longtext: 6igr-pdb

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HEADER    HYDROLASE                               25-SEP-18   6IGR
TITLE     CRYSTAL STRUCTURE OF S9 PEPTIDASE (S514A MUTANT IN INACTIVE STATE)
TITLE    2 FROM DEINOCOCCUS RADIODURANS R1
COMPND    MOL_ID: 1;
COMPND   2 MOLECULE: ACYL-PEPTIDE HYDROLASE, PUTATIVE;
COMPND   3 CHAIN: A, B, C, D;
COMPND   4 ENGINEERED: YES;
COMPND   5 MUTATION: YES
SOURCE    MOL_ID: 1;
SOURCE   2 ORGANISM_SCIENTIFIC: DEINOCOCCUS RADIODURANS STR. R1;
SOURCE   3 ORGANISM_TAXID: 243230;
SOURCE   4 STRAIN: R1;
SOURCE   5 GENE: DR_0165;
SOURCE   6 EXPRESSION_SYSTEM: ESCHERICHIA COLI BL21(DE3);
SOURCE   7 EXPRESSION_SYSTEM_TAXID: 469008;
SOURCE   8 EXPRESSION_SYSTEM_STRAIN: BL21(DE3);
SOURCE   9 EXPRESSION_SYSTEM_VARIANT: PLYSS;
SOURCE  10 EXPRESSION_SYSTEM_VECTOR_TYPE: PLASMID;
SOURCE  11 EXPRESSION_SYSTEM_PLASMID: PST50TR
KEYWDS    SERINE PEPTIDASE, MEROPS S9, POP FAMILY, HYDROLASE
EXPDTA    X-RAY DIFFRACTION
AUTHOR    P.YADAV,N.K.GAUR,V.D.GOYAL,A.KUMAR,R.D.MAKDE
REVDAT   1   14-NOV-18 6IGR    0
JRNL        AUTH   P.YADAV,N.K.GAUR,V.D.GOYAL,A.KUMAR,R.D.MAKDE
JRNL        TITL   CRYSTAL STRUCTURE OF S9 PEPTIDASE (S514A MUTANT IN INACTIVE
JRNL        TITL 2 STATE) FROM DEINOCOCCUS RADIODURANS R1
JRNL        REF    TO BE PUBLISHED
JRNL        REFN
REMARK   2
REMARK   2 RESOLUTION.    2.60 ANGSTROMS.
REMARK   3
REMARK   3 REFINEMENT.
REMARK   3   PROGRAM     : PHENIX (1.11.1_2575: ???)
REMARK   3   AUTHORS     : PAUL ADAMS,PAVEL AFONINE,VINCENT CHEN,IAN
REMARK   3               : DAVIS,KRESHNA GOPAL,RALF GROSSE-KUNSTLEVE,
REMARK   3               : LI-WEI HUNG,ROBERT IMMORMINO,TOM IOERGER,
REMARK   3               : AIRLIE MCCOY,ERIK MCKEE,NIGEL MORIARTY,
REMARK   3               : REETAL PAI,RANDY READ,JANE RICHARDSON,
REMARK   3               : DAVID RICHARDSON,TOD ROMO,JIM SACCHETTINI,
REMARK   3               : NICHOLAS SAUTER,JACOB SMITH,LAURENT
REMARK   3               : STORONI,TOM TERWILLIGER,PETER ZWART
REMARK   3
REMARK   3    REFINEMENT TARGET : NULL
REMARK   3
REMARK   3  DATA USED IN REFINEMENT.
REMARK   3   RESOLUTION RANGE HIGH (ANGSTROMS) : 2.60
REMARK   3   RESOLUTION RANGE LOW  (ANGSTROMS) : 39.76
REMARK   3   MIN(FOBS/SIGMA_FOBS)              : 1.340
REMARK   3   COMPLETENESS FOR RANGE        (%) : 99.6
REMARK   3   NUMBER OF REFLECTIONS             : 100744
REMARK   3
REMARK   3  FIT TO DATA USED IN REFINEMENT.
REMARK   3   R VALUE     (WORKING + TEST SET) : 0.218
REMARK   3   R VALUE            (WORKING SET) : 0.216
REMARK   3   FREE R VALUE                     : 0.253
REMARK   3   FREE R VALUE TEST SET SIZE   (%) : 4.950
REMARK   3   FREE R VALUE TEST SET COUNT      : 4982
REMARK   3
REMARK   3  FIT TO DATA USED IN REFINEMENT (IN BINS).
