longtext: 5j8j-pdb

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HEADER    HYDROLASE                               07-APR-16   5J8J
TITLE     A HISTONE DEACETYLASE FROM SACCHAROMYCES CEREVISIAE
COMPND    MOL_ID: 1;
COMPND   2 MOLECULE: HISTONE DEACETYLASE HDA1;
COMPND   3 CHAIN: A;
COMPND   4 FRAGMENT: UNP RESIDUES 457-698;
COMPND   5 EC: 3.5.1.98;
COMPND   6 ENGINEERED: YES
SOURCE    MOL_ID: 1;
SOURCE   2 ORGANISM_SCIENTIFIC: SACCHAROMYCES CEREVISIAE (STRAIN ATCC 204508 /
SOURCE   3 S288C);
SOURCE   4 ORGANISM_COMMON: BAKER'S YEAST;
SOURCE   5 ORGANISM_TAXID: 559292;
SOURCE   6 STRAIN: ATCC 204508 / S288C;
SOURCE   7 GENE: HDA1, YNL021W, N2819;
SOURCE   8 EXPRESSION_SYSTEM: ESCHERICHIA COLI;
SOURCE   9 EXPRESSION_SYSTEM_TAXID: 562
KEYWDS    ROSSMANN FOLD, DEACETYLASE, HYDROLASE
EXPDTA    X-RAY DIFFRACTION
AUTHOR    Y.ZHU,H.SHEN,X.LI,M.TENG
REVDAT   1   19-APR-17 5J8J    0
JRNL        AUTH   H.SHEN,Y.ZHU,C.WANG,H.YAN,M.TENG,X.LI
JRNL        TITL   STRUCTURAL AND HISTONE BINDING ABILITY CHARACTERIZATION OF
JRNL        TITL 2 THE ARB2 DOMAIN OF A HISTONE DEACETYLASE HDA1 FROM
JRNL        TITL 3 SACCHAROMYCES CEREVISIAE.
JRNL        REF    SCI REP                       V.   6 33905 2016
JRNL        REFN                   ESSN 2045-2322
JRNL        PMID   27665728
JRNL        DOI    10.1038/SREP33905
REMARK   2
REMARK   2 RESOLUTION.    2.72 ANGSTROMS.
REMARK   3
REMARK   3 REFINEMENT.
REMARK   3   PROGRAM     : PHENIX 1.9_1692
REMARK   3   AUTHORS     : PAUL ADAMS,PAVEL AFONINE,VINCENT CHEN,IAN
REMARK   3               : DAVIS,KRESHNA GOPAL,RALF GROSSE-KUNSTLEVE,
REMARK   3               : LI-WEI HUNG,ROBERT IMMORMINO,TOM IOERGER,
REMARK   3               : AIRLIE MCCOY,ERIK MCKEE,NIGEL MORIARTY,
REMARK   3               : REETAL PAI,RANDY READ,JANE RICHARDSON,
REMARK   3               : DAVID RICHARDSON,TOD ROMO,JIM SACCHETTINI,
REMARK   3               : NICHOLAS SAUTER,JACOB SMITH,LAURENT
REMARK   3               : STORONI,TOM TERWILLIGER,PETER ZWART
REMARK   3
REMARK   3    REFINEMENT TARGET : NULL
REMARK   3
REMARK   3  DATA USED IN REFINEMENT.
REMARK   3   RESOLUTION RANGE HIGH (ANGSTROMS) : 2.72
REMARK   3   RESOLUTION RANGE LOW  (ANGSTROMS) : 40.28
REMARK   3   MIN(FOBS/SIGMA_FOBS)              : 1.360
REMARK   3   COMPLETENESS FOR RANGE        (%) : 97.6
REMARK   3   NUMBER OF REFLECTIONS             : 14934
REMARK   3
REMARK   3  FIT TO DATA USED IN REFINEMENT.
