEQRES  33 B  543  ARG LEU ALA ALA GLN GLY ALA ARG VAL TYR ALA TYR ILE
SEQRES  34 B  543  PHE GLU HIS ARG ALA SER THR LEU THR TRP PRO LEU TRP
SEQRES  35 B  543  MET GLY VAL PRO HIS GLY TYR GLU ILE GLU PHE ILE PHE
SEQRES  36 B  543  GLY LEU PRO LEU ASP PRO SER LEU ASN TYR THR THR GLU
SEQRES  37 B  543  GLU ARG ILE PHE ALA GLN ARG LEU MET LYS TYR TRP THR
SEQRES  38 B  543  ASN PHE ALA ARG THR GLY ASP PRO ASN ASP PRO ARG ASP
SEQRES  39 B  543  SER LYS SER PRO GLN TRP PRO PRO TYR THR THR ALA ALA
SEQRES  40 B  543  GLN GLN TYR VAL SER LEU ASN LEU LYS PRO LEU GLU VAL
SEQRES  41 B  543  ARG ARG GLY LEU ARG ALA GLN THR CYS ALA PHE TRP ASN
SEQRES  42 B  543  ARG PHE LEU PRO LYS LEU LEU SER ALA THR
SEQRES   1 C  543  GLU GLY ARG GLU ASP PRO GLN LEU LEU VAL ARG VAL ARG
SEQRES   2 C  543  GLY GLY GLN LEU ARG GLY ILE ARG LEU LYS ALA PRO GLY
SEQRES   3 C  543  GLY PRO VAL SER ALA PHE LEU GLY ILE PRO PHE ALA GLU
SEQRES   4 C  543  PRO PRO VAL GLY SER ARG ARG PHE MET PRO PRO GLU PRO
SEQRES   5 C  543  LYS ARG PRO TRP SER GLY VAL LEU ASP ALA THR THR PHE
SEQRES   6 C  543  GLN ASN VAL CYS TYR GLN TYR VAL ASP THR LEU TYR PRO
SEQRES   7 C  543  GLY PHE GLU GLY THR GLU MET TRP ASN PRO ASN ARG GLU
SEQRES   8 C  543  LEU SER GLU ASP CYS LEU TYR LEU ASN VAL TRP THR PRO
SEQRES   9 C  543  TYR PRO ARG PRO ALA SER PRO THR PRO VAL LEU ILE TRP
SEQRES  10 C  543  ILE TYR GLY GLY GLY PHE TYR SER GLY ALA ALA SER LEU
SEQRES  11 C  543  ASP VAL TYR ASP GLY ARG PHE LEU ALA GLN VAL GLU GLY
SEQRES  12 C  543  ALA VAL LEU VAL SER MET ASN TYR ARG VAL GLY THR PHE
SEQRES  13 C  543  GLY PHE LEU ALA LEU PRO GLY SER ARG GLU ALA PRO GLY
SEQRES  14 C  543  ASN VAL GLY LEU LEU ASP GLN ARG LEU ALA LEU GLN TRP
SEQRES  15 C  543  VAL GLN GLU ASN ILE ALA ALA PHE GLY GLY ASP PRO MET
SEQRES  16 C  543  SER VAL THR LEU PHE GLY GLU SER ALA GLY ALA ALA SER
SEQRES  17 C  543  VAL GLY MET HIS ILE LEU SER LEU PRO SER ARG SER LEU
SEQRES  18 C  543  PHE HIS ARG ALA VAL LEU GLN SER GLY THR PRO ASN GLY
SEQRES  19 C  543  PRO TRP ALA THR VAL SER ALA GLY GLU ALA ARG ARG ARG
SEQRES  20 C  543  ALA THR LEU LEU ALA ARG LEU VAL GLY CYS PRO PRO GLY
SEQRES  21 C  543  GLY ALA GLY GLY ASN ASP THR GLU LEU ILE ALA CYS LEU
SEQRES  22 C  543  ARG THR ARG PRO ALA GLN ASP LEU VAL ASP HIS GLU TRP
SEQRES  23 C  543  HIS VAL LEU PRO GLN GLU SER ILE PHE ARG PHE SER PHE
SEQRES  24 C  543  VAL PRO VAL VAL ASP GLY ASP PHE LEU SER ASP THR PRO
SEQRES  25 C  543  GLU ALA LEU ILE ASN THR GLY ASP PHE GLN ASP LEU GLN
SEQRES  26 C  543  VAL LEU VAL GLY VAL VAL LYS ASP GLU GLY SER TYR PHE
SEQRES  27 C  543  LEU VAL TYR GLY VAL PRO GLY PHE SER LYS ASP ASN GLU
SEQRES  28 C  543  SER LEU ILE SER ARG ALA GLN PHE LEU ALA GLY VAL ARG
SEQRES  29 C  543  ILE GLY VAL PRO GLN ALA SER ASP LEU ALA ALA GLU ALA
SEQRES  30 C  543  VAL VAL LEU HIS TYR THR ASP TRP LEU HIS PRO GLU ASP
SEQRES  31 C  543  PRO THR HIS LEU ARG ASP ALA MET SER ALA VAL VAL GLY
SEQRES  32 C  543  ASP HIS ASN VAL VAL CYS PRO VAL ALA GLN LEU ALA GLY
SEQRES  33 C  543  ARG LEU ALA ALA GLN GLY ALA ARG VAL TYR ALA TYR ILE
SEQRES  34 C  543  PHE GLU HIS ARG ALA SER THR LEU THR TRP PRO LEU TRP