REMARK   3   BIN  RESOLUTION RANGE  COMPL.    NWORK NFREE   RWORK  RFREE
REMARK   3     1 39.7602 -  8.0571    0.98     3234   138  0.1995 0.2516
REMARK   3     2  8.0571 -  6.4039    0.99     3185   172  0.2001 0.2306
REMARK   3     3  6.4039 -  5.5969    1.00     3221   176  0.1947 0.2075
REMARK   3     4  5.5969 -  5.0863    1.00     3190   160  0.1784 0.1879
REMARK   3     5  5.0863 -  4.7223    0.99     3239   145  0.1639 0.1970
REMARK   3     6  4.7223 -  4.4443    0.99     3186   171  0.1609 0.1908
REMARK   3     7  4.4443 -  4.2220    0.99     3187   173  0.1714 0.2044
REMARK   3     8  4.2220 -  4.0384    0.99     3139   165  0.1842 0.1919
REMARK   3     9  4.0384 -  3.8831    1.00     3208   141  0.1890 0.2402
REMARK   3    10  3.8831 -  3.7492    1.00     3206   179  0.2034 0.2467
REMARK   3    11  3.7492 -  3.6320    1.00     3195   160  0.2075 0.2314
REMARK   3    12  3.6320 -  3.5283    0.99     3139   169  0.2162 0.2487
REMARK   3    13  3.5283 -  3.4354    0.99     3262   148  0.2341 0.2969
REMARK   3    14  3.4354 -  3.3517    1.00     3134   156  0.2256 0.2705
REMARK   3    15  3.3517 -  3.2755    1.00     3211   177  0.2403 0.2666
REMARK   3    16  3.2755 -  3.2058    1.00     3159   185  0.2422 0.2753
REMARK   3    17  3.2058 -  3.1417    1.00     3196   197  0.2441 0.2908
REMARK   3    18  3.1417 -  3.0825    1.00     3133   169  0.2483 0.3054
REMARK   3    19  3.0825 -  3.0274    1.00     3222   167  0.2614 0.3253
REMARK   3    20  3.0274 -  2.9761    1.00     3167   193  0.2600 0.2926
REMARK   3    21  2.9761 -  2.9281    1.00     3204   187  0.2507 0.3026
REMARK   3    22  2.9281 -  2.8831    1.00     3137   125  0.2528 0.2955
REMARK   3    23  2.8831 -  2.8407    1.00     3227   167  0.2644 0.3184
REMARK   3    24  2.8407 -  2.8007    1.00     3208   174  0.2707 0.3160
REMARK   3    25  2.8007 -  2.7629    1.00     3177   180  0.2792 0.3097
REMARK   3    26  2.7629 -  2.7270    1.00     3234   154  0.2786 0.3313
REMARK   3    27  2.7270 -  2.6929    1.00     3160   161  0.3051 0.3641
REMARK   3    28  2.6929 -  2.6605    1.00     3208   159  0.3025 0.3504
REMARK   3    29  2.6605 -  2.6296    1.00     3150   161  0.3084 0.3350
REMARK   3    30  2.6296 -  2.6000    1.00     3244   173  0.3118 0.3523
REMARK   3
REMARK   3  BULK SOLVENT MODELLING.
REMARK   3   METHOD USED        : NULL
REMARK   3   SOLVENT RADIUS     : 1.11
REMARK   3   SHRINKAGE RADIUS   : 0.90
REMARK   3   K_SOL              : NULL
REMARK   3   B_SOL              : NULL
REMARK   3
REMARK   3  ERROR ESTIMATES.
REMARK   3   COORDINATE ERROR (MAXIMUM-LIKELIHOOD BASED)     : 0.360
REMARK   3   PHASE ERROR (DEGREES, MAXIMUM-LIKELIHOOD BASED) : 28.110
REMARK   3
REMARK   3  B VALUES.
REMARK   3   FROM WILSON PLOT           (A**2) : 38.30
REMARK   3   MEAN B VALUE      (OVERALL, A**2) : NULL
REMARK   3   OVERALL ANISOTROPIC B VALUE.
REMARK   3    B11 (A**2) : NULL
REMARK   3    B22 (A**2) : NULL
REMARK   3    B33 (A**2) : NULL
REMARK   3    B12 (A**2) : NULL
REMARK   3    B13 (A**2) : NULL
REMARK   3    B23 (A**2) : NULL
REMARK   3
REMARK   3  TWINNING INFORMATION.
REMARK   3   FRACTION: NULL
REMARK   3   OPERATOR: NULL
REMARK   3
REMARK   3  DEVIATIONS FROM IDEAL VALUES.
REMARK   3                 RMSD          COUNT
REMARK   3   BOND      :  0.004          18844
REMARK   3   ANGLE     :  0.711          25726
REMARK   3   CHIRALITY :  0.053           2718
REMARK   3   PLANARITY :  0.005           3410
REMARK   3   DIHEDRAL  :  3.492          10814
REMARK   3
REMARK   3  TLS DETAILS
REMARK   3   NUMBER OF TLS GROUPS  : 1
REMARK   3   TLS GROUP : 1
REMARK   3    SELECTION: ALL
REMARK   3    ORIGIN FOR THE GROUP (A): -20.3015  46.0610 -24.8579
REMARK   3    T TENSOR
REMARK   3      T11:   0.2867 T22:   0.3160
REMARK   3      T33:   0.2954 T12:  -0.0036
REMARK   3      T13:   0.0165 T23:   0.0093
REMARK   3    L TENSOR
REMARK   3      L11:   0.0217 L22:   0.3606
REMARK   3      L33:   0.0896 L12:  -0.0232
REMARK   3      L13:   0.0321 L23:  -0.1095
REMARK   3    S TENSOR
REMARK   3      S11:   0.0102 S12:   0.0042 S13:  -0.0159
REMARK   3      S21:  -0.0700 S22:   0.0248 S23:   0.0245
REMARK   3      S31:   0.0153 S32:  -0.0368 S33:  -0.0365
REMARK   3
REMARK   3  NCS DETAILS
REMARK   3   NUMBER OF NCS GROUPS : NULL
REMARK   3
REMARK   3  OTHER REFINEMENT REMARKS: NULL
REMARK   4
REMARK   4 6IGR COMPLIES WITH FORMAT V. 3.30, 13-JUL-11
REMARK 100
REMARK 100 THIS ENTRY HAS BEEN PROCESSED BY PDBJ ON 09-OCT-18.
