longtext: 5zoa-pdb

content
HEADER    HYDROLASE                               12-APR-18   5ZOA
TITLE     THE CRYSTAL STRUCTURE OF A THERMOBIFIDA FUSCA CUTINASE
COMPND    MOL_ID: 1;
COMPND   2 MOLECULE: BTA-HYDROLASE 1;
COMPND   3 CHAIN: A;
COMPND   4 SYNONYM: CUTINASE;
COMPND   5 EC: 3.1.1.74;
COMPND   6 ENGINEERED: YES
SOURCE    MOL_ID: 1;
SOURCE   2 ORGANISM_SCIENTIFIC: THERMOBIFIDA FUSCA;
SOURCE   3 ORGANISM_COMMON: THERMOMONOSPORA FUSCA;
SOURCE   4 ORGANISM_TAXID: 2021;
SOURCE   5 GENE: BTA1, CUT_2;
SOURCE   6 EXPRESSION_SYSTEM: ESCHERICHIA COLI K-12;
SOURCE   7 EXPRESSION_SYSTEM_TAXID: 83333;
SOURCE   8 EXPRESSION_SYSTEM_STRAIN: K-12
KEYWDS    CUTIN, THERMOBIFIDA FUSCA CUTINASE HYDROLYSIS ACTIVITY, HYDROLASE
EXPDTA    X-RAY DIFFRACTION
AUTHOR    Q.L.DONG,L.WU,J.WU,J.H.ZHOU
REVDAT   1   17-APR-19 5ZOA    0
JRNL        AUTH   Q.L.DONG,L.WU,J.WU,J.H.ZHOU
JRNL        TITL   THE CRYSTAL STRUCTURE OF A CUTINASE FROM THERMOBIFIDA FUSCA
JRNL        REF    TO BE PUBLISHED
JRNL        REFN
REMARK   2
REMARK   2 RESOLUTION.    1.54 ANGSTROMS.
REMARK   3
REMARK   3 REFINEMENT.
REMARK   3   PROGRAM     : PHENIX (1.12_2829: ???)
REMARK   3   AUTHORS     : PAUL ADAMS,PAVEL AFONINE,VINCENT CHEN,IAN
REMARK   3               : DAVIS,KRESHNA GOPAL,RALF GROSSE-KUNSTLEVE,
REMARK   3               : LI-WEI HUNG,ROBERT IMMORMINO,TOM IOERGER,
REMARK   3               : AIRLIE MCCOY,ERIK MCKEE,NIGEL MORIARTY,
REMARK   3               : REETAL PAI,RANDY READ,JANE RICHARDSON,
REMARK   3               : DAVID RICHARDSON,TOD ROMO,JIM SACCHETTINI,
REMARK   3               : NICHOLAS SAUTER,JACOB SMITH,LAURENT
REMARK   3               : STORONI,TOM TERWILLIGER,PETER ZWART
REMARK   3
REMARK   3    REFINEMENT TARGET : NULL
REMARK   3
REMARK   3  DATA USED IN REFINEMENT.
REMARK   3   RESOLUTION RANGE HIGH (ANGSTROMS) : 1.54
REMARK   3   RESOLUTION RANGE LOW  (ANGSTROMS) : 28.54
REMARK   3   MIN(FOBS/SIGMA_FOBS)              : 1.340
REMARK   3   COMPLETENESS FOR RANGE        (%) : 99.7
REMARK   3   NUMBER OF REFLECTIONS             : 43229
REMARK   3
REMARK   3  FIT TO DATA USED IN REFINEMENT.
REMARK   3   R VALUE     (WORKING + TEST SET) : 0.166
REMARK   3   R VALUE            (WORKING SET) : 0.166
REMARK   3   FREE R VALUE                     : 0.180
REMARK   3   FREE R VALUE TEST SET SIZE   (%) : 4.830
REMARK   3   FREE R VALUE TEST SET COUNT      : 2089
REMARK   3
REMARK   3  FIT TO DATA USED IN REFINEMENT (IN BINS).