REMARK   3   R VALUE     (WORKING + TEST SET) : 0.192
REMARK   3   R VALUE            (WORKING SET) : 0.190
REMARK   3   FREE R VALUE                     : 0.238
REMARK   3   FREE R VALUE TEST SET SIZE   (%) : 5.230
REMARK   3   FREE R VALUE TEST SET COUNT      : 781
REMARK   3
REMARK   3  FIT TO DATA USED IN REFINEMENT (IN BINS).
REMARK   3   BIN  RESOLUTION RANGE  COMPL.    NWORK NFREE   RWORK  RFREE
REMARK   3     1 40.2885 -  4.9328    0.97     2456   123  0.1746 0.2090
REMARK   3     2  4.9328 -  3.9164    0.99     2407   131  0.1706 0.2006
REMARK   3     3  3.9164 -  3.4216    0.99     2358   137  0.1918 0.2622
REMARK   3     4  3.4216 -  3.1089    0.98     2338   136  0.2282 0.3164
REMARK   3     5  3.1089 -  2.8861    0.98     2334   135  0.2557 0.3408
REMARK   3     6  2.8861 -  2.7160    0.95     2260   119  0.2798 0.3546
REMARK   3
REMARK   3  BULK SOLVENT MODELLING.
REMARK   3   METHOD USED        : NULL
REMARK   3   SOLVENT RADIUS     : 1.11
REMARK   3   SHRINKAGE RADIUS   : 0.90
REMARK   3   K_SOL              : NULL
REMARK   3   B_SOL              : NULL
REMARK   3
REMARK   3  ERROR ESTIMATES.
REMARK   3   COORDINATE ERROR (MAXIMUM-LIKELIHOOD BASED)     : 0.370
REMARK   3   PHASE ERROR (DEGREES, MAXIMUM-LIKELIHOOD BASED) : 29.820
REMARK   3
REMARK   3  B VALUES.
REMARK   3   FROM WILSON PLOT           (A**2) : NULL
REMARK   3   MEAN B VALUE      (OVERALL, A**2) : NULL
REMARK   3   OVERALL ANISOTROPIC B VALUE.
REMARK   3    B11 (A**2) : NULL
REMARK   3    B22 (A**2) : NULL
REMARK   3    B33 (A**2) : NULL
REMARK   3    B12 (A**2) : NULL
REMARK   3    B13 (A**2) : NULL
REMARK   3    B23 (A**2) : NULL
REMARK   3
REMARK   3  TWINNING INFORMATION.
REMARK   3   FRACTION: NULL
REMARK   3   OPERATOR: NULL
REMARK   3
REMARK   3  DEVIATIONS FROM IDEAL VALUES.
REMARK   3                 RMSD          COUNT
REMARK   3   BOND      :  0.009           1979
REMARK   3   ANGLE     :  1.281           2698
REMARK   3   CHIRALITY :  0.049            312
REMARK   3   PLANARITY :  0.006            343
REMARK   3   DIHEDRAL  : 13.900            696
REMARK   3
REMARK   3  TLS DETAILS
REMARK   3   NUMBER OF TLS GROUPS  : 1
REMARK   3   TLS GROUP : 1
REMARK   3    SELECTION: ALL
REMARK   3    ORIGIN FOR THE GROUP (A): -46.2438  18.2399 -25.4993
REMARK   3    T TENSOR
REMARK   3      T11:   0.8134 T22:   0.7455
REMARK   3      T33:   0.8099 T12:  -0.0211
REMARK   3      T13:   0.1091 T23:   0.0487
REMARK   3    L TENSOR
REMARK   3      L11:   0.8873 L22:   2.5034
REMARK   3      L33:   2.5582 L12:  -0.7118
REMARK   3      L13:   1.0061 L23:  -0.2788
REMARK   3    S TENSOR
REMARK   3      S11:   0.1827 S12:   0.0380 S13:  -0.0494
REMARK   3      S21:  -0.1766 S22:  -0.0960 S23:  -0.0876
REMARK   3      S31:  -0.0447 S32:   0.2345 S33:  -0.0440
REMARK   3
REMARK   3  NCS DETAILS
REMARK   3   NUMBER OF NCS GROUPS : NULL
REMARK   3
REMARK   3  OTHER REFINEMENT REMARKS: NULL
REMARK   4
REMARK   4 5J8J COMPLIES WITH FORMAT V. 3.30, 13-JUL-11
REMARK 100
REMARK 100 THIS ENTRY HAS BEEN PROCESSED BY PDBJ ON 14-APR-16.