REMARK 100 THE DEPOSITION ID IS D_1300009159.
REMARK 200
REMARK 200 EXPERIMENTAL DETAILS
REMARK 200  EXPERIMENT TYPE                : X-RAY DIFFRACTION
REMARK 200  DATE OF DATA COLLECTION        : 08-SEP-18
REMARK 200  TEMPERATURE           (KELVIN) : 100
REMARK 200  PH                             : 5.0-5.4
REMARK 200  NUMBER OF CRYSTALS USED        : 1
REMARK 200
REMARK 200  SYNCHROTRON              (Y/N) : Y
REMARK 200  RADIATION SOURCE               : RRCAT INDUS-2
REMARK 200  BEAMLINE                       : PX-BL21
REMARK 200  X-RAY GENERATOR MODEL          : NULL
REMARK 200  MONOCHROMATIC OR LAUE    (M/L) : M
REMARK 200  WAVELENGTH OR RANGE        (A) : 0.97947
REMARK 200  MONOCHROMATOR                  : SI111
REMARK 200  OPTICS                         : MIRRORS
REMARK 200
REMARK 200  DETECTOR TYPE                  : IMAGE PLATE
REMARK 200  DETECTOR MANUFACTURER          : MAR SCANNER 345 MM PLATE
REMARK 200  INTENSITY-INTEGRATION SOFTWARE : XDS
REMARK 200  DATA SCALING SOFTWARE          : AIMLESS
REMARK 200
REMARK 200  NUMBER OF UNIQUE REFLECTIONS   : 100840
REMARK 200  RESOLUTION RANGE HIGH      (A) : 2.600
REMARK 200  RESOLUTION RANGE LOW       (A) : 47.300
REMARK 200  REJECTION CRITERIA  (SIGMA(I)) : NULL
REMARK 200
REMARK 200 OVERALL.
REMARK 200  COMPLETENESS FOR RANGE     (%) : 99.7
REMARK 200  DATA REDUNDANCY                : 3.500
REMARK 200  R MERGE                    (I) : 0.09600
REMARK 200  R SYM                      (I) : NULL
REMARK 200   FOR THE DATA SET  : 11.4000
REMARK 200
REMARK 200 IN THE HIGHEST RESOLUTION SHELL.
REMARK 200  HIGHEST RESOLUTION SHELL, RANGE HIGH (A) : 2.60
REMARK 200  HIGHEST RESOLUTION SHELL, RANGE LOW  (A) : 2.64
REMARK 200  COMPLETENESS FOR SHELL     (%) : 99.9
REMARK 200  DATA REDUNDANCY IN SHELL       : 3.30
REMARK 200  R MERGE FOR SHELL          (I) : 0.71000
REMARK 200  R SYM FOR SHELL            (I) : NULL
REMARK 200   FOR SHELL         : 2.100
REMARK 200
REMARK 200 DIFFRACTION PROTOCOL: SINGLE WAVELENGTH
REMARK 200 METHOD USED TO DETERMINE THE STRUCTURE: MOLECULAR REPLACEMENT
REMARK 200 SOFTWARE USED: PHASER
REMARK 200 STARTING MODEL: 5YZM
REMARK 200
REMARK 200 REMARK: CUBOID CRYSTALS (100-200 MICRON)
REMARK 280
REMARK 280 CRYSTAL
REMARK 280 SOLVENT CONTENT, VS   (%): 57.86
REMARK 280 MATTHEWS COEFFICIENT, VM (ANGSTROMS**3/DA): 2.92
REMARK 280
REMARK 280 CRYSTALLIZATION CONDITIONS: 40MM POTASSIUM PHOSPHATE, 16% PEG
REMARK 280  8000, 20% GLYCEROL, PH 5.28, MICROBATCH, TEMPERATURE 294K
REMARK 290
REMARK 290 CRYSTALLOGRAPHIC SYMMETRY
REMARK 290 SYMMETRY OPERATORS FOR SPACE GROUP: P 1 21 1
REMARK 290
REMARK 290      SYMOP   SYMMETRY
REMARK 290     NNNMMM   OPERATOR
REMARK 290       1555   X,Y,Z
REMARK 290       2555   -X,Y+1/2,-Z
REMARK 290
REMARK 290     WHERE NNN -> OPERATOR NUMBER
REMARK 290           MMM -> TRANSLATION VECTOR
REMARK 290
REMARK 290 CRYSTALLOGRAPHIC SYMMETRY TRANSFORMATIONS
REMARK 290 THE FOLLOWING TRANSFORMATIONS OPERATE ON THE ATOM/HETATM
REMARK 290 RECORDS IN THIS ENTRY TO PRODUCE CRYSTALLOGRAPHICALLY
REMARK 290 RELATED MOLECULES.