REMARK   3   BIN  RESOLUTION RANGE  COMPL.    NWORK NFREE   RWORK  RFREE
REMARK   3     1 28.5473 -  3.7887    0.99     2968   143  0.1640 0.1797
REMARK   3     2  3.7887 -  3.0083    1.00     2840   133  0.1668 0.1628
REMARK   3     3  3.0083 -  2.6283    1.00     2765   151  0.1842 0.2016
REMARK   3     4  2.6283 -  2.3881    1.00     2747   143  0.1732 0.1985
REMARK   3     5  2.3881 -  2.2170    1.00     2749   144  0.1626 0.1692
REMARK   3     6  2.2170 -  2.0864    1.00     2738   154  0.1546 0.1595
REMARK   3     7  2.0864 -  1.9819    1.00     2710   150  0.1513 0.1658
REMARK   3     8  1.9819 -  1.8956    1.00     2766   104  0.1568 0.1829
REMARK   3     9  1.8956 -  1.8227    1.00     2683   140  0.1567 0.1639
REMARK   3    10  1.8227 -  1.7598    1.00     2704   162  0.1498 0.2056
REMARK   3    11  1.7598 -  1.7048    1.00     2737   131  0.1546 0.1833
REMARK   3    12  1.7048 -  1.6561    1.00     2702   119  0.1561 0.1843
REMARK   3    13  1.6561 -  1.6125    1.00     2695   144  0.1696 0.1667
REMARK   3    14  1.6125 -  1.5731    1.00     2684   139  0.1841 0.2258
REMARK   3    15  1.5731 -  1.5374    0.98     2652   132  0.2111 0.2387
REMARK   3
REMARK   3  BULK SOLVENT MODELLING.
REMARK   3   METHOD USED        : NULL
REMARK   3   SOLVENT RADIUS     : 1.11
REMARK   3   SHRINKAGE RADIUS   : 0.90
REMARK   3   K_SOL              : NULL
REMARK   3   B_SOL              : NULL
REMARK   3
REMARK   3  ERROR ESTIMATES.
REMARK   3   COORDINATE ERROR (MAXIMUM-LIKELIHOOD BASED)     : 0.150
REMARK   3   PHASE ERROR (DEGREES, MAXIMUM-LIKELIHOOD BASED) : 16.680
REMARK   3
REMARK   3  B VALUES.
REMARK   3   FROM WILSON PLOT           (A**2) : NULL
REMARK   3   MEAN B VALUE      (OVERALL, A**2) : NULL
REMARK   3   OVERALL ANISOTROPIC B VALUE.
REMARK   3    B11 (A**2) : NULL
REMARK   3    B22 (A**2) : NULL
REMARK   3    B33 (A**2) : NULL
REMARK   3    B12 (A**2) : NULL
REMARK   3    B13 (A**2) : NULL
REMARK   3    B23 (A**2) : NULL
REMARK   3
REMARK   3  TWINNING INFORMATION.
REMARK   3   FRACTION: NULL
REMARK   3   OPERATOR: NULL
REMARK   3
REMARK   3  DEVIATIONS FROM IDEAL VALUES.
