longtext: 6cl4-pdb

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HEADER    HYDROLASE                               01-MAR-18   6CL4
TITLE     LIPC12 - LIPASE FROM METAGENOMICS
COMPND    MOL_ID: 1;
COMPND   2 MOLECULE: LIPASE C12;
COMPND   3 CHAIN: A;
COMPND   4 EC: 3.1.1.3;
COMPND   5 ENGINEERED: YES
SOURCE    MOL_ID: 1;
SOURCE   2 ORGANISM_SCIENTIFIC: UNCULTURED BACTERIUM;
SOURCE   3 ORGANISM_TAXID: 77133;
SOURCE   4 GENE: LIPC12;
SOURCE   5 EXPRESSION_SYSTEM: ESCHERICHIA COLI;
SOURCE   6 EXPRESSION_SYSTEM_TAXID: 562
KEYWDS    LIPASE, HYDROLASE
EXPDTA    X-RAY DIFFRACTION
AUTHOR    J.IULEK,V.P.MARTINI,N.KRIEGER,A.GLOGAUER,E.M.SOUZA
REVDAT   1   13-MAR-19 6CL4    0
JRNL        AUTH   V.P.MARTINI,N.KRIEGER,A.GLOGAUER,E.M.SOUZA,J.IULEK
JRNL        TITL   STRUCTURE SOLUTION AND ANALYSES OF THE FIRST TRUE LIPASE
JRNL        TITL 2 OBTAINED FROM METAGENOMICS
JRNL        REF    TO BE PUBLISHED
JRNL        REFN
REMARK   2
REMARK   2 RESOLUTION.    2.64 ANGSTROMS.
REMARK   3
REMARK   3 REFINEMENT.
REMARK   3   PROGRAM     : PHENIX 1.9_1692
REMARK   3   AUTHORS     : PAUL ADAMS,PAVEL AFONINE,VINCENT CHEN,IAN
REMARK   3               : DAVIS,KRESHNA GOPAL,RALF GROSSE-KUNSTLEVE,
REMARK   3               : LI-WEI HUNG,ROBERT IMMORMINO,TOM IOERGER,
REMARK   3               : AIRLIE MCCOY,ERIK MCKEE,NIGEL MORIARTY,
REMARK   3               : REETAL PAI,RANDY READ,JANE RICHARDSON,
REMARK   3               : DAVID RICHARDSON,TOD ROMO,JIM SACCHETTINI,
REMARK   3               : NICHOLAS SAUTER,JACOB SMITH,LAURENT
REMARK   3               : STORONI,TOM TERWILLIGER,PETER ZWART
REMARK   3
REMARK   3    REFINEMENT TARGET : NULL
REMARK   3
REMARK   3  DATA USED IN REFINEMENT.
REMARK   3   RESOLUTION RANGE HIGH (ANGSTROMS) : 2.64
REMARK   3   RESOLUTION RANGE LOW  (ANGSTROMS) : 48.18
REMARK   3   MIN(FOBS/SIGMA_FOBS)              : 1.350
REMARK   3   COMPLETENESS FOR RANGE        (%) : 99.4
REMARK   3   NUMBER OF REFLECTIONS             : 10487
REMARK   3
REMARK   3  FIT TO DATA USED IN REFINEMENT.
REMARK   3   R VALUE     (WORKING + TEST SET) : 0.195
REMARK   3   R VALUE            (WORKING SET) : 0.192
REMARK   3   FREE R VALUE                     : 0.251
REMARK   3   FREE R VALUE TEST SET SIZE   (%) : 4.800
REMARK   3   FREE R VALUE TEST SET COUNT      : 503
REMARK   3
REMARK   3  FIT TO DATA USED IN REFINEMENT (IN BINS).
REMARK   3   BIN  RESOLUTION RANGE  COMPL.    NWORK NFREE   RWORK  RFREE
REMARK   3     1 48.1830 -  4.1901    0.99     2638   127  0.1757 0.2374
REMARK   3     2  4.1901 -  3.3260    1.00     2504   120  0.1761 0.2306
REMARK   3     3  3.3260 -  2.9057    1.00     2419   144  0.2160 0.2757
REMARK   3     4  2.9057 -  2.6400    0.99     2423   112  0.2400 0.2830
REMARK   3
REMARK   3  BULK SOLVENT MODELLING.