REMARK 290   SMTRY1   1  1.000000  0.000000  0.000000        0.00000
REMARK 290   SMTRY2   1  0.000000  1.000000  0.000000        0.00000
REMARK 290   SMTRY3   1  0.000000  0.000000  1.000000        0.00000
REMARK 290   SMTRY1   2 -1.000000  0.000000  0.000000        0.00000
REMARK 290   SMTRY2   2  0.000000  1.000000  0.000000       94.60000
REMARK 290   SMTRY3   2  0.000000  0.000000 -1.000000        0.00000
REMARK 290
REMARK 290 REMARK: NULL
REMARK 300
REMARK 300 BIOMOLECULE: 1
REMARK 300 SEE REMARK 350 FOR THE AUTHOR PROVIDED AND/OR PROGRAM
REMARK 300 GENERATED ASSEMBLY INFORMATION FOR THE STRUCTURE IN
REMARK 300 THIS ENTRY. THE REMARK MAY ALSO PROVIDE INFORMATION ON
REMARK 300 BURIED SURFACE AREA.
REMARK 350
REMARK 350 COORDINATES FOR A COMPLETE MULTIMER REPRESENTING THE KNOWN
REMARK 350 BIOLOGICALLY SIGNIFICANT OLIGOMERIZATION STATE OF THE
REMARK 350 MOLECULE CAN BE GENERATED BY APPLYING BIOMT TRANSFORMATIONS
REMARK 350 GIVEN BELOW.  BOTH NON-CRYSTALLOGRAPHIC AND
REMARK 350 CRYSTALLOGRAPHIC OPERATIONS ARE GIVEN.
REMARK 350
REMARK 350 BIOMOLECULE: 1
REMARK 350 AUTHOR DETERMINED BIOLOGICAL UNIT: TETRAMERIC
REMARK 350 APPLY THE FOLLOWING TO CHAINS: A, B, C, D
REMARK 350   BIOMT1   1  1.000000  0.000000  0.000000        0.00000
REMARK 350   BIOMT2   1  0.000000  1.000000  0.000000        0.00000
REMARK 350   BIOMT3   1  0.000000  0.000000  1.000000        0.00000
REMARK 465
REMARK 465 MISSING RESIDUES
REMARK 465 THE FOLLOWING RESIDUES WERE NOT LOCATED IN THE
REMARK 465 EXPERIMENT. (M=MODEL NUMBER; RES=RESIDUE NAME; C=CHAIN
REMARK 465 IDENTIFIER; SSSEQ=SEQUENCE NUMBER; I=INSERTION CODE.)
REMARK 465
REMARK 465   M RES C SSSEQI
REMARK 465     GLY A     0
REMARK 465     SER A     1
REMARK 465     ASN A     2
REMARK 465     ASN A     3
REMARK 465     SER A     4
REMARK 465     GLU A     5
REMARK 465     THR A     6
REMARK 465     SER A    40
REMARK 465     GLU A    41
REMARK 465     GLU A    42
REMARK 465     ASP A    43
REMARK 465     PRO A    44
REMARK 465     ALA A    45
REMARK 465     LYS A    46
REMARK 465     PRO A    47
REMARK 465     ASP A    48
REMARK 465     LYS A    49
REMARK 465     ASP A    50
REMARK 465     PHE A    51
REMARK 465     ALA A    52
REMARK 465     ARG A    53
REMARK 465     GLY A    99
REMARK 465     GLU A   100
REMARK 465     ALA A   143
REMARK 465     ASP A   144
REMARK 465     THR A   145
REMARK 465     GLU A   146
REMARK 465     ASP A   147
REMARK 465     LYS A   148
REMARK 465     ARG A   149
REMARK 465     ASP A   150
REMARK 465     GLU A   151
REMARK 465     ARG A   152
REMARK 465     GLY A   153
REMARK 465     GLU A   154
REMARK 465     ALA A   155
REMARK 465     ARG A   156
REMARK 465     VAL A   157
REMARK 465     LEU A   158
REMARK 465     THR A   159
REMARK 465     ARG A   160
REMARK 465     PRO A   161
REMARK 465     VAL A   162
REMARK 465     TYR A   163
REMARK 465     ARG A   164
REMARK 465     ALA A   165
REMARK 465     ASN A   166
REMARK 465     GLY A   167
REMARK 465     ALA A   168
REMARK 465     ASP A   169
REMARK 465     TRP A   170
REMARK 465     LEU A   171
REMARK 465     PRO A   172
REMARK 465     GLU A   173
REMARK 465     ALA A   236
REMARK 465     ASP A   237
REMARK 465     ALA A   238
REMARK 465     GLY B     0
REMARK 465     SER B     1
REMARK 465     ASN B     2
REMARK 465     ASN B     3
REMARK 465     SER B     4
REMARK 465     GLU B     5
REMARK 465     THR B     6
REMARK 465     SER B    40
REMARK 465     GLU B    41
REMARK 465     GLU B    42
REMARK 465     ASP B    43
REMARK 465     PRO B    44
REMARK 465     ALA B    45
REMARK 465     LYS B    46