REMARK   3                 RMSD          COUNT
REMARK   3   BOND      :  0.010           2069
REMARK   3   ANGLE     :  1.147           2834
REMARK   3   CHIRALITY :  0.074            318
REMARK   3   PLANARITY :  0.008            372
REMARK   3   DIHEDRAL  :  2.791           1685
REMARK   3
REMARK   3  TLS DETAILS
REMARK   3   NUMBER OF TLS GROUPS  : 1
REMARK   3   TLS GROUP : 1
REMARK   3    SELECTION: ALL
REMARK   3    ORIGIN FOR THE GROUP (A): -15.0740  31.7331  17.1818
REMARK   3    T TENSOR
REMARK   3      T11:   0.0614 T22:   0.0815
REMARK   3      T33:   0.0583 T12:   0.0007
REMARK   3      T13:   0.0134 T23:   0.0049
REMARK   3    L TENSOR
REMARK   3      L11:   1.8747 L22:   1.8214
REMARK   3      L33:   1.5125 L12:   0.7580
REMARK   3      L13:  -0.2088 L23:  -0.1433
REMARK   3    S TENSOR
REMARK   3      S11:  -0.0907 S12:  -0.0371 S13:  -0.0604
REMARK   3      S21:  -0.0455 S22:   0.0439 S23:  -0.0109
REMARK   3      S31:   0.0040 S32:   0.1548 S33:  -0.0111
REMARK   3
REMARK   3  NCS DETAILS
REMARK   3   NUMBER OF NCS GROUPS : NULL
REMARK   3
REMARK   3  OTHER REFINEMENT REMARKS: NULL
REMARK   4
REMARK   4 5ZOA COMPLIES WITH FORMAT V. 3.30, 13-JUL-11
REMARK 100
REMARK 100 THIS ENTRY HAS BEEN PROCESSED BY PDBJ ON 14-APR-18.
REMARK 100 THE DEPOSITION ID IS D_1300007387.
REMARK 200
REMARK 200 EXPERIMENTAL DETAILS
REMARK 200  EXPERIMENT TYPE                : X-RAY DIFFRACTION
REMARK 200  DATE OF DATA COLLECTION        : 14-JAN-10
REMARK 200  TEMPERATURE           (KELVIN) : 100
REMARK 200  PH                             : 7.0
REMARK 200  NUMBER OF CRYSTALS USED        : 1
REMARK 200
REMARK 200  SYNCHROTRON              (Y/N) : Y
REMARK 200  RADIATION SOURCE               : SSRF
REMARK 200  BEAMLINE                       : BL17U1
REMARK 200  X-RAY GENERATOR MODEL          : NULL
REMARK 200  MONOCHROMATIC OR LAUE    (M/L) : M
REMARK 200  WAVELENGTH OR RANGE        (A) : 0.9796
REMARK 200  MONOCHROMATOR                  : NULL
REMARK 200  OPTICS                         : NULL
REMARK 200
REMARK 200  DETECTOR TYPE                  : PIXEL
REMARK 200  DETECTOR MANUFACTURER          : DECTRIS PILATUS 300K
REMARK 200  INTENSITY-INTEGRATION SOFTWARE : HKL-2000
REMARK 200  DATA SCALING SOFTWARE          : HKL-2000
REMARK 200
REMARK 200  NUMBER OF UNIQUE REFLECTIONS   : 43283
REMARK 200  RESOLUTION RANGE HIGH      (A) : 1.537
REMARK 200  RESOLUTION RANGE LOW       (A) : 50.000
REMARK 200  REJECTION CRITERIA  (SIGMA(I)) : NULL
REMARK 200
REMARK 200 OVERALL.
REMARK 200  COMPLETENESS FOR RANGE     (%) : 99.8
REMARK 200  DATA REDUNDANCY                : 18.60
REMARK 200  R MERGE                    (I) : NULL
REMARK 200  R SYM                      (I) : NULL
REMARK 200   FOR THE DATA SET  : 2.0000
REMARK 200
REMARK 200 IN THE HIGHEST RESOLUTION SHELL.