SEQRES  35 C  543  MET GLY VAL PRO HIS GLY TYR GLU ILE GLU PHE ILE PHE
SEQRES  36 C  543  GLY LEU PRO LEU ASP PRO SER LEU ASN TYR THR THR GLU
SEQRES  37 C  543  GLU ARG ILE PHE ALA GLN ARG LEU MET LYS TYR TRP THR
SEQRES  38 C  543  ASN PHE ALA ARG THR GLY ASP PRO ASN ASP PRO ARG ASP
SEQRES  39 C  543  SER LYS SER PRO GLN TRP PRO PRO TYR THR THR ALA ALA
SEQRES  40 C  543  GLN GLN TYR VAL SER LEU ASN LEU LYS PRO LEU GLU VAL
SEQRES  41 C  543  ARG ARG GLY LEU ARG ALA GLN THR CYS ALA PHE TRP ASN
SEQRES  42 C  543  ARG PHE LEU PRO LYS LEU LEU SER ALA THR
SEQRES   1 D  543  GLU GLY ARG GLU ASP PRO GLN LEU LEU VAL ARG VAL ARG
SEQRES   2 D  543  GLY GLY GLN LEU ARG GLY ILE ARG LEU LYS ALA PRO GLY
SEQRES   3 D  543  GLY PRO VAL SER ALA PHE LEU GLY ILE PRO PHE ALA GLU
SEQRES   4 D  543  PRO PRO VAL GLY SER ARG ARG PHE MET PRO PRO GLU PRO
SEQRES   5 D  543  LYS ARG PRO TRP SER GLY VAL LEU ASP ALA THR THR PHE
SEQRES   6 D  543  GLN ASN VAL CYS TYR GLN TYR VAL ASP THR LEU TYR PRO
SEQRES   7 D  543  GLY PHE GLU GLY THR GLU MET TRP ASN PRO ASN ARG GLU
SEQRES   8 D  543  LEU SER GLU ASP CYS LEU TYR LEU ASN VAL TRP THR PRO
SEQRES   9 D  543  TYR PRO ARG PRO ALA SER PRO THR PRO VAL LEU ILE TRP
SEQRES  10 D  543  ILE TYR GLY GLY GLY PHE TYR SER GLY ALA ALA SER LEU
SEQRES  11 D  543  ASP VAL TYR ASP GLY ARG PHE LEU ALA GLN VAL GLU GLY
SEQRES  12 D  543  ALA VAL LEU VAL SER MET ASN TYR ARG VAL GLY THR PHE
SEQRES  13 D  543  GLY PHE LEU ALA LEU PRO GLY SER ARG GLU ALA PRO GLY
SEQRES  14 D  543  ASN VAL GLY LEU LEU ASP GLN ARG LEU ALA LEU GLN TRP
SEQRES  15 D  543  VAL GLN GLU ASN ILE ALA ALA PHE GLY GLY ASP PRO MET
SEQRES  16 D  543  SER VAL THR LEU PHE GLY GLU SER ALA GLY ALA ALA SER
SEQRES  17 D  543  VAL GLY MET HIS ILE LEU SER LEU PRO SER ARG SER LEU
SEQRES  18 D  543  PHE HIS ARG ALA VAL LEU GLN SER GLY THR PRO ASN GLY
SEQRES  19 D  543  PRO TRP ALA THR VAL SER ALA GLY GLU ALA ARG ARG ARG
SEQRES  20 D  543  ALA THR LEU LEU ALA ARG LEU VAL GLY CYS PRO PRO GLY
SEQRES  21 D  543  GLY ALA GLY GLY ASN ASP THR GLU LEU ILE ALA CYS LEU
SEQRES  22 D  543  ARG THR ARG PRO ALA GLN ASP LEU VAL ASP HIS GLU TRP
SEQRES  23 D  543  HIS VAL LEU PRO GLN GLU SER ILE PHE ARG PHE SER PHE
SEQRES  24 D  543  VAL PRO VAL VAL ASP GLY ASP PHE LEU SER ASP THR PRO
SEQRES  25 D  543  GLU ALA LEU ILE ASN THR GLY ASP PHE GLN ASP LEU GLN
SEQRES  26 D  543  VAL LEU VAL GLY VAL VAL LYS ASP GLU GLY SER TYR PHE
SEQRES  27 D  543  LEU VAL TYR GLY VAL PRO GLY PHE SER LYS ASP ASN GLU
SEQRES  28 D  543  SER LEU ILE SER ARG ALA GLN PHE LEU ALA GLY VAL ARG
SEQRES  29 D  543  ILE GLY VAL PRO GLN ALA SER ASP LEU ALA ALA GLU ALA
SEQRES  30 D  543  VAL VAL LEU HIS TYR THR ASP TRP LEU HIS PRO GLU ASP
SEQRES  31 D  543  PRO THR HIS LEU ARG ASP ALA MET SER ALA VAL VAL GLY
SEQRES  32 D  543  ASP HIS ASN VAL VAL CYS PRO VAL ALA GLN LEU ALA GLY
SEQRES  33 D  543  ARG LEU ALA ALA GLN GLY ALA ARG VAL TYR ALA TYR ILE
SEQRES  34 D  543  PHE GLU HIS ARG ALA SER THR LEU THR TRP PRO LEU TRP
SEQRES  35 D  543  MET GLY VAL PRO HIS GLY TYR GLU ILE GLU PHE ILE PHE
SEQRES  36 D  543  GLY LEU PRO LEU ASP PRO SER LEU ASN TYR THR THR GLU
SEQRES  37 D  543  GLU ARG ILE PHE ALA GLN ARG LEU MET LYS TYR TRP THR