REMARK 465     PRO B    47
REMARK 465     ASP B    48
REMARK 465     LYS B    49
REMARK 465     ASP B    50
REMARK 465     PHE B    51
REMARK 465     ALA B    52
REMARK 465     ARG B    53
REMARK 465     GLY B    99
REMARK 465     GLU B   100
REMARK 465     VAL B   101
REMARK 465     ASP B   144
REMARK 465     THR B   145
REMARK 465     GLU B   146
REMARK 465     ASP B   147
REMARK 465     LYS B   148
REMARK 465     ARG B   149
REMARK 465     ASP B   150
REMARK 465     GLU B   151
REMARK 465     ARG B   152
REMARK 465     GLY B   153
REMARK 465     GLU B   154
REMARK 465     ALA B   155
REMARK 465     ARG B   156
REMARK 465     VAL B   157
REMARK 465     LEU B   158
REMARK 465     THR B   159
REMARK 465     ARG B   160
REMARK 465     PRO B   161
REMARK 465     VAL B   162
REMARK 465     TYR B   163
REMARK 465     ARG B   164
REMARK 465     ALA B   165
REMARK 465     ASN B   166
REMARK 465     GLY B   167
REMARK 465     ALA B   168
REMARK 465     ASP B   169
REMARK 465     TRP B   170
REMARK 465     LEU B   171
REMARK 465     PRO B   172
REMARK 465     GLU B   173
REMARK 465     ASP B   237
REMARK 465     ALA B   238
REMARK 465     PRO B   239
REMARK 465     ALA B   240
REMARK 465     ALA B   241
REMARK 465     GLY C     0
REMARK 465     SER C     1
REMARK 465     ASN C     2
REMARK 465     ASN C     3
REMARK 465     SER C     4
REMARK 465     GLU C     5
REMARK 465     THR C     6
REMARK 465     PRO C     7
REMARK 465     SER C    40
REMARK 465     GLU C    41
REMARK 465     GLU C    42
REMARK 465     ASP C    43
REMARK 465     PRO C    44
REMARK 465     ALA C    45
REMARK 465     LYS C    46
REMARK 465     PRO C    47
REMARK 465     ASP C    48
REMARK 465     LYS C    49
REMARK 465     ASP C    50
REMARK 465     PHE C    51
REMARK 465     ALA C    52
REMARK 465     ARG C    53
REMARK 465     GLY C    99
REMARK 465     GLU C   100
REMARK 465     ASP C   144
REMARK 465     THR C   145
REMARK 465     GLU C   146
REMARK 465     ASP C   147
REMARK 465     LYS C   148
REMARK 465     ARG C   149
REMARK 465     ASP C   150
REMARK 465     GLU C   151
REMARK 465     ARG C   152
REMARK 465     GLY C   153
REMARK 465     GLU C   154
REMARK 465     ALA C   155
REMARK 465     ARG C   156
REMARK 465     VAL C   157
REMARK 465     LEU C   158
REMARK 465     THR C   159
REMARK 465     ARG C   160
REMARK 465     PRO C   161
REMARK 465     VAL C   162
REMARK 465     TYR C   163
REMARK 465     ARG C   164
REMARK 465     ALA C   165
REMARK 465     ASN C   166
REMARK 465     GLY C   167
REMARK 465     ALA C   168
REMARK 465     ASP C   169
REMARK 465     TRP C   170
REMARK 465     LEU C   171
REMARK 465     PRO C   172
REMARK 465     GLU C   173
REMARK 465     GLU C   216
REMARK 465     ASP C   217
REMARK 465     ASP C   237
REMARK 465     ALA C   238
REMARK 465     PRO C   239
REMARK 465     ALA C   240
REMARK 465     ALA C   241
REMARK 465     GLY D     0
REMARK 465     SER D     1
REMARK 465     ASN D     2
REMARK 465     ASN D     3
REMARK 465     SER D     4
REMARK 465     GLU D     5
REMARK 465     THR D     6
REMARK 465     SER D    40
REMARK 465     GLU D    41
REMARK 465     GLU D    42
REMARK 465     ASP D    43
REMARK 465     PRO D    44
REMARK 465     ALA D    45
REMARK 465     LYS D    46
REMARK 465     PRO D    47
REMARK 465     ASP D    48
REMARK 465     LYS D    49
REMARK 465     ASP D    50
REMARK 465     PHE D    51
REMARK 465     ALA D    52
REMARK 465     ARG D    53
REMARK 465     ALA D    98
REMARK 465     GLY D    99
REMARK 465     GLU D   100
REMARK 465     VAL D   101
REMARK 465     ALA D   143
REMARK 465     ASP D   144