REMARK   3   METHOD USED        : NULL
REMARK   3   SOLVENT RADIUS     : 1.30
REMARK   3   SHRINKAGE RADIUS   : 1.00
REMARK   3   K_SOL              : NULL
REMARK   3   B_SOL              : NULL
REMARK   3
REMARK   3  ERROR ESTIMATES.
REMARK   3   COORDINATE ERROR (MAXIMUM-LIKELIHOOD BASED)     : 0.290
REMARK   3   PHASE ERROR (DEGREES, MAXIMUM-LIKELIHOOD BASED) : 22.630
REMARK   3
REMARK   3  B VALUES.
REMARK   3   FROM WILSON PLOT           (A**2) : NULL
REMARK   3   MEAN B VALUE      (OVERALL, A**2) : NULL
REMARK   3   OVERALL ANISOTROPIC B VALUE.
REMARK   3    B11 (A**2) : NULL
REMARK   3    B22 (A**2) : NULL
REMARK   3    B33 (A**2) : NULL
REMARK   3    B12 (A**2) : NULL
REMARK   3    B13 (A**2) : NULL
REMARK   3    B23 (A**2) : NULL
REMARK   3
REMARK   3  TWINNING INFORMATION.
REMARK   3   FRACTION: NULL
REMARK   3   OPERATOR: NULL
REMARK   3
REMARK   3  DEVIATIONS FROM IDEAL VALUES.
REMARK   3                 RMSD          COUNT
REMARK   3   BOND      :  0.002           2250
REMARK   3   ANGLE     :  0.447           3058
REMARK   3   CHIRALITY :  0.018            345
REMARK   3   PLANARITY :  0.002            400
REMARK   3   DIHEDRAL  :  9.172            807
REMARK   3
REMARK   3  TLS DETAILS
REMARK   3   NUMBER OF TLS GROUPS  : 1
REMARK   3   TLS GROUP : 1
REMARK   3    SELECTION: CHAIN A
REMARK   3    ORIGIN FOR THE GROUP (A):   4.5125  21.2000  22.0314
REMARK   3    T TENSOR
REMARK   3      T11:   0.1718 T22:   0.2189
REMARK   3      T33:   0.1874 T12:   0.0669
REMARK   3      T13:   0.0072 T23:   0.0056
REMARK   3    L TENSOR
REMARK   3      L11:   0.7649 L22:   1.2731
REMARK   3      L33:   3.0022 L12:   0.6386
REMARK   3      L13:   0.9212 L23:   1.0468
REMARK   3    S TENSOR
REMARK   3      S11:   0.0214 S12:  -0.0749 S13:  -0.0352
REMARK   3      S21:  -0.0523 S22:  -0.0010 S23:  -0.0416
REMARK   3      S31:  -0.0453 S32:  -0.0924 S33:  -0.0238
REMARK   3
REMARK   3  NCS DETAILS
REMARK   3   NUMBER OF NCS GROUPS : NULL
REMARK   3
REMARK   3  OTHER REFINEMENT REMARKS: NULL
REMARK   4
REMARK   4 6CL4 COMPLIES WITH FORMAT V. 3.30, 13-JUL-11
REMARK 100
REMARK 100 THIS ENTRY HAS BEEN PROCESSED BY RCSB ON 02-MAR-18.
REMARK 100 THE DEPOSITION ID IS D_1000230955.
