longtext: 5xpx-pdb

content
HEADER    HYDROLASE                               05-JUN-17   5XPX
TITLE     STRUCTURE ELUCIDATION OF TRUNCATED AMS3 LIPASE FROM AN ANTARCTIC
TITLE    2 PSEUDOMONAS
COMPND    MOL_ID: 1;
COMPND   2 MOLECULE: LIPASE;
COMPND   3 CHAIN: A, E;
COMPND   4 EC: 3.1.1.3;
COMPND   5 ENGINEERED: YES
SOURCE    MOL_ID: 1;
SOURCE   2 ORGANISM_SCIENTIFIC: PSEUDOMONAS SP. A3(2015C);
SOURCE   3 ORGANISM_TAXID: 1680634;
SOURCE   4 STRAIN: 2015C;
SOURCE   5 EXPRESSION_SYSTEM: ESCHERICHIA COLI 'BL21-GOLD(DE3)PLYSS AG';
SOURCE   6 EXPRESSION_SYSTEM_TAXID: 866768
KEYWDS    HYDROLASE
EXPDTA    X-RAY DIFFRACTION
AUTHOR    R.N.Z.R.A.RAHMAN,W.LATIP
REVDAT   1   20-JUN-18 5XPX    0
JRNL        AUTH   R.N.Z.R.A.RAHMAN,W.LATIP
JRNL        TITL   STRUCTURE ELUCIDATION OF TRUNCATED AMS3 LIPASE FROM AN
JRNL        TITL 2 ANTARCTIC PSEUDOMONAS
JRNL        REF    TO BE PUBLISHED
JRNL        REFN
REMARK   2
REMARK   2 RESOLUTION.    2.77 ANGSTROMS.
REMARK   3
REMARK   3 REFINEMENT.
REMARK   3   PROGRAM     : REFMAC 5.8.0158
REMARK   3   AUTHORS     : MURSHUDOV,SKUBAK,LEBEDEV,PANNU,STEINER,
REMARK   3               : NICHOLLS,WINN,LONG,VAGIN
REMARK   3
REMARK   3    REFINEMENT TARGET : NULL
REMARK   3
REMARK   3  DATA USED IN REFINEMENT.
REMARK   3   RESOLUTION RANGE HIGH (ANGSTROMS) : 2.77
REMARK   3   RESOLUTION RANGE LOW  (ANGSTROMS) : 40.00
REMARK   3   DATA CUTOFF            (SIGMA(F)) : NULL
REMARK   3   COMPLETENESS FOR RANGE        (%) : 99.0
REMARK   3   NUMBER OF REFLECTIONS             : 25583
REMARK   3
REMARK   3  FIT TO DATA USED IN REFINEMENT.
REMARK   3   CROSS-VALIDATION METHOD          : THROUGHOUT
REMARK   3   FREE R VALUE TEST SET SELECTION  : RANDOM
REMARK   3   R VALUE     (WORKING + TEST SET) : 0.225
REMARK   3   R VALUE            (WORKING SET) : 0.222
REMARK   3   FREE R VALUE                     : 0.277
REMARK   3   FREE R VALUE TEST SET SIZE   (%) : 5.200
REMARK   3   FREE R VALUE TEST SET COUNT      : 1391
REMARK   3
REMARK   3  FIT IN THE HIGHEST RESOLUTION BIN.
REMARK   3   TOTAL NUMBER OF BINS USED           : 20
REMARK   3   BIN RESOLUTION RANGE HIGH       (A) : 2.77
REMARK   3   BIN RESOLUTION RANGE LOW        (A) : 2.84
REMARK   3   REFLECTION IN BIN     (WORKING SET) : 1817
REMARK   3   BIN COMPLETENESS (WORKING+TEST) (%) : 96.41
REMARK   3   BIN R VALUE           (WORKING SET) : 0.3180
REMARK   3   BIN FREE R VALUE SET COUNT          : 92
REMARK   3   BIN FREE R VALUE                    : 0.3800
REMARK   3
REMARK   3  NUMBER OF NON-HYDROGEN ATOMS USED IN REFINEMENT.
REMARK   3   PROTEIN ATOMS            : 6042
REMARK   3   NUCLEIC ACID ATOMS       : 0
REMARK   3   HETEROGEN ATOMS          : 4
REMARK   3   SOLVENT ATOMS            : 20
REMARK   3
REMARK   3  B VALUES.
REMARK   3   FROM WILSON PLOT           (A**2) : NULL
REMARK   3   MEAN B VALUE      (OVERALL, A**2) : 27.18
REMARK   3   OVERALL ANISOTROPIC B VALUE.
REMARK   3    B11 (A**2) : 3.73000
REMARK   3    B22 (A**2) : -1.92000
REMARK   3    B33 (A**2) : -1.81000
REMARK   3    B12 (A**2) : 0.00000
REMARK   3    B13 (A**2) : 0.00000
REMARK   3    B23 (A**2) : 0.00000
REMARK   3
REMARK   3  ESTIMATED OVERALL COORDINATE ERROR.
REMARK   3   ESU BASED ON R VALUE                            (A): NULL
REMARK   3   ESU BASED ON FREE R VALUE                       (A): 0.381
REMARK   3   ESU BASED ON MAXIMUM LIKELIHOOD                 (A): 0.299
REMARK   3   ESU FOR B VALUES BASED ON MAXIMUM LIKELIHOOD (A**2): 15.282
REMARK   3
REMARK   3 CORRELATION COEFFICIENTS.