REMARK 100 THE DEPOSITION ID IS D_1000220112.
REMARK 200
REMARK 200 EXPERIMENTAL DETAILS
REMARK 200  EXPERIMENT TYPE                : X-RAY DIFFRACTION
REMARK 200  DATE OF DATA COLLECTION        : 22-MAR-16
REMARK 200  TEMPERATURE           (KELVIN) : 100
REMARK 200  PH                             : 4.6
REMARK 200  NUMBER OF CRYSTALS USED        : 1
REMARK 200
REMARK 200  SYNCHROTRON              (Y/N) : Y
REMARK 200  RADIATION SOURCE               : APS
REMARK 200  BEAMLINE                       : 17-BM
REMARK 200  X-RAY GENERATOR MODEL          : NULL
REMARK 200  MONOCHROMATIC OR LAUE    (M/L) : M
REMARK 200  WAVELENGTH OR RANGE        (A) : 0.9792
REMARK 200  MONOCHROMATOR                  : NULL
REMARK 200  OPTICS                         : NULL
REMARK 200
REMARK 200  DETECTOR TYPE                  : CCD
REMARK 200  DETECTOR MANUFACTURER          : MAR CCD 130 MM
REMARK 200  INTENSITY-INTEGRATION SOFTWARE : HKL-2000
REMARK 200  DATA SCALING SOFTWARE          : SCALA
REMARK 200
REMARK 200  NUMBER OF UNIQUE REFLECTIONS   : 14972
REMARK 200  RESOLUTION RANGE HIGH      (A) : 2.700
REMARK 200  RESOLUTION RANGE LOW       (A) : 50.000
REMARK 200  REJECTION CRITERIA  (SIGMA(I)) : NULL
REMARK 200
REMARK 200 OVERALL.
REMARK 200  COMPLETENESS FOR RANGE     (%) : 98.1
REMARK 200  DATA REDUNDANCY                : 10.00
REMARK 200  R MERGE                    (I) : 0.08600
REMARK 200  R SYM                      (I) : NULL
REMARK 200   FOR THE DATA SET  : 14.7000
REMARK 200
REMARK 200 IN THE HIGHEST RESOLUTION SHELL.
REMARK 200  HIGHEST RESOLUTION SHELL, RANGE HIGH (A) : NULL
REMARK 200  HIGHEST RESOLUTION SHELL, RANGE LOW  (A) : NULL
REMARK 200  COMPLETENESS FOR SHELL     (%) : 96.9
REMARK 200  DATA REDUNDANCY IN SHELL       : 10.30
REMARK 200  R MERGE FOR SHELL          (I) : NULL
REMARK 200  R SYM FOR SHELL            (I) : NULL
REMARK 200   FOR SHELL         : 3.100
REMARK 200
REMARK 200 DIFFRACTION PROTOCOL: SINGLE WAVELENGTH
REMARK 200 METHOD USED TO DETERMINE THE STRUCTURE: SAD
REMARK 200 SOFTWARE USED: PHENIX
REMARK 200 STARTING MODEL: NULL
REMARK 200
REMARK 200 REMARK: NULL
REMARK 280
REMARK 280 CRYSTAL
REMARK 280 SOLVENT CONTENT, VS   (%): 74.31
REMARK 280 MATTHEWS COEFFICIENT, VM (ANGSTROMS**3/DA): 4.79
REMARK 280
REMARK 280 CRYSTALLIZATION CONDITIONS: 0.1 M SODIUM ACETATE TRIHYDRATE PH