REMARK 200
REMARK 200 EXPERIMENTAL DETAILS
REMARK 200  EXPERIMENT TYPE                : X-RAY DIFFRACTION
REMARK 200  DATE OF DATA COLLECTION        : 29-JUL-09
REMARK 200  TEMPERATURE           (KELVIN) : 100
REMARK 200  PH                             : 7.0
REMARK 200  NUMBER OF CRYSTALS USED        : 1
REMARK 200
REMARK 200  SYNCHROTRON              (Y/N) : N
REMARK 200  RADIATION SOURCE               : ROTATING ANODE
REMARK 200  BEAMLINE                       : NULL
REMARK 200  X-RAY GENERATOR MODEL          : RIGAKU MICROMAX-007
REMARK 200  MONOCHROMATIC OR LAUE    (M/L) : M
REMARK 200  WAVELENGTH OR RANGE        (A) : 1.5418
REMARK 200  MONOCHROMATOR                  : NULL
REMARK 200  OPTICS                         : NULL
REMARK 200
REMARK 200  DETECTOR TYPE                  : IMAGE PLATE
REMARK 200  DETECTOR MANUFACTURER          : RIGAKU RAXIS IV++
REMARK 200  INTENSITY-INTEGRATION SOFTWARE : XDS VERSION DECEMBER 28, 2009
REMARK 200  DATA SCALING SOFTWARE          : XSCALE VERSION JANUARY 30, 2009
REMARK 200
REMARK 200  NUMBER OF UNIQUE REFLECTIONS   : 10489
REMARK 200  RESOLUTION RANGE HIGH      (A) : 2.640
REMARK 200  RESOLUTION RANGE LOW       (A) : 58.500
REMARK 200  REJECTION CRITERIA  (SIGMA(I)) : -3.000
REMARK 200
REMARK 200 OVERALL.
REMARK 200  COMPLETENESS FOR RANGE     (%) : 95.5
REMARK 200  DATA REDUNDANCY                : 8.820
REMARK 200  R MERGE                    (I) : NULL
REMARK 200  R SYM                      (I) : NULL
REMARK 200   FOR THE DATA SET  : 18.9100
REMARK 200
REMARK 200 IN THE HIGHEST RESOLUTION SHELL.
REMARK 200  HIGHEST RESOLUTION SHELL, RANGE HIGH (A) : 2.64
REMARK 200  HIGHEST RESOLUTION SHELL, RANGE LOW  (A) : 2.72
REMARK 200  COMPLETENESS FOR SHELL     (%) : 97.7
REMARK 200  DATA REDUNDANCY IN SHELL       : 8.38
REMARK 200  R MERGE FOR SHELL          (I) : NULL
REMARK 200  R SYM FOR SHELL            (I) : NULL
REMARK 200   FOR SHELL         : 4.290
REMARK 200
REMARK 200 DIFFRACTION PROTOCOL: SINGLE WAVELENGTH
REMARK 200 METHOD USED TO DETERMINE THE STRUCTURE: MOLECULAR REPLACEMENT
REMARK 200 SOFTWARE USED: PHASER
REMARK 200 STARTING MODEL: 1EX9
REMARK 200
REMARK 200 REMARK: NEEDLES
REMARK 280
REMARK 280 CRYSTAL
REMARK 280 SOLVENT CONTENT, VS   (%): 50.40
REMARK 280 MATTHEWS COEFFICIENT, VM (ANGSTROMS**3/DA): 2.48
REMARK 280
REMARK 280 CRYSTALLIZATION CONDITIONS: 2.0 M SODIUM FORMATE AND 0.1 M BIS
REMARK 280  -TRIS PROPANE, PH 7.0 USING A PROTEIN CONCENTRATION OF 10 MG /
REMARK 280  ML. CRYSTALS GROWN FOR TEN WEEKS, VAPOR DIFFUSION, SITTING DROP,
REMARK 280  TEMPERATURE 291K
REMARK 290
REMARK 290 CRYSTALLOGRAPHIC SYMMETRY
REMARK 290 SYMMETRY OPERATORS FOR SPACE GROUP: P 41 2 2
REMARK 290
REMARK 290      SYMOP   SYMMETRY
REMARK 290     NNNMMM   OPERATOR
REMARK 290       1555   X,Y,Z
REMARK 290       2555   -X,-Y,Z+1/2
REMARK 290       3555   -Y,X,Z+1/4
REMARK 290       4555   Y,-X,Z+3/4
REMARK 290       5555   -X,Y,-Z
REMARK 290       6555   X,-Y,-Z+1/2
REMARK 290       7555   Y,X,-Z+3/4
REMARK 290       8555   -Y,-X,-Z+1/4
REMARK 290
REMARK 290     WHERE NNN -> OPERATOR NUMBER
REMARK 290           MMM -> TRANSLATION VECTOR
REMARK 290
REMARK 290 CRYSTALLOGRAPHIC SYMMETRY TRANSFORMATIONS
REMARK 290 THE FOLLOWING TRANSFORMATIONS OPERATE ON THE ATOM/HETATM
REMARK 290 RECORDS IN THIS ENTRY TO PRODUCE CRYSTALLOGRAPHICALLY
REMARK 290 RELATED MOLECULES.