REMARK   3   CORRELATION COEFFICIENT FO-FC      : 0.909
REMARK   3   CORRELATION COEFFICIENT FO-FC FREE : 0.856
REMARK   3
REMARK   3  RMS DEVIATIONS FROM IDEAL VALUES        COUNT    RMS    WEIGHT
REMARK   3   BOND LENGTHS REFINED ATOMS        (A):  6208 ; 0.013 ; 0.019
REMARK   3   BOND LENGTHS OTHERS               (A):  5488 ; 0.002 ; 0.020
REMARK   3   BOND ANGLES REFINED ATOMS   (DEGREES):  8440 ; 1.689 ; 1.931
REMARK   3   BOND ANGLES OTHERS          (DEGREES): 12671 ; 1.098 ; 3.000
REMARK   3   TORSION ANGLES, PERIOD 1    (DEGREES):   763 ; 7.306 ; 5.000
REMARK   3   TORSION ANGLES, PERIOD 2    (DEGREES):   312 ;32.751 ;23.013
REMARK   3   TORSION ANGLES, PERIOD 3    (DEGREES):   942 ;19.322 ;15.000
REMARK   3   TORSION ANGLES, PERIOD 4    (DEGREES):    51 ;18.906 ;15.000
REMARK   3   CHIRAL-CENTER RESTRAINTS       (A**3):   883 ; 0.095 ; 0.200
REMARK   3   GENERAL PLANES REFINED ATOMS      (A):  7088 ; 0.006 ; 0.021
REMARK   3   GENERAL PLANES OTHERS             (A):  1415 ; 0.002 ; 0.020
REMARK   3   NON-BONDED CONTACTS REFINED ATOMS (A):  NULL ;  NULL ;  NULL
REMARK   3   NON-BONDED CONTACTS OTHERS        (A):  NULL ;  NULL ;  NULL
REMARK   3   NON-BONDED TORSION REFINED ATOMS  (A):  NULL ;  NULL ;  NULL
REMARK   3   NON-BONDED TORSION OTHERS         (A):  NULL ;  NULL ;  NULL
REMARK   3   H-BOND (X...Y) REFINED ATOMS      (A):  NULL ;  NULL ;  NULL
REMARK   3   H-BOND (X...Y) OTHERS             (A):  NULL ;  NULL ;  NULL
REMARK   3   POTENTIAL METAL-ION REFINED ATOMS (A):  NULL ;  NULL ;  NULL
REMARK   3   POTENTIAL METAL-ION OTHERS        (A):  NULL ;  NULL ;  NULL
REMARK   3   SYMMETRY VDW REFINED ATOMS        (A):  NULL ;  NULL ;  NULL
REMARK   3   SYMMETRY VDW OTHERS               (A):  NULL ;  NULL ;  NULL
REMARK   3   SYMMETRY H-BOND REFINED ATOMS     (A):  NULL ;  NULL ;  NULL
REMARK   3   SYMMETRY H-BOND OTHERS            (A):  NULL ;  NULL ;  NULL
REMARK   3   SYMMETRY METAL-ION REFINED ATOMS  (A):  NULL ;  NULL ;  NULL
REMARK   3   SYMMETRY METAL-ION OTHERS         (A):  NULL ;  NULL ;  NULL
REMARK   3
REMARK   3  ISOTROPIC THERMAL FACTOR RESTRAINTS.     COUNT   RMS    WEIGHT
REMARK   3   MAIN-CHAIN BOND REFINED ATOMS  (A**2):  3058 ; 1.671 ; 2.679
REMARK   3   MAIN-CHAIN BOND OTHER ATOMS    (A**2):  3057 ; 1.630 ; 2.677
REMARK   3   MAIN-CHAIN ANGLE REFINED ATOMS (A**2):  3819 ; 2.766 ; 4.011
REMARK   3   MAIN-CHAIN ANGLE OTHER ATOMS   (A**2):  3820 ; 2.767 ; 4.012
REMARK   3   SIDE-CHAIN BOND REFINED ATOMS  (A**2):  3150 ; 1.592 ; 2.830
REMARK   3   SIDE-CHAIN BOND OTHER ATOMS    (A**2):  3151 ; 1.592 ; 2.831
REMARK   3   SIDE-CHAIN ANGLE REFINED ATOMS (A**2):  NULL ;  NULL ;  NULL
REMARK   3   SIDE-CHAIN ANGLE OTHER ATOMS   (A**2):  4622 ; 2.704 ; 4.187
REMARK   3   LONG RANGE B REFINED ATOMS     (A**2):  7101 ; 4.510 ;30.835
REMARK   3   LONG RANGE B OTHER ATOMS       (A**2):  7102 ; 4.510 ;30.836
REMARK   3
REMARK   3 ANISOTROPIC THERMAL FACTOR RESTRAINTS.    COUNT   RMS   WEIGHT
REMARK   3   RIGID-BOND RESTRAINTS          (A**2):  NULL ;  NULL ;  NULL
REMARK   3   SPHERICITY; FREE ATOMS         (A**2):  NULL ;  NULL ;  NULL
REMARK   3   SPHERICITY; BONDED ATOMS       (A**2):  NULL ;  NULL ;  NULL
REMARK   3
REMARK   3  NCS RESTRAINTS STATISTICS
REMARK   3   NUMBER OF DIFFERENT NCS GROUPS : NULL
REMARK   3
REMARK   3  TLS DETAILS
REMARK   3   NUMBER OF TLS GROUPS  : NULL
REMARK   3
REMARK   3  BULK SOLVENT MODELLING.
REMARK   3   METHOD USED : NULL
REMARK   3   PARAMETERS FOR MASK CALCULATION
REMARK   3   VDW PROBE RADIUS   : 1.20
REMARK   3   ION PROBE RADIUS   : 0.80
REMARK   3   SHRINKAGE RADIUS   : 0.80
REMARK   3
REMARK   3  OTHER REFINEMENT REMARKS: HYDROGENS HAVE BEEN ADDED IN THE RIDING
REMARK   3  POSITIONS
REMARK   4
REMARK   4 5XPX COMPLIES WITH FORMAT V. 3.30, 13-JUL-11
REMARK 100
REMARK 100 THIS ENTRY HAS BEEN PROCESSED BY PDBJ ON 10-JUN-17.
REMARK 100 THE DEPOSITION ID IS D_1300003609.