REMARK 465     THR D   145
REMARK 465     GLU D   146
REMARK 465     ASP D   147
REMARK 465     LYS D   148
REMARK 465     ARG D   149
REMARK 465     ASP D   150
REMARK 465     GLU D   151
REMARK 465     ARG D   152
REMARK 465     GLY D   153
REMARK 465     GLU D   154
REMARK 465     ALA D   155
REMARK 465     ARG D   156
REMARK 465     VAL D   157
REMARK 465     LEU D   158
REMARK 465     THR D   159
REMARK 465     ARG D   160
REMARK 465     PRO D   161
REMARK 465     VAL D   162
REMARK 465     TYR D   163
REMARK 465     ARG D   164
REMARK 465     ALA D   165
REMARK 465     ASN D   166
REMARK 465     GLY D   167
REMARK 465     ALA D   168
REMARK 465     ASP D   169
REMARK 465     TRP D   170
REMARK 465     LEU D   171
REMARK 465     PRO D   172
REMARK 465     GLU D   173
REMARK 465     GLU D   216
REMARK 465     ASP D   217
REMARK 465     ALA D   236
REMARK 465     ASP D   237
REMARK 465     ALA D   238
REMARK 465     PRO D   239
REMARK 465     ALA D   240
REMARK 470
REMARK 470 MISSING ATOM
REMARK 470 THE FOLLOWING RESIDUES HAVE MISSING ATOMS (M=MODEL NUMBER;
REMARK 470 RES=RESIDUE NAME; C=CHAIN IDENTIFIER; SSEQ=SEQUENCE NUMBER;
REMARK 470 I=INSERTION CODE):
REMARK 470   M RES CSSEQI  ATOMS
REMARK 470     ARG A  78    CG   CD   NE   CZ   NH1  NH2
REMARK 470     LYS A 102    CG   CD   CE   NZ
REMARK 470     LYS A 122    CG   CD   CE   NZ
REMARK 470     ARG A 174    CG   CD   NE   CZ   NH1  NH2
REMARK 470     GLU A 184    CG   CD   OE1  OE2
REMARK 470     LYS A 187    CG   CD   CE   NZ
REMARK 470     GLU A 195    CG   CD   OE1  OE2
REMARK 470     GLU A 216    CG   CD   OE1  OE2
REMARK 470     GLU A 218    CG   CD   OE1  OE2
REMARK 470     TRP A 219    CG   CD1  CD2  NE1  CE2  CE3  CZ2
REMARK 470     TRP A 219    CZ3  CH2
REMARK 470     GLN A 220    CG   CD   OE1  NE2
REMARK 470     TRP A 224    CG   CD1  CD2  NE1  CE2  CE3  CZ2
REMARK 470     TRP A 224    CZ3  CH2
REMARK 470     GLN A 243    CG   CD   OE1  NE2
REMARK 470     LYS A 273    CG   CD   CE   NZ
REMARK 470     GLU A 285    CG   CD   OE1  OE2
REMARK 470     ASN A 286    CG   OD1  ND2
REMARK 470     GLN A 288    CG   CD   OE1  NE2
REMARK 470     LYS A 347    CG   CD   CE   NZ
REMARK 470     ARG A 554    CG   CD   NE   CZ   NH1  NH2
REMARK 470     ARG A 566    CG   CD   NE   CZ   NH1  NH2
REMARK 470     GLU B  64    CG   CD   OE1  OE2
REMARK 470     ARG B  78    CG   CD   NE   CZ   NH1  NH2
REMARK 470     LYS B 102    CG   CD   CE   NZ
REMARK 470     LYS B 122    CG   CD   CE   NZ
REMARK 470     ARG B 174    CG   CD   NE   CZ   NH1  NH2
REMARK 470     GLU B 184    CG   CD   OE1  OE2
REMARK 470     LYS B 187    CG   CD   CE   NZ
REMARK 470     GLU B 195    CG   CD   OE1  OE2
REMARK 470     GLU B 216    CG   CD   OE1  OE2
REMARK 470     ASP B 217    CG   OD1  OD2
REMARK 470     GLU B 218    CG   CD   OE1  OE2
REMARK 470     TRP B 219    CG   CD1  CD2  NE1  CE2  CE3  CZ2
REMARK 470     TRP B 219    CZ3  CH2
REMARK 470     GLN B 220    CG   CD   OE1  NE2
REMARK 470     TRP B 224    CG   CD1  CD2  NE1  CE2  CE3  CZ2
REMARK 470     TRP B 224    CZ3  CH2
REMARK 470     GLN B 243    CG   CD   OE1  NE2
REMARK 470     LYS B 273    CG   CD   CE   NZ
REMARK 470     GLU B 285    CG   CD   OE1  OE2
REMARK 470     GLN B 288    CG   CD   OE1  NE2
REMARK 470     LYS B 347    CG   CD   CE   NZ
REMARK 470     GLU B 421    CG   CD   OE1  OE2
REMARK 470     ARG B 554    CG   CD   NE   CZ   NH1  NH2
REMARK 470     ARG B 566    CG   CD   NE   CZ   NH1  NH2
REMARK 470     GLU C  64    CG   CD   OE1  OE2
REMARK 470     LYS C 102    CG   CD   CE   NZ