REMARK 290   SMTRY1   1  1.000000  0.000000  0.000000        0.00000
REMARK 290   SMTRY2   1  0.000000  1.000000  0.000000        0.00000
REMARK 290   SMTRY3   1  0.000000  0.000000  1.000000        0.00000
REMARK 290   SMTRY1   2 -1.000000  0.000000  0.000000        0.00000
REMARK 290   SMTRY2   2  0.000000 -1.000000  0.000000        0.00000
REMARK 290   SMTRY3   2  0.000000  0.000000  1.000000       96.35000
REMARK 290   SMTRY1   3  0.000000 -1.000000  0.000000        0.00000
REMARK 290   SMTRY2   3  1.000000  0.000000  0.000000        0.00000
REMARK 290   SMTRY3   3  0.000000  0.000000  1.000000       48.17500
REMARK 290   SMTRY1   4  0.000000  1.000000  0.000000        0.00000
REMARK 290   SMTRY2   4 -1.000000  0.000000  0.000000        0.00000
REMARK 290   SMTRY3   4  0.000000  0.000000  1.000000      144.52500
REMARK 290   SMTRY1   5 -1.000000  0.000000  0.000000        0.00000
REMARK 290   SMTRY2   5  0.000000  1.000000  0.000000        0.00000
REMARK 290   SMTRY3   5  0.000000  0.000000 -1.000000        0.00000
REMARK 290   SMTRY1   6  1.000000  0.000000  0.000000        0.00000
REMARK 290   SMTRY2   6  0.000000 -1.000000  0.000000        0.00000
REMARK 290   SMTRY3   6  0.000000  0.000000 -1.000000       96.35000
REMARK 290   SMTRY1   7  0.000000  1.000000  0.000000        0.00000
REMARK 290   SMTRY2   7  1.000000  0.000000  0.000000        0.00000
REMARK 290   SMTRY3   7  0.000000  0.000000 -1.000000      144.52500
REMARK 290   SMTRY1   8  0.000000 -1.000000  0.000000        0.00000
REMARK 290   SMTRY2   8 -1.000000  0.000000  0.000000        0.00000
REMARK 290   SMTRY3   8  0.000000  0.000000 -1.000000       48.17500
REMARK 290
REMARK 290 REMARK: NULL
REMARK 300
REMARK 300 BIOMOLECULE: 1
REMARK 300 SEE REMARK 350 FOR THE AUTHOR PROVIDED AND/OR PROGRAM
REMARK 300 GENERATED ASSEMBLY INFORMATION FOR THE STRUCTURE IN
REMARK 300 THIS ENTRY. THE REMARK MAY ALSO PROVIDE INFORMATION ON
REMARK 300 BURIED SURFACE AREA.
REMARK 350
REMARK 350 COORDINATES FOR A COMPLETE MULTIMER REPRESENTING THE KNOWN
REMARK 350 BIOLOGICALLY SIGNIFICANT OLIGOMERIZATION STATE OF THE
REMARK 350 MOLECULE CAN BE GENERATED BY APPLYING BIOMT TRANSFORMATIONS
REMARK 350 GIVEN BELOW.  BOTH NON-CRYSTALLOGRAPHIC AND
REMARK 350 CRYSTALLOGRAPHIC OPERATIONS ARE GIVEN.