REMARK 200
REMARK 200 EXPERIMENTAL DETAILS
REMARK 200  EXPERIMENT TYPE                : X-RAY DIFFRACTION
REMARK 200  DATE OF DATA COLLECTION        : 08-NOV-16
REMARK 200  TEMPERATURE           (KELVIN) : 100
REMARK 200  PH                             : 7.5
REMARK 200  NUMBER OF CRYSTALS USED        : 1
REMARK 200
REMARK 200  SYNCHROTRON              (Y/N) : N
REMARK 200  RADIATION SOURCE               : ROTATING ANODE
REMARK 200  BEAMLINE                       : NULL
REMARK 200  X-RAY GENERATOR MODEL          : RIGAKU MICROMAX-007
REMARK 200  MONOCHROMATIC OR LAUE    (M/L) : M
REMARK 200  WAVELENGTH OR RANGE        (A) : 1.54
REMARK 200  MONOCHROMATOR                  : NULL
REMARK 200  OPTICS                         : NULL
REMARK 200
REMARK 200  DETECTOR TYPE                  : CCD
REMARK 200  DETECTOR MANUFACTURER          : RIGAKU
REMARK 200  INTENSITY-INTEGRATION SOFTWARE : NULL
REMARK 200  DATA SCALING SOFTWARE          : HKL-3000
REMARK 200
REMARK 200  NUMBER OF UNIQUE REFLECTIONS   : 27263
REMARK 200  RESOLUTION RANGE HIGH      (A) : 2.770
REMARK 200  RESOLUTION RANGE LOW       (A) : 40.000
REMARK 200  REJECTION CRITERIA  (SIGMA(I)) : NULL
REMARK 200
REMARK 200 OVERALL.
REMARK 200  COMPLETENESS FOR RANGE     (%) : 99.7
REMARK 200  DATA REDUNDANCY                : 2.100
REMARK 200  R MERGE                    (I) : NULL
REMARK 200  R SYM                      (I) : NULL
REMARK 200   FOR THE DATA SET  : 9.4000
REMARK 200
REMARK 200 IN THE HIGHEST RESOLUTION SHELL.
REMARK 200  HIGHEST RESOLUTION SHELL, RANGE HIGH (A) : 2.77
REMARK 200  HIGHEST RESOLUTION SHELL, RANGE LOW  (A) : 2.82
REMARK 200  COMPLETENESS FOR SHELL     (%) : NULL
REMARK 200  DATA REDUNDANCY IN SHELL       : NULL
REMARK 200  R MERGE FOR SHELL          (I) : NULL
REMARK 200  R SYM FOR SHELL            (I) : NULL
REMARK 200   FOR SHELL         : NULL
REMARK 200
REMARK 200 DIFFRACTION PROTOCOL: SINGLE WAVELENGTH
REMARK 200 METHOD USED TO DETERMINE THE STRUCTURE: MOLECULAR REPLACEMENT
REMARK 200 SOFTWARE USED: REFMAC
REMARK 200 STARTING MODEL: 4FDM
REMARK 200
REMARK 200 REMARK: NULL
REMARK 280
REMARK 280 CRYSTAL
REMARK 280 SOLVENT CONTENT, VS   (%): 58.14
REMARK 280 MATTHEWS COEFFICIENT, VM (ANGSTROMS**3/DA): 2.94
REMARK 280
REMARK 280 CRYSTALLIZATION CONDITIONS: 0.1 M HEPES SODIUM PH 7.5, 0.8 M
REMARK 280  POTASSIUM SODIUM TARTRATE TETRAHYDRATE, VAPOR DIFFUSION, SITTING
REMARK 280  DROP, TEMPERATURE 293.15K
REMARK 290
REMARK 290 CRYSTALLOGRAPHIC SYMMETRY
REMARK 290 SYMMETRY OPERATORS FOR SPACE GROUP: P 21 21 21
REMARK 290
REMARK 290      SYMOP   SYMMETRY
REMARK 290     NNNMMM   OPERATOR
REMARK 290       1555   X,Y,Z
REMARK 290       2555   -X+1/2,-Y,Z+1/2
REMARK 290       3555   -X,Y+1/2,-Z+1/2
REMARK 290       4555   X+1/2,-Y+1/2,-Z
REMARK 290
REMARK 290     WHERE NNN -> OPERATOR NUMBER
REMARK 290           MMM -> TRANSLATION VECTOR
REMARK 290
REMARK 290 CRYSTALLOGRAPHIC SYMMETRY TRANSFORMATIONS
REMARK 290 THE FOLLOWING TRANSFORMATIONS OPERATE ON THE ATOM/HETATM
REMARK 290 RECORDS IN THIS ENTRY TO PRODUCE CRYSTALLOGRAPHICALLY
REMARK 290 RELATED MOLECULES.
REMARK 290   SMTRY1   1  1.000000  0.000000  0.000000        0.00000
REMARK 290   SMTRY2   1  0.000000  1.000000  0.000000        0.00000
REMARK 290   SMTRY3   1  0.000000  0.000000  1.000000        0.00000
REMARK 290   SMTRY1   2 -1.000000  0.000000  0.000000       43.37650
REMARK 290   SMTRY2   2  0.000000 -1.000000  0.000000        0.00000
REMARK 290   SMTRY3   2  0.000000  0.000000  1.000000       63.21550
REMARK 290   SMTRY1   3 -1.000000  0.000000  0.000000        0.00000
REMARK 290   SMTRY2   3  0.000000  1.000000  0.000000       47.34650
REMARK 290   SMTRY3   3  0.000000  0.000000 -1.000000       63.21550
REMARK 290   SMTRY1   4  1.000000  0.000000  0.000000       43.37650
REMARK 290   SMTRY2   4  0.000000 -1.000000  0.000000       47.34650
REMARK 290   SMTRY3   4  0.000000  0.000000 -1.000000        0.00000
REMARK 290
REMARK 290 REMARK: NULL
REMARK 300
REMARK 300 BIOMOLECULE: 1
REMARK 300 SEE REMARK 350 FOR THE AUTHOR PROVIDED AND/OR PROGRAM
REMARK 300 GENERATED ASSEMBLY INFORMATION FOR THE STRUCTURE IN
REMARK 300 THIS ENTRY. THE REMARK MAY ALSO PROVIDE INFORMATION ON
REMARK 300 BURIED SURFACE AREA.
REMARK 350
REMARK 350 COORDINATES FOR A COMPLETE MULTIMER REPRESENTING THE KNOWN
REMARK 350 BIOLOGICALLY SIGNIFICANT OLIGOMERIZATION STATE OF THE
REMARK 350 MOLECULE CAN BE GENERATED BY APPLYING BIOMT TRANSFORMATIONS
REMARK 350 GIVEN BELOW.  BOTH NON-CRYSTALLOGRAPHIC AND
REMARK 350 CRYSTALLOGRAPHIC OPERATIONS ARE GIVEN.