REMARK 200  HIGHEST RESOLUTION SHELL, RANGE HIGH (A) : 1.54
REMARK 200  HIGHEST RESOLUTION SHELL, RANGE LOW  (A) : 1.60
REMARK 200  COMPLETENESS FOR SHELL     (%) : NULL
REMARK 200  DATA REDUNDANCY IN SHELL       : NULL
REMARK 200  R MERGE FOR SHELL          (I) : NULL
REMARK 200  R SYM FOR SHELL            (I) : NULL
REMARK 200   FOR SHELL         : NULL
REMARK 200
REMARK 200 DIFFRACTION PROTOCOL: SINGLE WAVELENGTH
REMARK 200 METHOD USED TO DETERMINE THE STRUCTURE: MOLECULAR REPLACEMENT
REMARK 200 SOFTWARE USED: PHASER
REMARK 200 STARTING MODEL: NULL
REMARK 200
REMARK 200 REMARK: NULL
REMARK 280
REMARK 280 CRYSTAL
REMARK 280 SOLVENT CONTENT, VS   (%): 51.04
REMARK 280 MATTHEWS COEFFICIENT, VM (ANGSTROMS**3/DA): 2.51
REMARK 280
REMARK 280 CRYSTALLIZATION CONDITIONS: 3.0M NACL, 4.0%(V/V) POLYPROPYLENE
REMARK 280  GLYCEL P400, 0.1M HEPES PH 7.0, VAPOR DIFFUSION, SITTING DROP,
REMARK 280  TEMPERATURE 293K
REMARK 290
REMARK 290 CRYSTALLOGRAPHIC SYMMETRY
REMARK 290 SYMMETRY OPERATORS FOR SPACE GROUP: P 4 2 2
REMARK 290
REMARK 290      SYMOP   SYMMETRY
REMARK 290     NNNMMM   OPERATOR
REMARK 290       1555   X,Y,Z
REMARK 290       2555   -X,-Y,Z
REMARK 290       3555   -Y,X,Z
REMARK 290       4555   Y,-X,Z
REMARK 290       5555   -X,Y,-Z
REMARK 290       6555   X,-Y,-Z
REMARK 290       7555   Y,X,-Z
REMARK 290       8555   -Y,-X,-Z
REMARK 290
REMARK 290     WHERE NNN -> OPERATOR NUMBER
REMARK 290           MMM -> TRANSLATION VECTOR
REMARK 290
REMARK 290 CRYSTALLOGRAPHIC SYMMETRY TRANSFORMATIONS
REMARK 290 THE FOLLOWING TRANSFORMATIONS OPERATE ON THE ATOM/HETATM
REMARK 290 RECORDS IN THIS ENTRY TO PRODUCE CRYSTALLOGRAPHICALLY
REMARK 290 RELATED MOLECULES.
REMARK 290   SMTRY1   1  1.000000  0.000000  0.000000        0.00000
REMARK 290   SMTRY2   1  0.000000  1.000000  0.000000        0.00000
REMARK 290   SMTRY3   1  0.000000  0.000000  1.000000        0.00000
REMARK 290   SMTRY1   2 -1.000000  0.000000  0.000000        0.00000
REMARK 290   SMTRY2   2  0.000000 -1.000000  0.000000        0.00000
REMARK 290   SMTRY3   2  0.000000  0.000000  1.000000        0.00000
REMARK 290   SMTRY1   3  0.000000 -1.000000  0.000000        0.00000
REMARK 290   SMTRY2   3  1.000000  0.000000  0.000000        0.00000
REMARK 290   SMTRY3   3  0.000000  0.000000  1.000000        0.00000
REMARK 290   SMTRY1   4  0.000000  1.000000  0.000000        0.00000
REMARK 290   SMTRY2   4 -1.000000  0.000000  0.000000        0.00000
REMARK 290   SMTRY3   4  0.000000  0.000000  1.000000        0.00000
REMARK 290   SMTRY1   5 -1.000000  0.000000  0.000000        0.00000
REMARK 290   SMTRY2   5  0.000000  1.000000  0.000000        0.00000
REMARK 290   SMTRY3   5  0.000000  0.000000 -1.000000        0.00000
REMARK 290   SMTRY1   6  1.000000  0.000000  0.000000        0.00000
REMARK 290   SMTRY2   6  0.000000 -1.000000  0.000000        0.00000
REMARK 290   SMTRY3   6  0.000000  0.000000 -1.000000        0.00000
REMARK 290   SMTRY1   7  0.000000  1.000000  0.000000        0.00000
REMARK 290   SMTRY2   7  1.000000  0.000000  0.000000        0.00000
REMARK 290   SMTRY3   7  0.000000  0.000000 -1.000000        0.00000
REMARK 290   SMTRY1   8  0.000000 -1.000000  0.000000        0.00000
REMARK 290   SMTRY2   8 -1.000000  0.000000  0.000000        0.00000
REMARK 290   SMTRY3   8  0.000000  0.000000 -1.000000        0.00000
REMARK 290
REMARK 290 REMARK: NULL
REMARK 300
REMARK 300 BIOMOLECULE: 1
REMARK 300 SEE REMARK 350 FOR THE AUTHOR PROVIDED AND/OR PROGRAM
REMARK 300 GENERATED ASSEMBLY INFORMATION FOR THE STRUCTURE IN
REMARK 300 THIS ENTRY. THE REMARK MAY ALSO PROVIDE INFORMATION ON
REMARK 300 BURIED SURFACE AREA.