REMARK 350
REMARK 350 BIOMOLECULE: 1
REMARK 350 AUTHOR DETERMINED BIOLOGICAL UNIT: MONOMERIC
REMARK 350 APPLY THE FOLLOWING TO CHAINS: A
REMARK 350   BIOMT1   1  1.000000  0.000000  0.000000        0.00000
REMARK 350   BIOMT2   1  0.000000  1.000000  0.000000        0.00000
REMARK 350   BIOMT3   1  0.000000  0.000000  1.000000        0.00000
REMARK 465
REMARK 465 MISSING RESIDUES
REMARK 465 THE FOLLOWING RESIDUES WERE NOT LOCATED IN THE
REMARK 465 EXPERIMENT. (M=MODEL NUMBER; RES=RESIDUE NAME; C=CHAIN
REMARK 465 IDENTIFIER; SSSEQ=SEQUENCE NUMBER; I=INSERTION CODE.)
REMARK 465
REMARK 465   M RES C SSSEQI
REMARK 465     MET A   -19
REMARK 465     GLY A   -18
REMARK 465     SER A   -17
REMARK 465     SER A   -16
REMARK 465     HIS A   -15
REMARK 465     HIS A   -14
REMARK 465     HIS A   -13
REMARK 465     HIS A   -12
REMARK 465     HIS A   -11
REMARK 465     HIS A   -10
REMARK 465     SER A    -9
REMARK 465     SER A    -8
REMARK 465     GLY A    -7
REMARK 465     LEU A    -6
REMARK 465     VAL A    -5
REMARK 465     PRO A    -4
REMARK 465     ARG A    -3
REMARK 465     GLY A    -2
REMARK 465     SER A    -1
REMARK 465     HIS A     0
REMARK 465     MET A     1
REMARK 465     SER A     2
REMARK 465     ALA A     3
REMARK 470
REMARK 470 MISSING ATOM
REMARK 470 THE FOLLOWING RESIDUES HAVE MISSING ATOMS (M=MODEL NUMBER;
REMARK 470 RES=RESIDUE NAME; C=CHAIN IDENTIFIER; SSEQ=SEQUENCE NUMBER;
REMARK 470 I=INSERTION CODE):
REMARK 470   M RES CSSEQI  ATOMS
REMARK 470     LYS A  42    NZ
REMARK 470     GLU A  71    CD   OE1  OE2
REMARK 470     LYS A 175    NZ
REMARK 470     LYS A 250    NZ
REMARK 500
REMARK 500 GEOMETRY AND STEREOCHEMISTRY
REMARK 500 SUBTOPIC: TORSION ANGLES
REMARK 500
REMARK 500 TORSION ANGLES OUTSIDE THE EXPECTED RAMACHANDRAN REGIONS:
REMARK 500 (M=MODEL NUMBER; RES=RESIDUE NAME; C=CHAIN IDENTIFIER;
REMARK 500 SSEQ=SEQUENCE NUMBER; I=INSERTION CODE).
REMARK 500
REMARK 500 STANDARD TABLE:
REMARK 500 FORMAT:(10X,I3,1X,A3,1X,A1,I4,A1,4X,F7.2,3X,F7.2)
REMARK 500
REMARK 500 EXPECTED VALUES: GJ KLEYWEGT AND TA JONES (1996). PHI/PSI-
REMARK 500 CHOLOGY: RAMACHANDRAN REVISITED. STRUCTURE 4, 1395 - 1400
REMARK 500
REMARK 500  M RES CSSEQI        PSI       PHI
REMARK 500    ILE A  25      -31.69   -133.52
REMARK 500    SER A  83     -104.91     57.84
REMARK 500    PRO A 125       96.05    -64.50
REMARK 500    ALA A 213       43.82   -149.23
REMARK 500    GLN A 236       78.40   -159.89
REMARK 500    LEU A 240      -33.26   -138.07
REMARK 500
REMARK 500 REMARK: NULL
DBREF  6CL4 A    1   293  UNP    G1APT8   G1APT8_9BACT     1    293
SEQADV 6CL4 MET A  -19  UNP  G1APT8              EXPRESSION TAG
SEQADV 6CL4 GLY A  -18  UNP  G1APT8              EXPRESSION TAG