REMARK 350
REMARK 350 BIOMOLECULE: 1
REMARK 350 AUTHOR DETERMINED BIOLOGICAL UNIT: DIMERIC
REMARK 350 APPLY THE FOLLOWING TO CHAINS: A, E
REMARK 350   BIOMT1   1  1.000000  0.000000  0.000000        0.00000
REMARK 350   BIOMT2   1  0.000000  1.000000  0.000000        0.00000
REMARK 350   BIOMT3   1  0.000000  0.000000  1.000000        0.00000
REMARK 465
REMARK 465 MISSING RESIDUES
REMARK 465 THE FOLLOWING RESIDUES WERE NOT LOCATED IN THE
REMARK 465 EXPERIMENT. (M=MODEL NUMBER; RES=RESIDUE NAME; C=CHAIN
REMARK 465 IDENTIFIER; SSSEQ=SEQUENCE NUMBER; I=INSERTION CODE.)
REMARK 465
REMARK 465   M RES C SSSEQI
REMARK 465     MET A   -22
REMARK 465     ALA A   -21
REMARK 465     SER A   -20
REMARK 465     TRP A   -19
REMARK 465     SER A   -18
REMARK 465     HIS A   -17
REMARK 465     PRO A   -16
REMARK 465     GLN A   -15
REMARK 465     PHE A   -14
REMARK 465     GLU A   -13
REMARK 465     LYS A   -12
REMARK 465     GLY A   -11
REMARK 465     ALA A   -10
REMARK 465     ASP A    -9
REMARK 465     ASP A    -8
REMARK 465     ASP A    -7
REMARK 465     ASP A    -6
REMARK 465     LYS A    -5
REMARK 465     VAL A    -4
REMARK 465     PRO A    -3
REMARK 465     ARG A    -2
REMARK 465     GLY A    -1
REMARK 465     SER A     0
REMARK 465     ALA A     1
REMARK 465     SER A     2
REMARK 465     LEU A     3
REMARK 465     PRO A   388
REMARK 465     PRO A   389
REMARK 465     GLY A   390
REMARK 465     PHE A   391
REMARK 465     SER A   392
REMARK 465     SER A   393
REMARK 465     ILE A   394
REMARK 465     SER A   395
REMARK 465     ALA A   396
REMARK 465     HIS A   397
REMARK 465     HIS A   398
REMARK 465     HIS A   399
REMARK 465     HIS A   400
REMARK 465     HIS A   401
REMARK 465     HIS A   402
REMARK 465     HIS A   403
REMARK 465     HIS A   404
REMARK 465     HIS A   405
REMARK 465     HIS A   406
REMARK 465     MET E   -22
REMARK 465     ALA E   -21
REMARK 465     SER E   -20
REMARK 465     TRP E   -19
REMARK 465     SER E   -18
REMARK 465     HIS E   -17
REMARK 465     PRO E   -16
REMARK 465     GLN E   -15
REMARK 465     PHE E   -14
REMARK 465     GLU E   -13
REMARK 465     LYS E   -12
REMARK 465     GLY E   -11
REMARK 465     ALA E   -10
REMARK 465     ASP E    -9
REMARK 465     ASP E    -8
REMARK 465     ASP E    -7
REMARK 465     ASP E    -6
REMARK 465     LYS E    -5
REMARK 465     VAL E    -4
REMARK 465     PRO E    -3
REMARK 465     ARG E    -2
REMARK 465     GLY E    -1
REMARK 465     SER E     0
REMARK 465     ALA E     1
REMARK 465     SER E     2
REMARK 465     LEU E     3
REMARK 465     ARG E     4
REMARK 465     ALA E     5
REMARK 465     ASN E     6
REMARK 465     PRO E   388
REMARK 465     PRO E   389
REMARK 465     GLY E   390
REMARK 465     PHE E   391
REMARK 465     SER E   392
REMARK 465     SER E   393
REMARK 465     ILE E   394
REMARK 465     SER E   395
REMARK 465     ALA E   396
REMARK 465     HIS E   397
REMARK 465     HIS E   398
REMARK 465     HIS E   399
REMARK 465     HIS E   400
REMARK 465     HIS E   401
REMARK 465     HIS E   402
REMARK 465     HIS E   403
REMARK 465     HIS E   404
REMARK 465     HIS E   405
REMARK 465     HIS E   406
REMARK 500
REMARK 500 GEOMETRY AND STEREOCHEMISTRY
REMARK 500 SUBTOPIC: CLOSE CONTACTS IN SAME ASYMMETRIC UNIT
REMARK 500
REMARK 500 THE FOLLOWING ATOMS ARE IN CLOSE CONTACT.
REMARK 500
REMARK 500  ATM1  RES C  SSEQI   ATM2  RES C  SSEQI           DISTANCE
REMARK 500   O    ILE E   107     O    VAL E   155              2.06
REMARK 500
REMARK 500 REMARK: NULL
REMARK 500
REMARK 500 GEOMETRY AND STEREOCHEMISTRY
REMARK 500 SUBTOPIC: COVALENT BOND ANGLES
REMARK 500
REMARK 500 THE STEREOCHEMICAL PARAMETERS OF THE FOLLOWING RESIDUES
REMARK 500 HAVE VALUES WHICH DEVIATE FROM EXPECTED VALUES BY MORE
REMARK 500 THAN 6*RMSD (M=MODEL NUMBER; RES=RESIDUE NAME; C=CHAIN
REMARK 500 IDENTIFIER; SSEQ=SEQUENCE NUMBER; I=INSERTION CODE).
REMARK 500
REMARK 500 STANDARD TABLE:
REMARK 500 FORMAT: (10X,I3,1X,A3,1X,A1,I4,A1,3(1X,A4,2X),12X,F5.1)
REMARK 500
REMARK 500 EXPECTED VALUES PROTEIN: ENGH AND HUBER, 1999
REMARK 500 EXPECTED VALUES NUCLEIC ACID: CLOWNEY ET AL 1996
REMARK 500
REMARK 500  M RES CSSEQI ATM1   ATM2   ATM3
REMARK 500    ARG A 274   NE  -  CZ  -  NH1 ANGL. DEV. =   3.1 DEGREES
REMARK 500    LEU A 386   CA  -  CB  -  CG  ANGL. DEV. =  14.7 DEGREES
REMARK 500
REMARK 500 REMARK: NULL
REMARK 500
REMARK 500 GEOMETRY AND STEREOCHEMISTRY
REMARK 500 SUBTOPIC: TORSION ANGLES
REMARK 500
REMARK 500 TORSION ANGLES OUTSIDE THE EXPECTED RAMACHANDRAN REGIONS:
REMARK 500 (M=MODEL NUMBER; RES=RESIDUE NAME; C=CHAIN IDENTIFIER;
REMARK 500 SSEQ=SEQUENCE NUMBER; I=INSERTION CODE).