REMARK 350
REMARK 350 COORDINATES FOR A COMPLETE MULTIMER REPRESENTING THE KNOWN
REMARK 350 BIOLOGICALLY SIGNIFICANT OLIGOMERIZATION STATE OF THE
REMARK 350 MOLECULE CAN BE GENERATED BY APPLYING BIOMT TRANSFORMATIONS
REMARK 350 GIVEN BELOW.  BOTH NON-CRYSTALLOGRAPHIC AND
REMARK 350 CRYSTALLOGRAPHIC OPERATIONS ARE GIVEN.
REMARK 350
REMARK 350 BIOMOLECULE: 1
REMARK 350 AUTHOR DETERMINED BIOLOGICAL UNIT: MONOMERIC
REMARK 350 SOFTWARE DETERMINED QUATERNARY STRUCTURE: MONOMERIC
REMARK 350 SOFTWARE USED: PISA
REMARK 350 TOTAL BURIED SURFACE AREA: 140 ANGSTROM**2
REMARK 350 SURFACE AREA OF THE COMPLEX: 9940 ANGSTROM**2
REMARK 350 CHANGE IN SOLVENT FREE ENERGY: -10.0 KCAL/MOL
REMARK 350 APPLY THE FOLLOWING TO CHAINS: A
REMARK 350   BIOMT1   1  1.000000  0.000000  0.000000        0.00000
REMARK 350   BIOMT2   1  0.000000  1.000000  0.000000        0.00000
REMARK 350   BIOMT3   1  0.000000  0.000000  1.000000        0.00000
REMARK 500
REMARK 500 GEOMETRY AND STEREOCHEMISTRY
REMARK 500 SUBTOPIC: CLOSE CONTACTS IN SAME ASYMMETRIC UNIT
REMARK 500
REMARK 500 THE FOLLOWING ATOMS ARE IN CLOSE CONTACT.
REMARK 500
REMARK 500  ATM1  RES C  SSEQI   ATM2  RES C  SSEQI           DISTANCE
REMARK 500   O    HOH A   514     O    HOH A   517              2.05
REMARK 500   OE1  GLU A    64     O    HOH A   401              2.13
REMARK 500
REMARK 500 REMARK: NULL
REMARK 500
REMARK 500 GEOMETRY AND STEREOCHEMISTRY
REMARK 500 SUBTOPIC: COVALENT BOND ANGLES
REMARK 500
REMARK 500 THE STEREOCHEMICAL PARAMETERS OF THE FOLLOWING RESIDUES
REMARK 500 HAVE VALUES WHICH DEVIATE FROM EXPECTED VALUES BY MORE
REMARK 500 THAN 6*RMSD (M=MODEL NUMBER; RES=RESIDUE NAME; C=CHAIN
REMARK 500 IDENTIFIER; SSEQ=SEQUENCE NUMBER; I=INSERTION CODE).