SEQRES  38 D  543  ASN PHE ALA ARG THR GLY ASP PRO ASN ASP PRO ARG ASP
SEQRES  39 D  543  SER LYS SER PRO GLN TRP PRO PRO TYR THR THR ALA ALA
SEQRES  40 D  543  GLN GLN TYR VAL SER LEU ASN LEU LYS PRO LEU GLU VAL
SEQRES  41 D  543  ARG ARG GLY LEU ARG ALA GLN THR CYS ALA PHE TRP ASN
SEQRES  42 D  543  ARG PHE LEU PRO LYS LEU LEU SER ALA THR
MODRES 5FKJ ASN A  265  ASN  GLYCOSYLATION SITE
MODRES 5FKJ ASN B  265  ASN  GLYCOSYLATION SITE
MODRES 5FKJ ASN B  350  ASN  GLYCOSYLATION SITE
MODRES 5FKJ ASN C  265  ASN  GLYCOSYLATION SITE
MODRES 5FKJ ASN D  265  ASN  GLYCOSYLATION SITE
MODRES 5FKJ ASN D  350  ASN  GLYCOSYLATION SITE
HET    G0W  A 550      49
HET    NAG  A 560      14
HET     CL  A 601       1
HET     CL  A 604       1
HET     CL  A 605       1
HET     CL  A 606       1
HET     CL  A 607       1
HET     CL  A 608       1
HET     CL  A 609       1
HET     CL  A 610       1
HET     CL  A 611       1
HET    G0W  B 550      31
HET    NAG  B 560      14
HET    NAG  B 561      14
HET     CL  B 605       1
HET     CL  B 606       1
HET     CL  B 607       1
HET     CL  B 608       1
HET    SO4  B1542       5
HET    G0W  C 550      49
HET    NAG  C 560      14
HET     CL  C 603       1
HET     CL  C 605       1
HET     CL  C 606       1
HET     CL  C 607       1
HET     CL  C 608       1
HET     CL  C 609       1
HET     CL  C 610       1
HET     CL  C 611       1
HET     CL  C 612       1
HET    SO4  C1541       5
HET    G0W  D 550      31
HET    NAG  D 560      14
HET    NAG  D 561      14
HET     CL  D 605       1
HET     CL  D 606       1
HET     CL  D 607       1
HET     CL  D 608       1
HET     CL  D 609       1
HET     CL  D 610       1
HET    SO4  D1540       5
HETNAM     G0W 1,3-BIS[5(DIETHYL-O-NITROBENZYLAMMONIUM)PENTYL]-6-
HETNAM   2 G0W  METHYLURACIL
HETNAM     NAG N-ACETYL-D-GLUCOSAMINE
HETNAM      CL CHLORIDE ION
HETNAM     SO4 SULFATE ION
FORMUL   5  G0W    4(C37 H56 N6 O6 2+)
FORMUL   6  NAG    6(C8 H15 N O6)
FORMUL   7   CL    28(CL 1-)
FORMUL  23  SO4    3(O4 S 2-)
FORMUL  46  HOH   *374(H2 O)
HELIX    1   1 VAL A   42  ARG A   46  5                                   5
HELIX    2   2 PHE A   80  MET A   85  1                                   6
HELIX    3   3 LEU A  130  ASP A  134  5                                   5
HELIX    4   4 GLY A  135  GLY A  143  1                                   9
HELIX    5   5 VAL A  153  LEU A  159  1                                   7
HELIX    6   6 ASN A  170  ILE A  187  1                                  18
HELIX    7   7 ALA A  188  PHE A  190  5                                   3
HELIX    8   8 SER A  203  SER A  215  1                                  13
HELIX    9   9 SER A  215  SER A  220  1                                   6
HELIX   10  10 SER A  240  VAL A  255  1                                  16
HELIX   11  11 ASN A  265  ARG A  274  1                                  10
HELIX   12  12 PRO A  277  HIS A  284  1                                   8
HELIX   13  13 GLU A  285  LEU A  289  5                                   5
HELIX   14  14 THR A  311  GLY A  319  1                                   9