REMARK 500
REMARK 500 STANDARD TABLE:
REMARK 500 FORMAT:(10X,I3,1X,A3,1X,A1,I4,A1,4X,F7.2,3X,F7.2)
REMARK 500
REMARK 500 EXPECTED VALUES: GJ KLEYWEGT AND TA JONES (1996). PHI/PSI-
REMARK 500 CHOLOGY: RAMACHANDRAN REVISITED. STRUCTURE 4, 1395 - 1400
REMARK 500
REMARK 500  M RES CSSEQI        PSI       PHI
REMARK 500    ALA A   5       19.58   -172.60
REMARK 500    ALA A  52       89.25   -151.50
REMARK 500    SER A 113     -131.33     54.54
REMARK 500    ASP A 175       30.20    -95.49
REMARK 500    VAL A 203      -66.12     74.42
REMARK 500    LEU A 208       39.81    -97.02
REMARK 500    ARG A 271       45.13   -151.98
REMARK 500    ASP A 310     -157.36   -118.92
REMARK 500    ILE A 319      -48.07   -139.35
REMARK 500    ASN A 326      -54.74    -21.42
REMARK 500    LYS A 329      -63.81   -130.03
REMARK 500    ASN A 367       86.91   -156.70
REMARK 500    ALA E   8      121.21     72.47
REMARK 500    GLU E 100      -15.29    -44.30
REMARK 500    SER E 113     -130.41     59.34
REMARK 500    ASN E 141       70.87     52.97
REMARK 500    HIS E 153       59.34   -149.17
REMARK 500    VAL E 155      -73.63    -67.13
REMARK 500    LEU E 156      -62.75     97.57
REMARK 500    ASP E 175       38.52    -99.88
REMARK 500    SER E 201      153.47    -46.32
REMARK 500    VAL E 203      -66.97     68.79
REMARK 500    ASP E 238       50.52    -97.05
REMARK 500    ARG E 271       37.45   -158.70
REMARK 500    ASN E 304       99.81   -171.37
REMARK 500    ILE E 319      -55.71   -132.09
REMARK 500    LYS E 329      -55.44   -140.22
REMARK 500    ASP E 357      165.49    -46.52
REMARK 500    ASN E 367       80.68   -173.35
REMARK 500    SER E 385       45.06    -72.54
REMARK 500    LEU E 386      -48.30   -175.10
REMARK 500
REMARK 500 REMARK: NULL
REMARK 500
REMARK 500 GEOMETRY AND STEREOCHEMISTRY
REMARK 500 SUBTOPIC: NON-CIS, NON-TRANS
REMARK 500
REMARK 500 THE FOLLOWING PEPTIDE BONDS DEVIATE SIGNIFICANTLY FROM BOTH
REMARK 500 CIS AND TRANS CONFORMATION.  CIS BONDS, IF ANY, ARE LISTED
REMARK 500 ON CISPEP RECORDS.  TRANS IS DEFINED AS 180 +/- 30 AND
REMARK 500 CIS IS DEFINED AS 0 +/- 30 DEGREES.
REMARK 500                                 MODEL     OMEGA
REMARK 500 SER A  385     LEU A  386                 -149.21
REMARK 500
REMARK 500 REMARK: NULL
REMARK 620
REMARK 620 METAL COORDINATION
REMARK 620 (M=MODEL NUMBER; RES=RESIDUE NAME; C=CHAIN IDENTIFIER;
REMARK 620 SSEQ=SEQUENCE NUMBER; I=INSERTION CODE):
REMARK 620
REMARK 620 COORDINATION ANGLES FOR:  M RES CSSEQI METAL
REMARK 620                              ZN A 501  ZN
REMARK 620 N RES CSSEQI ATOM
REMARK 620 1 ASP A  61   OD1
REMARK 620 2 HIS A  87   NE2 119.1
REMARK 620 3 ASP A 238   OD2 127.7  92.1
REMARK 620 N                    1     2
REMARK 620
REMARK 620 COORDINATION ANGLES FOR:  M RES CSSEQI METAL
REMARK 620                              CA A 502  CA
REMARK 620 N RES CSSEQI ATOM
REMARK 620 1 GLY A 286   O
REMARK 620 2 GLU A 360   OE2  72.6
REMARK 620 3 ASP A 365   OD2 108.2 115.2
REMARK 620 4 PRO A 366   O   150.9  82.7  96.1
REMARK 620 N                    1     2     3
REMARK 620
REMARK 620 COORDINATION ANGLES FOR:  M RES CSSEQI METAL
REMARK 620                              ZN E 501  ZN
REMARK 620 N RES CSSEQI ATOM
REMARK 620 1 ASP E  61   OD1
REMARK 620 2 HIS E  81   NE2  98.8
REMARK 620 3 HIS E  87   NE2 124.5 107.7
REMARK 620 4 ASP E 238   OD2 116.2 105.8 102.3
REMARK 620 N                    1     2     3
REMARK 620
REMARK 620 COORDINATION ANGLES FOR:  M RES CSSEQI METAL
REMARK 620                              CA E 502  CA
REMARK 620 N RES CSSEQI ATOM
REMARK 620 1 GLY E 286   O
REMARK 620 2 GLU E 360   OE2  73.4
REMARK 620 3 ASP E 365   OD2  98.1  93.9
REMARK 620 4 PRO E 366   O   142.6  69.2  85.3
REMARK 620 N                    1     2     3
REMARK 800
REMARK 800 SITE
REMARK 800 SITE_IDENTIFIER: AC1
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: binding site for residue ZN A 501
REMARK 800
REMARK 800 SITE_IDENTIFIER: AC2
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: binding site for residue CA A 502
REMARK 800
REMARK 800 SITE_IDENTIFIER: AC3
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: binding site for residue ZN E 501
REMARK 800
REMARK 800 SITE_IDENTIFIER: AC4
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: binding site for residue CA E 502
DBREF1 5XPX A    1   388  UNP                  A0A0K0PTR1_9PSED
DBREF2 5XPX A     A0A0K0PTR1                          1         388
DBREF1 5XPX E    1   388  UNP                  A0A0K0PTR1_9PSED
DBREF2 5XPX E     A0A0K0PTR1                          1         388
SEQADV 5XPX MET A  -22  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX ALA A  -21  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX SER A  -20  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX TRP A  -19  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX SER A  -18  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX HIS A  -17  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX PRO A  -16  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX GLN A  -15  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX PHE A  -14  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX GLU A  -13  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX LYS A  -12  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX GLY A  -11  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX ALA A  -10  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX ASP A   -9  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX ASP A   -8  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX ASP A   -7  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX ASP A   -6  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX LYS A   -5  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX VAL A   -4  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX PRO A   -3  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX ARG A   -2  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX GLY A   -1  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX SER A    0  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX PRO A  389  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX GLY A  390  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX PHE A  391  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX SER A  392  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX SER A  393  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX ILE A  394  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX SER A  395  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX ALA A  396  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX HIS A  397  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX HIS A  398  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX HIS A  399  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX HIS A  400  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX HIS A  401  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX HIS A  402  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX HIS A  403  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX HIS A  404  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX HIS A  405  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX HIS A  406  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX MET E  -22  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX ALA E  -21  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX SER E  -20  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX TRP E  -19  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX SER E  -18  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX HIS E  -17  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX PRO E  -16  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX GLN E  -15  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX PHE E  -14  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX GLU E  -13  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX LYS E  -12  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX GLY E  -11  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX ALA E  -10  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX ASP E   -9  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX ASP E   -8  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX ASP E   -7  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX ASP E   -6  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX LYS E   -5  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX VAL E   -4  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX PRO E   -3  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX ARG E   -2  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX GLY E   -1  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX SER E    0  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX PRO E  389  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX GLY E  390  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX PHE E  391  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX SER E  392  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX SER E  393  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX ILE E  394  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX SER E  395  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX ALA E  396  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX HIS E  397  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX HIS E  398  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX HIS E  399  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX HIS E  400  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX HIS E  401  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX HIS E  402  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX HIS E  403  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX HIS E  404  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX HIS E  405  UNP  A0A0K0PTR           EXPRESSION TAG
SEQADV 5XPX HIS E  406  UNP  A0A0K0PTR           EXPRESSION TAG
SEQRES   1 A  429  MET ALA SER TRP SER HIS PRO GLN PHE GLU LYS GLY ALA
SEQRES   2 A  429  ASP ASP ASP ASP LYS VAL PRO ARG GLY SER ALA SER LEU
SEQRES   3 A  429  ARG ALA ASN ASP ALA PRO ILE VAL LEU LEU HIS GLY PHE
SEQRES   4 A  429  THR GLY TRP GLY ARG GLU GLU MET PHE GLY PHE LYS TYR
SEQRES   5 A  429  TRP GLY GLY VAL ARG GLY ASP ILE GLU GLN TRP LEU ASN
SEQRES   6 A  429  ASP ASN GLY TYR ARG THR TYR THR LEU ALA VAL GLY PRO
SEQRES   7 A  429  LEU SER SER ASN TRP ASP ARG ALA CYS GLU ALA TYR ALA
SEQRES   8 A  429  GLN LEU VAL GLY GLY THR VAL ASP TYR GLY ALA ALA HIS
SEQRES   9 A  429  ALA ALA LYS HIS GLY HIS ALA ARG PHE GLY ARG THR TYR
SEQRES  10 A  429  PRO GLY LEU LEU PRO GLU LEU LYS ARG GLY GLY ARG ILE