REMARK 470     LYS C 111    CG   CD   CE   NZ
REMARK 470     LYS C 122    CG   CD   CE   NZ
REMARK 470     ARG C 174    CG   CD   NE   CZ   NH1  NH2
REMARK 470     GLU C 184    CG   CD   OE1  OE2
REMARK 470     LYS C 187    CG   CD   CE   NZ
REMARK 470     GLU C 195    CG   CD   OE1  OE2
REMARK 470     GLU C 218    CG   CD   OE1  OE2
REMARK 470     TRP C 219    CG   CD1  CD2  NE1  CE2  CE3  CZ2
REMARK 470     TRP C 219    CZ3  CH2
REMARK 470     GLN C 223    CG   CD   OE1  NE2
REMARK 470     TRP C 224    CG   CD1  CD2  NE1  CE2  CE3  CZ2
REMARK 470     TRP C 224    CZ3  CH2
REMARK 470     GLN C 243    CG   CD   OE1  NE2
REMARK 470     LYS C 244    CG   CD   CE   NZ
REMARK 470     ASP C 247    CG   OD1  OD2
REMARK 470     LYS C 273    CG   CD   CE   NZ
REMARK 470     LYS C 347    CG   CD   CE   NZ
REMARK 470     ARG C 399    CG   CD   NE   CZ   NH1  NH2
REMARK 470     GLU C 421    CG   CD   OE1  OE2
REMARK 470     GLU C 423    CG   CD   OE1  OE2
REMARK 470     ARG C 554    CG   CD   NE   CZ   NH1  NH2
REMARK 470     ARG C 599    CG   CD   NE   CZ   NH1  NH2
REMARK 470     LYS C 614    CG   CD   CE   NZ
REMARK 470     LYS D  30    CG   CD   CE   NZ
REMARK 470     GLU D  64    CG   CD   OE1  OE2
REMARK 470     ARG D  78    CG   CD   NE   CZ   NH1  NH2
REMARK 470     LYS D 102    CG   CD   CE   NZ
REMARK 470     LYS D 111    CG   CD   CE   NZ
REMARK 470     LYS D 122    CG   CD   CE   NZ
REMARK 470     ARG D 174    CG   CD   NE   CZ   NH1  NH2
REMARK 470     GLU D 184    CG   CD   OE1  OE2
REMARK 470     LYS D 187    CG   CD   CE   NZ
REMARK 470     GLU D 195    CG   CD   OE1  OE2
REMARK 470     ARG D 208    CG   CD   NE   CZ   NH1  NH2
REMARK 470     GLU D 218    CG   CD   OE1  OE2
REMARK 470     TRP D 219    CG   CD1  CD2  NE1  CE2  CE3  CZ2
REMARK 470     TRP D 219    CZ3  CH2
REMARK 470     GLN D 223    CG   CD   OE1  NE2
REMARK 470     TRP D 224    CG   CD1  CD2  NE1  CE2  CE3  CZ2
REMARK 470     TRP D 224    CZ3  CH2
REMARK 470     ARG D 225    CG   CD   NE   CZ   NH1  NH2
REMARK 470     GLN D 243    CG   CD   OE1  NE2
REMARK 470     ASP D 247    CG   OD1  OD2
REMARK 470     LYS D 273    CG   CD   CE   NZ
REMARK 470     LYS D 347    CG   CD   CE   NZ
REMARK 470     ARG D 376    CG   CD   NE   CZ   NH1  NH2
REMARK 470     GLU D 400    CG   CD   OE1  OE2
REMARK 470     GLU D 421    CG   CD   OE1  OE2
REMARK 470     GLU D 423    CG   CD   OE1  OE2
REMARK 470     LYS D 425    CG   CD   CE   NZ
REMARK 470     ARG D 554    CG   CD   NE   CZ   NH1  NH2
REMARK 470     ARG D 599    CG   CD   NE   CZ   NH1  NH2
REMARK 500
REMARK 500 GEOMETRY AND STEREOCHEMISTRY
REMARK 500 SUBTOPIC: COVALENT BOND ANGLES
REMARK 500
REMARK 500 THE STEREOCHEMICAL PARAMETERS OF THE FOLLOWING RESIDUES
REMARK 500 HAVE VALUES WHICH DEVIATE FROM EXPECTED VALUES BY MORE
REMARK 500 THAN 6*RMSD (M=MODEL NUMBER; RES=RESIDUE NAME; C=CHAIN
REMARK 500 IDENTIFIER; SSEQ=SEQUENCE NUMBER; I=INSERTION CODE).
REMARK 500
REMARK 500 STANDARD TABLE:
REMARK 500 FORMAT: (10X,I3,1X,A3,1X,A1,I4,A1,3(1X,A4,2X),12X,F5.1)
REMARK 500
REMARK 500 EXPECTED VALUES PROTEIN: ENGH AND HUBER, 1999
REMARK 500 EXPECTED VALUES NUCLEIC ACID: CLOWNEY ET AL 1996
REMARK 500
REMARK 500  M RES CSSEQI ATM1   ATM2   ATM3
REMARK 500    LEU B 266   CA  -  CB  -  CG  ANGL. DEV. =  14.9 DEGREES
REMARK 500
REMARK 500 REMARK: NULL
REMARK 500
REMARK 500 GEOMETRY AND STEREOCHEMISTRY
REMARK 500 SUBTOPIC: TORSION ANGLES
REMARK 500
REMARK 500 TORSION ANGLES OUTSIDE THE EXPECTED RAMACHANDRAN REGIONS:
REMARK 500 (M=MODEL NUMBER; RES=RESIDUE NAME; C=CHAIN IDENTIFIER;
REMARK 500 SSEQ=SEQUENCE NUMBER; I=INSERTION CODE).