HELIX   15  15 GLY A  335  GLY A  342  5                                   8
HELIX   16  16 SER A  355  VAL A  367  1                                  13
HELIX   17  17 SER A  371  THR A  383  1                                  13
HELIX   18  18 ASP A  390  VAL A  407  1                                  18
HELIX   19  19 VAL A  407  GLN A  421  1                                  15
HELIX   20  20 PRO A  440  GLY A  444  5                                   5
HELIX   21  21 GLU A  450  PHE A  455  1                                   6
HELIX   22  22 GLY A  456  ASP A  460  5                                   5
HELIX   23  23 ASP A  460  ASN A  464  5                                   5
HELIX   24  24 THR A  466  GLY A  487  1                                  22
HELIX   25  25 ARG A  525  ARG A  534  1                                  10
HELIX   26  26 PHE A  535  LEU A  540  5                                   6
HELIX   27  27 VAL B   42  ARG B   46  5                                   5
HELIX   28  28 PHE B   80  MET B   85  1                                   6
HELIX   29  29 LEU B  130  ASP B  134  5                                   5
HELIX   30  30 GLY B  135  GLY B  143  1                                   9
HELIX   31  31 VAL B  153  LEU B  159  1                                   7
HELIX   32  32 ASN B  170  ILE B  187  1                                  18
HELIX   33  33 ALA B  188  PHE B  190  5                                   3
HELIX   34  34 SER B  203  SER B  215  1                                  13
HELIX   35  35 LEU B  216  LEU B  221  5                                   6
HELIX   36  36 SER B  240  VAL B  255  1                                  16
HELIX   37  37 ASN B  265  THR B  275  1                                  11
HELIX   38  38 PRO B  277  HIS B  284  1                                   8
HELIX   39  39 GLU B  285  LEU B  289  5                                   5
HELIX   40  40 THR B  311  GLY B  319  1                                   9
HELIX   41  41 SER B  336  GLY B  342  5                                   7
HELIX   42  42 SER B  355  VAL B  367  1                                  13
HELIX   43  43 SER B  371  THR B  383  1                                  13
HELIX   44  44 ASP B  390  VAL B  407  1                                  18
HELIX   45  45 VAL B  407  GLN B  421  1                                  15
HELIX   46  46 PRO B  440  GLY B  444  5                                   5
HELIX   47  47 GLU B  450  PHE B  455  1                                   6
HELIX   48  48 GLY B  456  ASP B  460  5                                   5
HELIX   49  49 ASP B  460  ASN B  464  5                                   5
HELIX   50  50 THR B  466  GLY B  487  1                                  22
HELIX   51  51 ARG B  525  ARG B  534  1                                  10
HELIX   52  52 ARG B  534  SER B  541  1                                   8
HELIX   53  53 VAL C   42  ARG C   46  5                                   5
HELIX   54  54 PHE C   80  MET C   85  1                                   6
HELIX   55  55 LEU C  130  ASP C  134  5                                   5