SEQRES  11 A  429  HIS ILE ILE ALA HIS SER GLN GLY GLY GLN THR ALA ARG
SEQRES  12 A  429  MET LEU VAL SER LEU LEU GLU ASN GLY SER GLN GLU GLU
SEQRES  13 A  429  ARG GLU TYR ALA LYS ALA HIS ASN VAL SER LEU SER PRO
SEQRES  14 A  429  LEU PHE GLU GLY GLY HIS HIS PHE VAL LEU SER VAL THR
SEQRES  15 A  429  THR ILE ALA THR PRO HIS ASP GLY THR THR LEU VAL ASN
SEQRES  16 A  429  MET VAL ASP PHE THR ASP ARG PHE PHE ASP LEU GLN LYS
SEQRES  17 A  429  ALA VAL LEU GLU ALA ALA ALA VAL ALA SER ASN VAL PRO
SEQRES  18 A  429  TYR THR SER GLN VAL TYR ASP PHE LYS LEU ASP GLN TRP
SEQRES  19 A  429  GLY LEU ARG ARG GLN PRO GLY GLU SER PHE ASP HIS TYR
SEQRES  20 A  429  PHE GLU ARG LEU LYS ARG SER PRO VAL TRP THR SER THR
SEQRES  21 A  429  ASP THR ALA ARG TYR ASP LEU SER VAL SER GLY ALA GLU
SEQRES  22 A  429  LYS LEU ASN GLN TRP VAL GLN ALA SER PRO ASN THR TYR
SEQRES  23 A  429  TYR LEU SER PHE SER THR GLU ARG THR TYR ARG GLY ALA
SEQRES  24 A  429  LEU THR GLY ASN HIS TYR PRO GLU LEU GLY MET ASN ALA
SEQRES  25 A  429  PHE SER ALA VAL VAL CYS ALA PRO PHE LEU GLY SER TYR
SEQRES  26 A  429  ARG ASN PRO THR LEU GLY ILE ASP ASP ARG TRP LEU GLU
SEQRES  27 A  429  ASN ASP GLY ILE VAL ASN THR VAL SER MET ASN GLY PRO
SEQRES  28 A  429  LYS ARG GLY SER SER ASP ARG ILE VAL PRO TYR ASP GLY
SEQRES  29 A  429  THR LEU LYS LYS GLY VAL TRP ASN ASP MET GLY THR TYR
SEQRES  30 A  429  ASN VAL ASP HIS LEU GLU ILE ILE GLY VAL ASP PRO ASN
SEQRES  31 A  429  PRO SER PHE ASP ILE ARG ALA PHE TYR LEU ARG LEU ALA
SEQRES  32 A  429  GLU GLN LEU ALA SER LEU ARG PRO PRO GLY PHE SER SER
SEQRES  33 A  429  ILE SER ALA HIS HIS HIS HIS HIS HIS HIS HIS HIS HIS
SEQRES   1 E  429  MET ALA SER TRP SER HIS PRO GLN PHE GLU LYS GLY ALA
SEQRES   2 E  429  ASP ASP ASP ASP LYS VAL PRO ARG GLY SER ALA SER LEU
SEQRES   3 E  429  ARG ALA ASN ASP ALA PRO ILE VAL LEU LEU HIS GLY PHE
SEQRES   4 E  429  THR GLY TRP GLY ARG GLU GLU MET PHE GLY PHE LYS TYR
SEQRES   5 E  429  TRP GLY GLY VAL ARG GLY ASP ILE GLU GLN TRP LEU ASN
SEQRES   6 E  429  ASP ASN GLY TYR ARG THR TYR THR LEU ALA VAL GLY PRO
SEQRES   7 E  429  LEU SER SER ASN TRP ASP ARG ALA CYS GLU ALA TYR ALA
SEQRES   8 E  429  GLN LEU VAL GLY GLY THR VAL ASP TYR GLY ALA ALA HIS
SEQRES   9 E  429  ALA ALA LYS HIS GLY HIS ALA ARG PHE GLY ARG THR TYR
SEQRES  10 E  429  PRO GLY LEU LEU PRO GLU LEU LYS ARG GLY GLY ARG ILE
SEQRES  11 E  429  HIS ILE ILE ALA HIS SER GLN GLY GLY GLN THR ALA ARG
SEQRES  12 E  429  MET LEU VAL SER LEU LEU GLU ASN GLY SER GLN GLU GLU
SEQRES  13 E  429  ARG GLU TYR ALA LYS ALA HIS ASN VAL SER LEU SER PRO
SEQRES  14 E  429  LEU PHE GLU GLY GLY HIS HIS PHE VAL LEU SER VAL THR
SEQRES  15 E  429  THR ILE ALA THR PRO HIS ASP GLY THR THR LEU VAL ASN
SEQRES  16 E  429  MET VAL ASP PHE THR ASP ARG PHE PHE ASP LEU GLN LYS
SEQRES  17 E  429  ALA VAL LEU GLU ALA ALA ALA VAL ALA SER ASN VAL PRO
SEQRES  18 E  429  TYR THR SER GLN VAL TYR ASP PHE LYS LEU ASP GLN TRP
SEQRES  19 E  429  GLY LEU ARG ARG GLN PRO GLY GLU SER PHE ASP HIS TYR
SEQRES  20 E  429  PHE GLU ARG LEU LYS ARG SER PRO VAL TRP THR SER THR
SEQRES  21 E  429  ASP THR ALA ARG TYR ASP LEU SER VAL SER GLY ALA GLU
SEQRES  22 E  429  LYS LEU ASN GLN TRP VAL GLN ALA SER PRO ASN THR TYR
SEQRES  23 E  429  TYR LEU SER PHE SER THR GLU ARG THR TYR ARG GLY ALA
SEQRES  24 E  429  LEU THR GLY ASN HIS TYR PRO GLU LEU GLY MET ASN ALA
SEQRES  25 E  429  PHE SER ALA VAL VAL CYS ALA PRO PHE LEU GLY SER TYR
SEQRES  26 E  429  ARG ASN PRO THR LEU GLY ILE ASP ASP ARG TRP LEU GLU
SEQRES  27 E  429  ASN ASP GLY ILE VAL ASN THR VAL SER MET ASN GLY PRO
SEQRES  28 E  429  LYS ARG GLY SER SER ASP ARG ILE VAL PRO TYR ASP GLY
SEQRES  29 E  429  THR LEU LYS LYS GLY VAL TRP ASN ASP MET GLY THR TYR
SEQRES  30 E  429  ASN VAL ASP HIS LEU GLU ILE ILE GLY VAL ASP PRO ASN
SEQRES  31 E  429  PRO SER PHE ASP ILE ARG ALA PHE TYR LEU ARG LEU ALA
SEQRES  32 E  429  GLU GLN LEU ALA SER LEU ARG PRO PRO GLY PHE SER SER
SEQRES  33 E  429  ILE SER ALA HIS HIS HIS HIS HIS HIS HIS HIS HIS HIS
HET     ZN  A 501       1
HET     CA  A 502       1
HET     ZN  E 501       1
HET     CA  E 502       1
HETNAM      ZN ZINC ION
HETNAM      CA CALCIUM ION
FORMUL   3   ZN    2(ZN 2+)
FORMUL   4   CA    2(CA 2+)
FORMUL   7  HOH   *20(H2 O)
HELIX    1 AA1 GLU A   23  PHE A   27  5                                   5
HELIX    2 AA2 GLY A   31  GLY A   35  5                                   5
HELIX    3 AA3 ASP A   36  ASN A   44  1                                   9
HELIX    4 AA4 SER A   58  GLY A   72  1                                  15
HELIX    5 AA5 GLY A   78  GLY A   86  1                                   9
HELIX    6 AA6 LEU A   98  LYS A  102  5                                   5
HELIX    7 AA7 GLN A  114  GLY A  129  1                                  16
HELIX    8 AA8 SER A  130  ASN A  141  1                                  12
HELIX    9 AA9 SER A  145  GLU A  149  5                                   5
HELIX   10 AB1 THR A  168  MET A  173  5                                   6
HELIX   11 AB2 ASP A  175  ALA A  191  1                                  17
HELIX   12 AB3 SER A  220  ARG A  230  1                                  11
HELIX   13 AB4 SER A  231  SER A  236  1                                   6
HELIX   14 AB5 THR A  239  SER A  245  1                                   7
HELIX   15 AB6 SER A  245  VAL A  256  1                                  12