REMARK 280  4.6, 2.0 M SODIUM FORMATE, VAPOR DIFFUSION, HANGING DROP,
REMARK 280  TEMPERATURE 285K
REMARK 290
REMARK 290 CRYSTALLOGRAPHIC SYMMETRY
REMARK 290 SYMMETRY OPERATORS FOR SPACE GROUP: P 31 2 1
REMARK 290
REMARK 290      SYMOP   SYMMETRY
REMARK 290     NNNMMM   OPERATOR
REMARK 290       1555   X,Y,Z
REMARK 290       2555   -Y,X-Y,Z+1/3
REMARK 290       3555   -X+Y,-X,Z+2/3
REMARK 290       4555   Y,X,-Z
REMARK 290       5555   X-Y,-Y,-Z+2/3
REMARK 290       6555   -X,-X+Y,-Z+1/3
REMARK 290
REMARK 290     WHERE NNN -> OPERATOR NUMBER
REMARK 290           MMM -> TRANSLATION VECTOR
REMARK 290
REMARK 290 CRYSTALLOGRAPHIC SYMMETRY TRANSFORMATIONS
REMARK 290 THE FOLLOWING TRANSFORMATIONS OPERATE ON THE ATOM/HETATM
REMARK 290 RECORDS IN THIS ENTRY TO PRODUCE CRYSTALLOGRAPHICALLY
REMARK 290 RELATED MOLECULES.
REMARK 290   SMTRY1   1  1.000000  0.000000  0.000000        0.00000
REMARK 290   SMTRY2   1  0.000000  1.000000  0.000000        0.00000
REMARK 290   SMTRY3   1  0.000000  0.000000  1.000000        0.00000
REMARK 290   SMTRY1   2 -0.500000 -0.866025  0.000000        0.00000
REMARK 290   SMTRY2   2  0.866025 -0.500000  0.000000        0.00000
REMARK 290   SMTRY3   2  0.000000  0.000000  1.000000       28.98800
REMARK 290   SMTRY1   3 -0.500000  0.866025  0.000000        0.00000
REMARK 290   SMTRY2   3 -0.866025 -0.500000  0.000000        0.00000
REMARK 290   SMTRY3   3  0.000000  0.000000  1.000000       57.97600
REMARK 290   SMTRY1   4 -0.500000  0.866025  0.000000        0.00000
REMARK 290   SMTRY2   4  0.866025  0.500000  0.000000        0.00000
REMARK 290   SMTRY3   4  0.000000  0.000000 -1.000000        0.00000
REMARK 290   SMTRY1   5  1.000000  0.000000  0.000000        0.00000
REMARK 290   SMTRY2   5  0.000000 -1.000000  0.000000        0.00000
REMARK 290   SMTRY3   5  0.000000  0.000000 -1.000000       57.97600
REMARK 290   SMTRY1   6 -0.500000 -0.866025  0.000000        0.00000
REMARK 290   SMTRY2   6 -0.866025  0.500000  0.000000        0.00000
REMARK 290   SMTRY3   6  0.000000  0.000000 -1.000000       28.98800
REMARK 290
REMARK 290 REMARK: NULL
REMARK 300
REMARK 300 BIOMOLECULE: 1
REMARK 300 SEE REMARK 350 FOR THE AUTHOR PROVIDED AND/OR PROGRAM
REMARK 300 GENERATED ASSEMBLY INFORMATION FOR THE STRUCTURE IN
REMARK 300 THIS ENTRY. THE REMARK MAY ALSO PROVIDE INFORMATION ON
REMARK 300 BURIED SURFACE AREA.