HELIX   56  56 GLY C  135  GLY C  143  1                                   9
HELIX   57  57 GLY C  154  LEU C  159  1                                   6
HELIX   58  58 ASN C  170  ILE C  187  1                                  18
HELIX   59  59 ALA C  188  PHE C  190  5                                   3
HELIX   60  60 SER C  203  SER C  215  1                                  13
HELIX   61  61 LEU C  216  PHE C  222  5                                   7
HELIX   62  62 SER C  240  VAL C  255  1                                  16
HELIX   63  63 ASN C  265  ARG C  274  1                                  10
HELIX   64  64 PRO C  277  GLU C  285  1                                   9
HELIX   65  65 TRP C  286  LEU C  289  5                                   4
HELIX   66  66 THR C  311  GLY C  319  1                                   9
HELIX   67  67 GLY C  335  GLY C  342  5                                   8
HELIX   68  68 SER C  355  VAL C  367  1                                  13
HELIX   69  69 SER C  371  THR C  383  1                                  13
HELIX   70  70 ASP C  390  VAL C  407  1                                  18
HELIX   71  71 VAL C  407  GLN C  421  1                                  15
HELIX   72  72 PRO C  440  GLY C  444  5                                   5
HELIX   73  73 GLU C  450  PHE C  455  1                                   6
HELIX   74  74 GLY C  456  ASP C  460  5                                   5
HELIX   75  75 ASP C  460  ASN C  464  5                                   5
HELIX   76  76 THR C  466  GLY C  487  1                                  22
HELIX   77  77 ARG C  525  ARG C  534  1                                  10
HELIX   78  78 PHE C  535  LEU C  539  5                                   5
HELIX   79  79 ASP D    5  GLN D    7  5                                   3
HELIX   80  80 VAL D   42  ARG D   46  5                                   5
HELIX   81  81 PHE D   80  MET D   85  1                                   6
HELIX   82  82 LEU D  130  ASP D  134  5                                   5
HELIX   83  83 GLY D  135  GLY D  143  1                                   9
HELIX   84  84 VAL D  153  LEU D  159  1                                   7
HELIX   85  85 ASN D  170  ILE D  187  1                                  18
HELIX   86  86 ALA D  188  PHE D  190  5                                   3
HELIX   87  87 SER D  203  SER D  215  1                                  13
HELIX   88  88 LEU D  216  PHE D  222  5                                   7
HELIX   89  89 SER D  240  VAL D  255  1                                  16
HELIX   90  90 ASN D  265  ARG D  274  1                                  10
HELIX   91  91 PRO D  277  GLU D  285  1                                   9
HELIX   92  92 TRP D  286  LEU D  289  5                                   4
HELIX   93  93 THR D  311  GLY D  319  1                                   9
HELIX   94  94 SER D  336  GLY D  342  5                                   7
HELIX   95  95 SER D  355  VAL D  367  1                                  13
HELIX   96  96 SER D  371  THR D  383  1                                  13