REMARK 500
REMARK 500 STANDARD TABLE:
REMARK 500 FORMAT: (10X,I3,1X,A3,1X,A1,I4,A1,3(1X,A4,2X),12X,F5.1)
REMARK 500
REMARK 500 EXPECTED VALUES PROTEIN: ENGH AND HUBER, 1999
REMARK 500 EXPECTED VALUES NUCLEIC ACID: CLOWNEY ET AL 1996
REMARK 500
REMARK 500  M RES CSSEQI ATM1   ATM2   ATM3
REMARK 500    LEU A  14   CA  -  CB  -  CG  ANGL. DEV. =  17.1 DEGREES
REMARK 500
REMARK 500 REMARK: NULL
REMARK 500
REMARK 500 GEOMETRY AND STEREOCHEMISTRY
REMARK 500 SUBTOPIC: TORSION ANGLES
REMARK 500
REMARK 500 TORSION ANGLES OUTSIDE THE EXPECTED RAMACHANDRAN REGIONS:
REMARK 500 (M=MODEL NUMBER; RES=RESIDUE NAME; C=CHAIN IDENTIFIER;
REMARK 500 SSEQ=SEQUENCE NUMBER; I=INSERTION CODE).
REMARK 500
REMARK 500 STANDARD TABLE:
REMARK 500 FORMAT:(10X,I3,1X,A3,1X,A1,I4,A1,4X,F7.2,3X,F7.2)
REMARK 500
REMARK 500 EXPECTED VALUES: GJ KLEYWEGT AND TA JONES (1996). PHI/PSI-
REMARK 500 CHOLOGY: RAMACHANDRAN REVISITED. STRUCTURE 4, 1395 - 1400
REMARK 500
REMARK 500  M RES CSSEQI        PSI       PHI
REMARK 500    THR A  61       -0.66     70.43
REMARK 500    SER A 130     -119.90     65.74
REMARK 500    THR A 153       59.32     35.39
REMARK 500    HIS A 184      -84.64   -124.53
REMARK 500
REMARK 500 REMARK: NULL
REMARK 800
REMARK 800 SITE
REMARK 800 SITE_IDENTIFIER: AC1
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: binding site for residue CL A 301
REMARK 800
REMARK 800 SITE_IDENTIFIER: AC2
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: binding site for residue CL A 302
DBREF  5ZOA A    1   261  UNP    Q6A0I4   Q6A0I4_THEFU    41    301
SEQRES   1 A  261  ALA ASN PRO TYR GLU ARG GLY PRO ASN PRO THR ASP ALA
SEQRES   2 A  261  LEU LEU GLU ALA SER SER GLY PRO PHE SER VAL SER GLU
SEQRES   3 A  261  GLU ASN VAL SER ARG LEU SER ALA SER GLY PHE GLY GLY
SEQRES   4 A  261  GLY THR ILE TYR TYR PRO ARG GLU ASN ASN THR TYR GLY
SEQRES   5 A  261  ALA VAL ALA ILE SER PRO GLY TYR THR GLY THR GLU ALA
SEQRES   6 A  261  SER ILE ALA TRP LEU GLY GLU ARG ILE ALA SER HIS GLY
SEQRES   7 A  261  PHE VAL VAL ILE THR ILE ASP THR ILE THR THR LEU ASP
SEQRES   8 A  261  GLN PRO ASP SER ARG ALA GLU GLN LEU ASN ALA ALA LEU
SEQRES   9 A  261  ASN HIS MET ILE ASN ARG ALA SER SER THR VAL ARG SER
SEQRES  10 A  261  ARG ILE ASP SER SER ARG LEU ALA VAL MET GLY HIS SER
SEQRES  11 A  261  MET GLY GLY GLY GLY THR LEU ARG LEU ALA SER GLN ARG
SEQRES  12 A  261  PRO ASP LEU LYS ALA ALA ILE PRO LEU THR PRO TRP HIS
SEQRES  13 A  261  LEU ASN LYS ASN TRP SER SER VAL THR VAL PRO THR LEU
SEQRES  14 A  261  ILE ILE GLY ALA ASP LEU ASP THR ILE ALA PRO VAL ALA
SEQRES  15 A  261  THR HIS ALA LYS PRO PHE TYR ASN SER LEU PRO SER SER