REMARK 350
REMARK 350 COORDINATES FOR A COMPLETE MULTIMER REPRESENTING THE KNOWN
REMARK 350 BIOLOGICALLY SIGNIFICANT OLIGOMERIZATION STATE OF THE
REMARK 350 MOLECULE CAN BE GENERATED BY APPLYING BIOMT TRANSFORMATIONS
REMARK 350 GIVEN BELOW.  BOTH NON-CRYSTALLOGRAPHIC AND
REMARK 350 CRYSTALLOGRAPHIC OPERATIONS ARE GIVEN.
REMARK 350
REMARK 350 BIOMOLECULE: 1
REMARK 350 AUTHOR DETERMINED BIOLOGICAL UNIT: DIMERIC
REMARK 350 SOFTWARE DETERMINED QUATERNARY STRUCTURE: DIMERIC
REMARK 350 SOFTWARE USED: PISA
REMARK 350 TOTAL BURIED SURFACE AREA: 3390 ANGSTROM**2
REMARK 350 SURFACE AREA OF THE COMPLEX: 21400 ANGSTROM**2
REMARK 350 CHANGE IN SOLVENT FREE ENERGY: -27.0 KCAL/MOL
REMARK 350 APPLY THE FOLLOWING TO CHAINS: A
REMARK 350   BIOMT1   1  1.000000  0.000000  0.000000        0.00000
REMARK 350   BIOMT2   1  0.000000  1.000000  0.000000        0.00000
REMARK 350   BIOMT3   1  0.000000  0.000000  1.000000        0.00000
REMARK 350   BIOMT1   2  1.000000  0.000000  0.000000        0.00000
REMARK 350   BIOMT2   2  0.000000 -1.000000  0.000000        0.00000
REMARK 350   BIOMT3   2  0.000000  0.000000 -1.000000      -28.98800
REMARK 465
REMARK 465 MISSING RESIDUES
REMARK 465 THE FOLLOWING RESIDUES WERE NOT LOCATED IN THE
REMARK 465 EXPERIMENT. (M=MODEL NUMBER; RES=RESIDUE NAME; C=CHAIN
REMARK 465 IDENTIFIER; SSSEQ=SEQUENCE NUMBER; I=INSERTION CODE.)
REMARK 465
REMARK 465   M RES C SSSEQI
REMARK 465     HIS A   448
REMARK 465     HIS A   449
REMARK 465     GLU A   659
REMARK 465     ASN A   660
REMARK 465     GLU A   661
REMARK 465     SER A   662
REMARK 465     ARG A   663
REMARK 470
REMARK 470 MISSING ATOM
REMARK 470 THE FOLLOWING RESIDUES HAVE MISSING ATOMS (M=MODEL NUMBER;
REMARK 470 RES=RESIDUE NAME; C=CHAIN IDENTIFIER; SSEQ=SEQUENCE NUMBER;
REMARK 470 I=INSERTION CODE):
REMARK 470   M RES CSSEQI  ATOMS
REMARK 470     VAL A 476    CG1  CG2
REMARK 470     LEU A 480    CG   CD1  CD2
REMARK 470     ASP A 484    CG   OD1  OD2
REMARK 470     LEU A 485    CD1  CD2
REMARK 470     GLU A 498    CG   CD   OE1  OE2
REMARK 470     LYS A 515    CG   CD   CE   NZ
REMARK 470     ARG A 516    NH1  NH2
REMARK 470     LYS A 582    CG   CD   CE   NZ
REMARK 470     LYS A 589    CG   CD   CE   NZ
REMARK 470     LYS A 616    CG   CD   CE   NZ
REMARK 470     GLN A 626    CD   OE1  NE2
REMARK 470     GLN A 655    CG   CD   OE1  NE2
REMARK 470     LYS A 658    CG   CD   CE   NZ
REMARK 470     LYS A 664    CG   CD   CE   NZ
REMARK 470     ARG A 666    CG   CD   NE   CZ   NH1  NH2
REMARK 470     LYS A 667    CG   CD   CE   NZ
REMARK 500
REMARK 500 GEOMETRY AND STEREOCHEMISTRY
REMARK 500 SUBTOPIC: CLOSE CONTACTS IN SAME ASYMMETRIC UNIT
REMARK 500
REMARK 500 THE FOLLOWING ATOMS ARE IN CLOSE CONTACT.