HELIX   97  97 ASP D  390  VAL D  407  1                                  18
HELIX   98  98 VAL D  407  GLN D  421  1                                  15
HELIX   99  99 PRO D  440  GLY D  444  5                                   5
HELIX  100 100 GLU D  450  PHE D  455  1                                   6
HELIX  101 101 GLY D  456  ASP D  460  5                                   5
HELIX  102 102 ASP D  460  ASN D  464  5                                   5
HELIX  103 103 THR D  466  GLY D  487  1                                  22
HELIX  104 104 ARG D  525  LEU D  539  1                                  15
SHEET    1  AA 3 LEU A   9  VAL A  12  0
SHEET    2  AA 3 GLY A  15  ARG A  18 -1  O  GLY A  15   N  VAL A  12
SHEET    3  AA 3 VAL A  59  ASP A  61  1  O  LEU A  60   N  ARG A  18
SHEET    1  AB11 ILE A  20  ALA A  24  0
SHEET    2  AB11 GLY A  27  PRO A  36 -1  O  GLY A  27   N  ALA A  24
SHEET    3  AB11 TYR A  98  PRO A 104 -1  O  LEU A  99   N  ILE A  35
SHEET    4  AB11 VAL A 145  MET A 149 -1  O  LEU A 146   N  TRP A 102
SHEET    5  AB11 THR A 112  ILE A 118  1  O  PRO A 113   N  VAL A 145
SHEET    6  AB11 GLY A 192  GLU A 202  1  N  ASP A 193   O  THR A 112
SHEET    7  AB11 ARG A 224  GLN A 228  1  O  ARG A 224   N  LEU A 199
SHEET    8  AB11 GLN A 325  VAL A 331  1  O  GLN A 325   N  ALA A 225
SHEET    9  AB11 ARG A 424  PHE A 430  1  O  ARG A 424   N  VAL A 326
SHEET   10  AB11 GLN A 509  LEU A 513  1  O  VAL A 511   N  ILE A 429
SHEET   11  AB11 GLU A 519  ARG A 522 -1  O  GLU A 519   N  SER A 512
SHEET    1  AC 2 VAL A  68  CYS A  69  0
SHEET    2  AC 2 LEU A  92  SER A  93  1  N  SER A  93   O  VAL A  68
SHEET    1  BA 3 LEU B   9  VAL B  12  0
SHEET    2  BA 3 GLY B  15  ARG B  18 -1  O  GLY B  15   N  VAL B  12
SHEET    3  BA 3 VAL B  59  ASP B  61  1  O  LEU B  60   N  ARG B  18
SHEET    1  BB11 ILE B  20  ALA B  24  0
SHEET    2  BB11 GLY B  27  ILE B  35 -1  O  GLY B  27   N  ALA B  24
SHEET    3  BB11 LEU B  99  PRO B 104 -1  O  LEU B  99   N  ILE B  35
SHEET    4  BB11 VAL B 145  MET B 149 -1  O  LEU B 146   N  TRP B 102
SHEET    5  BB11 THR B 112  ILE B 118  1  O  PRO B 113   N  VAL B 145
SHEET    6  BB11 GLY B 192  GLU B 202  1  N  ASP B 193   O  THR B 112
SHEET    7  BB11 ARG B 224  GLN B 228  1  O  ARG B 224   N  LEU B 199
SHEET    8  BB11 GLN B 325  VAL B 331  1  O  GLN B 325   N  ALA B 225
SHEET    9  BB11 ARG B 424  PHE B 430  1  O  ARG B 424   N  VAL B 326
SHEET   10  BB11 GLN B 509  LEU B 513  1  O  VAL B 511   N  ILE B 429
SHEET   11  BB11 GLU B 519  ARG B 522 -1  O  GLU B 519   N  SER B 512
SHEET    1  BC 2 VAL B  68  CYS B  69  0
SHEET    2  BC 2 LEU B  92  SER B  93  1  N  SER B  93   O  VAL B  68
SHEET    1  CA 3 LEU C   9  ARG C  11  0
SHEET    2  CA 3 GLN C  16  ARG C  18 -1  O  LEU C  17   N  VAL C  10
SHEET    3  CA 3 VAL C  59  ASP C  61  1  O  LEU C  60   N  ARG C  18
SHEET    1  CB11 ILE C  20  ALA C  24  0
SHEET    2  CB11 GLY C  27  PRO C  36 -1  O  GLY C  27   N  ALA C  24
SHEET    3  CB11 TYR C  98  PRO C 104 -1  O  LEU C  99   N  ILE C  35
SHEET    4  CB11 VAL C 145  MET C 149 -1  O  LEU C 146   N  TRP C 102