SEQADV 6CL4 SER A  -17  UNP  G1APT8              EXPRESSION TAG
SEQADV 6CL4 SER A  -16  UNP  G1APT8              EXPRESSION TAG
SEQADV 6CL4 HIS A  -15  UNP  G1APT8              EXPRESSION TAG
SEQADV 6CL4 HIS A  -14  UNP  G1APT8              EXPRESSION TAG
SEQADV 6CL4 HIS A  -13  UNP  G1APT8              EXPRESSION TAG
SEQADV 6CL4 HIS A  -12  UNP  G1APT8              EXPRESSION TAG
SEQADV 6CL4 HIS A  -11  UNP  G1APT8              EXPRESSION TAG
SEQADV 6CL4 HIS A  -10  UNP  G1APT8              EXPRESSION TAG
SEQADV 6CL4 SER A   -9  UNP  G1APT8              EXPRESSION TAG
SEQADV 6CL4 SER A   -8  UNP  G1APT8              EXPRESSION TAG
SEQADV 6CL4 GLY A   -7  UNP  G1APT8              EXPRESSION TAG
SEQADV 6CL4 LEU A   -6  UNP  G1APT8              EXPRESSION TAG
SEQADV 6CL4 VAL A   -5  UNP  G1APT8              EXPRESSION TAG
SEQADV 6CL4 PRO A   -4  UNP  G1APT8              EXPRESSION TAG
SEQADV 6CL4 ARG A   -3  UNP  G1APT8              EXPRESSION TAG
SEQADV 6CL4 GLY A   -2  UNP  G1APT8              EXPRESSION TAG
SEQADV 6CL4 SER A   -1  UNP  G1APT8              EXPRESSION TAG
SEQADV 6CL4 HIS A    0  UNP  G1APT8              EXPRESSION TAG
SEQRES   1 A  313  MET GLY SER SER HIS HIS HIS HIS HIS HIS SER SER GLY
SEQRES   2 A  313  LEU VAL PRO ARG GLY SER HIS MET SER ALA SER SER LEU
SEQRES   3 A  313  LYS PHE PRO ILE VAL LEU VAL HIS GLY LEU LEU GLY PHE
SEQRES   4 A  313  ASP LYS ILE GLY GLY ILE TYR PRO TYR PHE TYR GLY ILE
SEQRES   5 A  313  LYS GLU ALA LEU GLU LYS ALA GLY ALA LYS VAL TYR ILE
SEQRES   6 A  313  ALA THR LEU SER ALA LEU ASN SER ASN GLU LEU ARG GLY
SEQRES   7 A  313  GLU GLN LEU LEU GLU PHE VAL ARG LYS VAL GLN ALA GLU
SEQRES   8 A  313  THR GLY ALA ALA LYS VAL ASN LEU ILE GLY HIS SER GLN
SEQRES   9 A  313  GLY PRO LEU ALA CYS ARG TYR VAL ALA ALA THR HIS PRO
SEQRES  10 A  313  GLU LEU ILE ALA SER VAL THR SER VAL ASN GLY VAL ASN
SEQRES  11 A  313  HIS GLY SER GLU VAL ALA ASP LEU VAL ARG LEU ALA LEU
SEQRES  12 A  313  THR PRO GLY ARG LEU PRO GLU SER ILE ALA ASN ALA ALA
SEQRES  13 A  313  MET SER ALA PHE GLY GLN LEU LEU SER ALA LEU ALA GLY
SEQRES  14 A  313  SER PRO ARG LEU PRO GLN SER GLY ILE GLU ALA LEU GLU
SEQRES  15 A  313  ALA LEU THR SER GLU GLY VAL ALA ALA PHE ASN ASN LYS
SEQRES  16 A  313  TYR PRO GLN GLY LEU PRO ALA GLU TRP GLY GLY GLU GLY
SEQRES  17 A  313  LYS GLU LEU VAL ASN GLY VAL TYR TYR TYR SER TRP SER
SEQRES  18 A  313  GLY VAL ILE ASP TYR ASN PRO LEU HIS GLN GLY ALA ASN
SEQRES  19 A  313  ASN LEU ASP PRO LEU HIS VAL ALA MET LEU ALA PHE SER
SEQRES  20 A  313  ILE LEU PHE THR ASN GLU ARG PHE GLN ASN ASP GLY LEU
SEQRES  21 A  313  VAL GLY ARG TYR SER SER HIS LEU GLY LYS VAL ILE GLY
SEQRES  22 A  313  SER ASP TYR SER MET ASP HIS VAL ASP ALA ILE ASN GLN