REMARK 500
REMARK 500  ATM1  RES C  SSEQI   ATM2  RES C  SSEQI           DISTANCE
REMARK 500   CD2  TYR A   599     OD1  ASN A   620              1.74
REMARK 500
REMARK 500 REMARK: NULL
REMARK 500
REMARK 500 GEOMETRY AND STEREOCHEMISTRY
REMARK 500 SUBTOPIC: TORSION ANGLES
REMARK 500
REMARK 500 TORSION ANGLES OUTSIDE THE EXPECTED RAMACHANDRAN REGIONS:
REMARK 500 (M=MODEL NUMBER; RES=RESIDUE NAME; C=CHAIN IDENTIFIER;
REMARK 500 SSEQ=SEQUENCE NUMBER; I=INSERTION CODE).
REMARK 500
REMARK 500 STANDARD TABLE:
REMARK 500 FORMAT:(10X,I3,1X,A3,1X,A1,I4,A1,4X,F7.2,3X,F7.2)
REMARK 500
REMARK 500 EXPECTED VALUES: GJ KLEYWEGT AND TA JONES (1996). PHI/PSI-
REMARK 500 CHOLOGY: RAMACHANDRAN REVISITED. STRUCTURE 4, 1395 - 1400
REMARK 500
REMARK 500  M RES CSSEQI        PSI       PHI
REMARK 500    LEU A 480       53.58   -106.55
REMARK 500    GLU A 559      146.79   -175.42
REMARK 500    ILE A 581      -59.95     63.24
REMARK 500    LYS A 589      103.71     76.76
REMARK 500    THR A 611      -14.39   -151.14
REMARK 500    ARG A 671       83.11     76.03
REMARK 500    ASP A 697       26.70    -72.64
REMARK 500
REMARK 500 REMARK: NULL
DBREF  5J8J A  457   698  UNP    P53973   HDA1_YEAST     457    698
SEQADV 5J8J HIS A  448  UNP  P53973              EXPRESSION TAG
SEQADV 5J8J HIS A  449  UNP  P53973              EXPRESSION TAG
SEQADV 5J8J HIS A  450  UNP  P53973              EXPRESSION TAG
SEQADV 5J8J HIS A  451  UNP  P53973              EXPRESSION TAG
SEQADV 5J8J HIS A  452  UNP  P53973              EXPRESSION TAG
SEQADV 5J8J HIS A  453  UNP  P53973              EXPRESSION TAG
SEQADV 5J8J GLY A  454  UNP  P53973              EXPRESSION TAG
SEQADV 5J8J SER A  455  UNP  P53973              EXPRESSION TAG
SEQADV 5J8J MET A  456  UNP  P53973              EXPRESSION TAG
SEQRES   1 A  251  HIS HIS HIS HIS HIS HIS GLY SER MET LEU GLN LYS ALA
SEQRES   2 A  251  ILE ARG GLN GLN GLN GLN HIS TYR LEU SER ASP GLU PHE
SEQRES   3 A  251  ASN PHE VAL THR LEU PRO LEU VAL SER MET ASP LEU PRO
SEQRES   4 A  251  ASP ASN THR VAL LEU CYS THR PRO ASN ILE SER GLU SER
SEQRES   5 A  251  ASN THR ILE ILE ILE VAL VAL HIS ASP THR SER ASP ILE
SEQRES   6 A  251  TRP ALA LYS ARG ASN VAL ILE SER GLY THR ILE ASP LEU
SEQRES   7 A  251  SER SER SER VAL ILE ILE ASP ASN SER LEU ASP PHE ILE
SEQRES   8 A  251  LYS TRP GLY LEU ASP ARG LYS TYR GLY ILE ILE ASP VAL
SEQRES   9 A  251  ASN ILE PRO LEU THR LEU PHE GLU PRO ASP ASN TYR SER
SEQRES  10 A  251  GLY MET ILE THR SER GLN GLU VAL LEU ILE TYR LEU TRP
SEQRES  11 A  251  ASP ASN TYR ILE LYS TYR PHE PRO SER VAL ALA LYS ILE