HELIX   16 AB7 ASN A  288  CYS A  295  1                                   8
HELIX   17 AB8 CYS A  295  GLY A  300  1                                   6
HELIX   18 AB9 ASN A  304  GLY A  308  5                                   5
HELIX   19 AC1 ASP A  310  LEU A  314  5                                   5
HELIX   20 AC2 ASN A  321  ASN A  326  5                                   6
HELIX   21 AC3 ASP A  371  ALA A  384  1                                  14
HELIX   22 AC4 GLU E   23  PHE E   27  5                                   5
HELIX   23 AC5 GLY E   31  GLY E   35  5                                   5
HELIX   24 AC6 ASP E   36  ASN E   44  1                                   9
HELIX   25 AC7 SER E   58  GLY E   72  1                                  15
HELIX   26 AC8 GLY E   78  GLY E   86  1                                   9
HELIX   27 AC9 LEU E   98  LYS E  102  5                                   5
HELIX   28 AD1 GLN E  114  GLY E  129  1                                  16
HELIX   29 AD2 SER E  130  ASN E  141  1                                  12
HELIX   30 AD3 SER E  145  GLU E  149  5                                   5
HELIX   31 AD4 THR E  168  MET E  173  5                                   6
HELIX   32 AD5 ASP E  175  ALA E  191  1                                  17
HELIX   33 AD6 LEU E  208  GLY E  212  5                                   5
HELIX   34 AD7 SER E  220  ARG E  230  1                                  11
HELIX   35 AD8 SER E  231  SER E  236  1                                   6
HELIX   36 AD9 THR E  239  SER E  245  1                                   7
HELIX   37 AE1 SER E  245  GLN E  254  1                                  10
HELIX   38 AE2 ASN E  288  CYS E  295  1                                   8
HELIX   39 AE3 CYS E  295  GLY E  300  1                                   6
HELIX   40 AE4 ASP E  310  LEU E  314  5                                   5
HELIX   41 AE5 ASN E  321  ASN E  326  5                                   6
HELIX   42 AE6 ASP E  371  SER E  385  1                                  15
SHEET    1 AA1 7 THR A  48  LEU A  51  0
SHEET    2 AA1 7 ILE A  10  LEU A  13  1  N  LEU A  12   O  LEU A  51
SHEET    3 AA1 7 ILE A 107  HIS A 112  1  O  HIS A 108   N  VAL A  11
SHEET    4 AA1 7 VAL A 155  ILE A 161  1  O  SER A 157   N  ILE A 109
SHEET    5 AA1 7 TYR A 263  THR A 269  1  O  LEU A 265   N  THR A 160
SHEET    6 AA1 7 TRP A 348  TYR A 354  1  O  GLY A 352   N  SER A 268
SHEET    7 AA1 7 ILE A 336  PRO A 338  1  N  VAL A 337   O  TRP A 348
SHEET    1 AA2 2 GLY A  73  ASP A  76  0
SHEET    2 AA2 2 PHE A  90  TYR A  94 -1  O  GLY A  91   N  VAL A  75
SHEET    1 AA3 2 THR A 272  ARG A 274  0
SHEET    2 AA3 2 HIS A 281  PRO A 283 -1  O  TYR A 282   N  TYR A 273
SHEET    1 AA4 7 THR E  48  THR E  50  0
SHEET    2 AA4 7 ILE E  10  LEU E  13  1  N  ILE E  10   O  TYR E  49
SHEET    3 AA4 7 ILE E 107  HIS E 112  1  O  HIS E 108   N  VAL E  11
SHEET    4 AA4 7 LEU E 156  ILE E 161  1  O  THR E 159   N  ALA E 111
SHEET    5 AA4 7 TYR E 263  GLU E 270  1  O  PHE E 267   N  THR E 160
SHEET    6 AA4 7 TRP E 348  ASN E 355  1  O  ASN E 349   N  SER E 266
SHEET    7 AA4 7 ILE E 336  PRO E 338  1  N  VAL E 337   O  ASP E 350
SHEET    1 AA5 2 GLY E  73  ASP E  76  0
SHEET    2 AA5 2 PHE E  90  TYR E  94 -1  O  TYR E  94   N  GLY E  73
SHEET    1 AA6 2 THR E 272  ARG E 274  0
SHEET    2 AA6 2 HIS E 281  PRO E 283 -1  O  TYR E 282   N  TYR E 273
LINK         OD1 ASP A  61                ZN    ZN A 501     1555   1555  1.97
LINK         NE2 HIS A  87                ZN    ZN A 501     1555   1555  2.24
LINK         OD2 ASP A 238                ZN    ZN A 501     1555   1555  1.92
LINK         O   GLY A 286                CA    CA A 502     1555   1555  2.44
LINK         OE2 GLU A 360                CA    CA A 502     1555   1555  2.73
LINK         OD2 ASP A 365                CA    CA A 502     1555   1555  2.58
LINK         O   PRO A 366                CA    CA A 502     1555   1555  2.39
LINK         OD1 ASP E  61                ZN    ZN E 501     1555   1555  2.03
LINK         NE2 HIS E  81                ZN    ZN E 501     1555   1555  2.09
LINK         NE2 HIS E  87                ZN    ZN E 501     1555   1555  2.25
LINK         OD2 ASP E 238                ZN    ZN E 501     1555   1555  1.78
LINK         O   GLY E 286                CA    CA E 502     1555   1555  2.47
LINK         OE2 GLU E 360                CA    CA E 502     1555   1555  2.75
LINK         OD2 ASP E 365                CA    CA E 502     1555   1555  2.76
LINK         O   PRO E 366                CA    CA E 502     1555   1555  2.59
SITE     1 AC1  4 ASP A  61  HIS A  81  HIS A  87  ASP A 238
SITE     1 AC2  4 GLY A 286  GLU A 360  ASP A 365  PRO A 366
SITE     1 AC3  4 ASP E  61  HIS E  81  HIS E  87  ASP E 238
SITE     1 AC4  4 GLY E 286  GLU E 360  ASP E 365  PRO E 366
CRYST1   86.753   94.693  126.431  90.00  90.00  90.00 P 21 21 21    8
ORIGX1      1.000000  0.000000  0.000000        0.00000
ORIGX2      0.000000  1.000000  0.000000        0.00000
ORIGX3      0.000000  0.000000  1.000000        0.00000
SCALE1      0.011527  0.000000  0.000000        0.00000
SCALE2      0.000000  0.010560  0.000000        0.00000
SCALE3      0.000000  0.000000  0.007909        0.00000
TER    3034      ARG A 387
TER    6044      ARG E 387
MASTER      481    0    4   42   22    0    4    6 6066    2   19   66
END