SHEET    5  CB11 THR C 112  ILE C 118  1  O  PRO C 113   N  VAL C 145
SHEET    6  CB11 GLY C 192  GLU C 202  1  N  ASP C 193   O  THR C 112
SHEET    7  CB11 ARG C 224  GLN C 228  1  O  ARG C 224   N  LEU C 199
SHEET    8  CB11 GLN C 325  VAL C 331  1  O  GLN C 325   N  ALA C 225
SHEET    9  CB11 ARG C 424  PHE C 430  1  O  ARG C 424   N  VAL C 326
SHEET   10  CB11 GLN C 509  LEU C 513  1  O  VAL C 511   N  ILE C 429
SHEET   11  CB11 GLU C 519  ARG C 522 -1  O  GLU C 519   N  SER C 512
SHEET    1  CC 2 ALA C  38  GLU C  39  0
SHEET    2  CC 2 GLU C  51  PRO C  52 -1  O  GLU C  51   N  GLU C  39
SHEET    1  CD 2 VAL C  68  CYS C  69  0
SHEET    2  CD 2 LEU C  92  SER C  93  1  N  SER C  93   O  VAL C  68
SHEET    1  DA 3 LEU D   9  ARG D  11  0
SHEET    2  DA 3 GLN D  16  ARG D  18 -1  O  LEU D  17   N  VAL D  10
SHEET    3  DA 3 VAL D  59  ASP D  61  1  O  LEU D  60   N  ARG D  18
SHEET    1  DB11 ILE D  20  ALA D  24  0
SHEET    2  DB11 GLY D  27  PRO D  36 -1  O  GLY D  27   N  ALA D  24
SHEET    3  DB11 TYR D  98  PRO D 104 -1  O  LEU D  99   N  ILE D  35
SHEET    4  DB11 VAL D 145  MET D 149 -1  O  LEU D 146   N  TRP D 102
SHEET    5  DB11 THR D 112  ILE D 118  1  O  PRO D 113   N  VAL D 145
SHEET    6  DB11 GLY D 192  GLU D 202  1  N  ASP D 193   O  THR D 112
SHEET    7  DB11 ARG D 224  GLN D 228  1  O  ARG D 224   N  LEU D 199
SHEET    8  DB11 GLN D 325  VAL D 331  1  O  GLN D 325   N  ALA D 225
SHEET    9  DB11 ARG D 424  PHE D 430  1  O  ARG D 424   N  VAL D 326
SHEET   10  DB11 GLN D 509  LEU D 513  1  O  VAL D 511   N  ILE D 429
SHEET   11  DB11 GLU D 519  ARG D 522 -1  O  GLU D 519   N  SER D 512
SHEET    1  DC 2 VAL D  68  CYS D  69  0
SHEET    2  DC 2 LEU D  92  SER D  93  1  N  SER D  93   O  VAL D  68
SSBOND   1 CYS A   69    CYS A   96                          1555   1555  2.02
SSBOND   2 CYS A  257    CYS A  272                          1555   1555  2.04
SSBOND   3 CYS A  409    CYS A  529                          1555   1555  2.03
SSBOND   4 CYS B   69    CYS B   96                          1555   1555  2.03
SSBOND   5 CYS B  257    CYS B  272                          1555   1555  2.02
SSBOND   6 CYS B  409    CYS B  529                          1555   1555  2.04
SSBOND   7 CYS C   69    CYS C   96                          1555   1555  2.04
SSBOND   8 CYS C  257    CYS C  272                          1555   1555  2.02
SSBOND   9 CYS C  409    CYS C  529                          1555   1555  2.04
SSBOND  10 CYS D   69    CYS D   96                          1555   1555  2.03
SSBOND  11 CYS D  257    CYS D  272                          1555   1555  2.04
SSBOND  12 CYS D  409    CYS D  529                          1555   1555  2.03
LINK         ND2 ASN A 265                 C1  NAG A 560     1555   1555  1.45
LINK         ND2 ASN B 265                 C1  NAG B 560     1555   1555  1.46
LINK         ND2 ASN B 350                 C1  NAG B 561     1555   1555  1.45
LINK         ND2 ASN C 265                 C1  NAG C 560     1555   1555  1.45
LINK         ND2 ASN D 265                 C1  NAG D 560     1555   1555  1.46
LINK         ND2 ASN D 350                 C1  NAG D 561     1555   1555  1.45