SEQRES  12 A  251  ALA PHE ILE GLY ILE GLY ASP SER TYR SER GLY ILE VAL
SEQRES  13 A  251  HIS LEU LEU GLY HIS ARG ASP THR ARG ALA VAL THR LYS
SEQRES  14 A  251  THR VAL ILE ASN PHE LEU GLY ASP LYS GLN LEU LYS PRO
SEQRES  15 A  251  LEU VAL PRO LEU VAL ASP GLU THR LEU SER GLU TRP TYR
SEQRES  16 A  251  PHE LYS ASN SER LEU ILE PHE SER ASN ASN SER HIS GLN
SEQRES  17 A  251  CYS TRP LYS GLU ASN GLU SER ARG LYS PRO ARG LYS LYS
SEQRES  18 A  251  PHE GLY ARG VAL LEU ARG CYS ASP THR ASP GLY LEU ASN
SEQRES  19 A  251  ASN ILE ILE GLU GLU ARG PHE GLU GLU ALA THR ASP PHE
SEQRES  20 A  251  ILE LEU ASP SER
HELIX    1 AA1 HIS A  453  ASN A  474  1                                  22
HELIX    2 AA2 PRO A  486  ASN A  488  5                                   3
HELIX    3 AA3 ASN A  495  SER A  499  5                                   5
HELIX    4 AA4 ASP A  524  SER A  528  5                                   5
HELIX    5 AA5 SER A  534  ASP A  543  1                                  10
HELIX    6 AA6 ASN A  562  TYR A  580  1                                  19
HELIX    7 AA7 SER A  598  ARG A  609  1                                  12
HELIX    8 AA8 GLU A  636  ASN A  645  1                                  10
HELIX    9 AA9 ARG A  666  GLY A  670  5                                   5
HELIX   10 AB1 GLY A  679  ASP A  697  1                                  19
SHEET    1 AA1 8 VAL A 476  THR A 477  0
SHEET    2 AA1 8 VAL A 490  CYS A 492 -1  O  CYS A 492   N  VAL A 476
SHEET    3 AA1 8 GLY A 547  ILE A 553 -1  O  ASP A 550   N  LEU A 491
SHEET    4 AA1 8 ILE A 502  ASP A 508  1  N  ILE A 503   O  GLY A 547
SHEET    5 AA1 8 ILE A 590  ILE A 595  1  O  ILE A 593   N  VAL A 506
SHEET    6 AA1 8 THR A 615  GLY A 623  1  O  ILE A 619   N  GLY A 594
SHEET    7 AA1 8 SER A 646  SER A 650  1  O  LEU A 647   N  ASN A 620
SHEET    8 AA1 8 VAL A 672  ARG A 674  1  O  LEU A 673   N  ILE A 648
SHEET    1 AA2 2 ASP A 511  TRP A 513  0
SHEET    2 AA2 2 VAL A 529  ILE A 531 -1  O  VAL A 529   N  TRP A 513
LINK         CG  TYR A 599                 OD1 ASN A 620     1555   1555  1.50
CRYST1  104.974  104.974   86.964  90.00  90.00 120.00 P 31 2 1      6
ORIGX1      1.000000  0.000000  0.000000        0.00000
ORIGX2      0.000000  1.000000  0.000000        0.00000
ORIGX3      0.000000  0.000000  1.000000        0.00000
SCALE1      0.009526  0.005500  0.000000        0.00000
SCALE2      0.000000  0.011000  0.000000        0.00000
SCALE3      0.000000  0.000000  0.011499        0.00000
TER    1918      SER A 698
MASTER      294    0    0   10   10    0    0    6 1917    1    2   20
END