SEQRES  23 A  313  LEU ALA GLY VAL VAL ALA ASN ASN THR ASP PRO VAL GLN
SEQRES  24 A  313  LEU PHE VAL GLU HIS VAL ALA ARG LEU LYS SER LYS GLY
SEQRES  25 A  313  LEU
FORMUL   2  HOH   *150(H2 O)
HELIX    1 AA1 GLY A   31  ALA A   39  1                                   9
HELIX    2 AA2 SER A   53  GLY A   73  1                                  21
HELIX    3 AA3 GLN A   84  HIS A   96  1                                  13
HELIX    4 AA4 SER A  113  ARG A  120  1                                   8
HELIX    5 AA5 LEU A  121  THR A  124  5                                   4
HELIX    6 AA6 PRO A  129  GLY A  149  1                                  21
HELIX    7 AA7 LEU A  153  SER A  156  5                                   4
HELIX    8 AA8 GLY A  157  GLU A  162  1                                   6
HELIX    9 AA9 THR A  165  ASN A  174  1                                  10
HELIX   10 AB1 ASP A  217  LEU A  229  1                                  13
HELIX   11 AB2 ARG A  243  HIS A  247  5                                   5
HELIX   12 AB3 VAL A  261  ASN A  265  5                                   5
HELIX   13 AB4 ASP A  276  LYS A  291  1                                  16
SHEET    1 AA1 6 VAL A  43  ILE A  45  0
SHEET    2 AA1 6 ILE A  10  VAL A  13  1  N  ILE A  10   O  TYR A  44
SHEET    3 AA1 6 VAL A  77  HIS A  82  1  O  ILE A  80   N  VAL A  13
SHEET    4 AA1 6 ILE A 100  VAL A 106  1  O  THR A 104   N  LEU A  79
SHEET    5 AA1 6 VAL A 195  VAL A 203  1  O  TYR A 196   N  VAL A 103
SHEET    6 AA1 6 LEU A 191  VAL A 192 -1  N  VAL A 192   O  VAL A 195
SHEET    1 AA2 6 VAL A  43  ILE A  45  0
SHEET    2 AA2 6 ILE A  10  VAL A  13  1  N  ILE A  10   O  TYR A  44
SHEET    3 AA2 6 VAL A  77  HIS A  82  1  O  ILE A  80   N  VAL A  13
SHEET    4 AA2 6 ILE A 100  VAL A 106  1  O  THR A 104   N  LEU A  79
SHEET    5 AA2 6 VAL A 195  VAL A 203  1  O  TYR A 196   N  VAL A 103
SHEET    6 AA2 6 LYS A 250  SER A 257  1  O  TYR A 256   N  VAL A 203
SHEET    1 AA3 2 LYS A  21  ILE A  22  0
SHEET    2 AA3 2 TYR A  26  PRO A  27 -1  O  TYR A  26   N  ILE A  22
CISPEP   1 GLN A  266    LEU A  267          0         3.39
CRYST1   58.500   58.500  192.700  90.00  90.00  90.00 P 41 2 2      8
ORIGX1      1.000000  0.000000  0.000000        0.00000
ORIGX2      0.000000  1.000000  0.000000        0.00000
ORIGX3      0.000000  0.000000  1.000000        0.00000
SCALE1      0.017094  0.000000  0.000000        0.00000
SCALE2      0.000000  0.017094  0.000000        0.00000
SCALE3      0.000000  0.000000  0.005189        0.00000
TER    2204      LEU A 293
MASTER      286    0    0   13   14    0    0    6 2331    1    0   25
END