SEQRES  16 A  261  ILE SER LYS ALA TYR LEU GLU LEU ASP GLY ALA THR HIS
SEQRES  17 A  261  PHE ALA PRO ASN ILE PRO ASN LYS ILE ILE GLY LYS TYR
SEQRES  18 A  261  SER VAL ALA TRP LEU LYS ARG PHE VAL ASP ASN ASP THR
SEQRES  19 A  261  ARG TYR THR GLN PHE LEU CYS PRO GLY PRO ARG ASP GLY
SEQRES  20 A  261  LEU PHE GLY GLU VAL GLU GLU TYR ARG SER THR CYS PRO
SEQRES  21 A  261  PHE
HET     CL  A 301       1
HET     CL  A 302       1
HETNAM      CL CHLORIDE ION
FORMUL   2   CL    2(CL 1-)
FORMUL   4  HOH   *158(H2 O)
HELIX    1 AA1 THR A   11  ALA A   17  1                                   7
HELIX    2 AA2 THR A   63  SER A   66  5                                   4
HELIX    3 AA3 ILE A   67  SER A   76  1                                  10
HELIX    4 AA4 GLN A   92  ARG A  110  1                                  19
HELIX    5 AA5 SER A  112  SER A  117  1                                   6
HELIX    6 AA6 SER A  130  ARG A  143  1                                  14
HELIX    7 AA7 HIS A  184  LEU A  192  1                                   9
HELIX    8 AA8 PHE A  209  ILE A  213  5                                   5
HELIX    9 AA9 ASN A  215  ASP A  231  1                                  17
HELIX   10 AB1 ASP A  233  ARG A  235  5                                   3
HELIX   11 AB2 TYR A  236  CYS A  241  1                                   6
SHEET    1 AA1 6 VAL A  24  VAL A  29  0
SHEET    2 AA1 6 GLY A  40  PRO A  45 -1  O  ILE A  42   N  GLU A  27
SHEET    3 AA1 6 VAL A  80  ILE A  84 -1  O  VAL A  81   N  TYR A  43
SHEET    4 AA1 6 TYR A  51  SER A  57  1  N  VAL A  54   O  ILE A  82
SHEET    5 AA1 6 ILE A 119  HIS A 129  1  O  ASP A 120   N  TYR A  51
SHEET    6 AA1 6 ALA A 148  LEU A 152  1  O  LEU A 152   N  GLY A 128
SHEET    1 AA2 3 THR A 168  ALA A 173  0
SHEET    2 AA2 3 LYS A 198  LEU A 203  1  O  LEU A 203   N  GLY A 172
SHEET    3 AA2 3 GLU A 254  SER A 257 -1  O  GLU A 254   N  GLU A 202
CISPEP   1 CYS A  241    PRO A  242          0         9.30
CISPEP   2 CYS A  259    PRO A  260          0        15.86
SITE     1 AC1  1 ASN A 215
SITE     1 AC2  3 ASN A 215  LYS A 216  HOH A 532
CRYST1   86.298   86.298   76.117  90.00  90.00  90.00 P 4 2 2       8
ORIGX1      1.000000  0.000000  0.000000        0.00000
ORIGX2      0.000000  1.000000  0.000000        0.00000
ORIGX3      0.000000  0.000000  1.000000        0.00000
SCALE1      0.011588  0.000000  0.000000        0.00000
SCALE2      0.000000  0.011588  0.000000        0.00000
SCALE3      0.000000  0.000000  0.013138        0.00000
TER    2013      PHE A 261
MASTER      298    0    2   11    9    0    2    6 2148    1    0   21
END