CISPEP   1 TYR A  105    PRO A  106          0         2.77
CISPEP   2 PRO A  258    PRO A  259          0        -6.34
CISPEP   3 TYR B  105    PRO B  106          0        -1.02
CISPEP   4 CYS B  257    PRO B  258          0       -12.13
CISPEP   5 TYR C  105    PRO C  106          0         3.66
CISPEP   6 PRO C  258    PRO C  259          0        -6.72
CISPEP   7 SER C  497    PRO C  498          0         5.53
CISPEP   8 TYR D  105    PRO D  106          0         1.89
CISPEP   9 CYS D  257    PRO D  258          0        -7.45
SITE     1 AC1 22 TYR A  72  ASP A  74  TRP A  86  GLY A 121
SITE     2 AC1 22 TYR A 124  GLU A 202  SER A 203  ASP A 283
SITE     3 AC1 22 TRP A 286  HIS A 287  SER A 293  PHE A 295
SITE     4 AC1 22 TYR A 337  PHE A 338  TYR A 341  HIS A 447
SITE     5 AC1 22 ARG D 253  GLY D 256  PRO D 258  PRO D 259
SITE     6 AC1 22 GLY D 261  ALA D 262
SITE     1 AC2 11 TRP B  86  GLY B 121  TYR B 124  SER B 203
SITE     2 AC2 11 TRP B 286  SER B 293  PHE B 295  TYR B 337
SITE     3 AC2 11 PHE B 338  TYR B 341  TRP B 439
SITE     1 AC3 22 ARG B 253  PRO B 258  PRO B 259  GLY B 261
SITE     2 AC3 22 ALA B 262  TYR C  72  ASP C  74  TRP C  86
SITE     3 AC3 22 GLY C 121  TYR C 124  GLU C 202  SER C 203
SITE     4 AC3 22 ASP C 283  TRP C 286  HIS C 287  ILE C 294
SITE     5 AC3 22 PHE C 295  ARG C 296  TYR C 337  PHE C 338
SITE     6 AC3 22 TYR C 341  HOH C2017
SITE     1 AC4 12 ASP D  74  TRP D  86  GLY D 121  TYR D 124
SITE     2 AC4 12 GLU D 202  SER D 203  TRP D 286  PHE D 295
SITE     3 AC4 12 TYR D 337  PHE D 338  TYR D 341  HOH D2022
SITE     1 AC5  4 ARG D 525  ALA D 526  GLN D 527  THR D 528
SITE     1 AC6  4 ARG B 525  ALA B 526  GLN B 527  THR B 528
SITE     1 AC7  4 ARG C 525  ALA C 526  GLN C 527  THR C 528
SITE     1 AC8  1 GLN A 413
SITE     1 AC9  1 LEU A 515
SITE     1 BC1  1 GLN A 527
SITE     1 BC2  1 ARG A 356
SITE     1 BC3  1 ARG A 136
SITE     1 BC4  1 HOH B2049
SITE     1 BC5  1 ARG B 356
SITE     1 BC6  1 LYS B 332
SITE     1 BC7  1 GLN B 413
SITE     1 BC8  1 SER B 240
SITE     1 BC9  1 ARG C 356
SITE     1 CC1  1 SER C  44
SITE     1 CC2  1 ASP C 333
SITE     1 CC3  1 ARG D  45
SITE     1 CC4  1 GLN C 413
SITE     1 CC5  1 SER C 240
SITE     1 CC6  1 ARG D 356
SITE     1 CC7  1 ARG D 136
SITE     1 CC8  1 ARG C  11
SITE     1 CC9  1 ARG D 525
SITE     1 DC1  2 ASN A 265  GLU A 268
SITE     1 DC2  1 ASN B 265
SITE     1 DC3  2 ASN B 350  LEU B 353
SITE     1 DC4  2 ASN C 265  GLU C 268
SITE     1 DC5  2 ASN D 265  THR D 267
SITE     1 DC6  2 SER D 347  ASN D 350
CRYST1  137.150  175.450  224.400  90.00  90.00  90.00 P 21 21 21   16
ORIGX1      1.000000  0.000000  0.000000        0.00000
ORIGX2      0.000000  1.000000  0.000000        0.00000
ORIGX3      0.000000  0.000000  1.000000        0.00000
SCALE1      0.007291  0.000000  0.000000        0.00000
SCALE2      0.000000  0.005700  0.000000        0.00000
SCALE3      0.000000  0.000000  0.004456        0.00000
TER    4212      THR A 543
TER    8420      SER B 541
TER   12606      LEU C 539
TER   16780      LEU D 539
MASTER      579    0   41  104   66    0   47    617437    4  289  168
END