REMARK 500
REMARK 500 STANDARD TABLE:
REMARK 500 FORMAT:(10X,I3,1X,A3,1X,A1,I4,A1,4X,F7.2,3X,F7.2)
REMARK 500
REMARK 500 EXPECTED VALUES: GJ KLEYWEGT AND TA JONES (1996). PHI/PSI-
REMARK 500 CHOLOGY: RAMACHANDRAN REVISITED. STRUCTURE 4, 1395 - 1400
REMARK 500
REMARK 500  M RES CSSEQI        PSI       PHI
REMARK 500    ALA A 103       78.23   -164.34
REMARK 500    ALA A 240       84.45     73.32
REMARK 500    ARG A 480       50.35   -154.19
REMARK 500    THR A 483      -95.95   -108.58
REMARK 500    ALA A 514     -113.18     55.77
REMARK 500    ALA B 103       72.72   -166.36
REMARK 500    ARG B 189      126.14   -170.55
REMARK 500    THR B 235      -66.91   -125.83
REMARK 500    ARG B 480       51.34   -154.46
REMARK 500    THR B 483      -95.98   -108.91
REMARK 500    ALA B 514     -113.00     55.38
REMARK 500    ALA C 103       78.37   -163.11
REMARK 500    THR C 235      -77.49   -130.56
REMARK 500    ARG C 480       50.68   -151.48
REMARK 500    THR C 483      -94.75   -108.50
REMARK 500    ALA C 514     -114.67     56.23
REMARK 500    ALA D 103       77.64   -162.99
REMARK 500    ARG D 480       50.89   -152.45
REMARK 500    THR D 483      -95.35   -108.88
REMARK 500    ALA D 514     -113.72     56.37
REMARK 500
REMARK 500 REMARK: NULL
REMARK 800
REMARK 800 SITE
REMARK 800 SITE_IDENTIFIER: AC1
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: binding site for residue GOL A 701
REMARK 800
REMARK 800 SITE_IDENTIFIER: AC2
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: binding site for residue GOL A 702
REMARK 900
REMARK 900 RELATED ENTRIES
REMARK 900 RELATED ID: 5YZO   RELATED DB: PDB
REMARK 900 5YZO CONTAINS THE SAME PROTEIN CRYSTALLIZED IN INACTIVE STATE
DBREF  6IGR A    2   655  UNP    Q9RXY9   Q9RXY9_DEIRA     2    655
DBREF  6IGR B    2   655  UNP    Q9RXY9   Q9RXY9_DEIRA     2    655
DBREF  6IGR C    2   655  UNP    Q9RXY9   Q9RXY9_DEIRA     2    655
DBREF  6IGR D    2   655  UNP    Q9RXY9   Q9RXY9_DEIRA     2    655
SEQADV 6IGR GLY A    0  UNP  Q9RXY9              EXPRESSION TAG
SEQADV 6IGR SER A    1  UNP  Q9RXY9              EXPRESSION TAG
SEQADV 6IGR ALA A  514  UNP  Q9RXY9    SER   514 ENGINEERED MUTATION
SEQADV 6IGR GLY B    0  UNP  Q9RXY9              EXPRESSION TAG
SEQADV 6IGR SER B    1  UNP  Q9RXY9              EXPRESSION TAG
SEQADV 6IGR ALA B  514  UNP  Q9RXY9    SER   514 ENGINEERED MUTATION
SEQADV 6IGR GLY C    0  UNP  Q9RXY9              EXPRESSION TAG
SEQADV 6IGR SER C    1  UNP  Q9RXY9              EXPRESSION TAG
SEQADV 6IGR ALA C  514  UNP  Q9RXY9    SER   514 ENGINEERED MUTATION
SEQADV 6IGR GLY D    0  UNP  Q9RXY9              EXPRESSION TAG
SEQADV 6IGR SER D    1  UNP  Q9RXY9              EXPRESSION TAG
SEQADV 6IGR ALA D  514  UNP  Q9RXY9    SER   514 ENGINEERED MUTATION
SEQRES   1 A  656  GLY SER ASN ASN SER GLU THR PRO ALA PRO GLY PRO ASP
SEQRES   2 A  656  SER LEU LEU ALA LEU ALA PHE PRO SER ASP PRO GLN VAL
SEQRES   3 A  656  SER PRO ASP GLY LYS GLN VAL ALA PHE VAL LEU ALA GLN
SEQRES   4 A  656  ILE SER GLU GLU ASP PRO ALA LYS PRO ASP LYS ASP PHE
SEQRES   5 A  656  ALA ARG PRO ARG TYR ARG SER GLY LEU TRP LEU SER GLU
SEQRES   6 A  656  GLY GLY ALA ALA ARG PRO LEU THR HIS ALA GLU THR GLY
SEQRES   7 A  656  ARG GLY ASP SER ALA PRO ARG TRP SER PRO ASP GLY GLN
SEQRES   8 A  656  ASN LEU ALA PHE VAL ARG SER ALA GLY GLU VAL LYS ALA
SEQRES   9 A  656  ALA LEU MET LEU LEU PRO LEU LYS GLY GLY GLU ALA ARG
SEQRES  10 A  656  ARG VAL THR HIS PHE LYS ASN GLY VAL SER GLY PRO GLN
SEQRES  11 A  656  TRP SER PRO ASP GLY ARG PHE ILE ALA PHE THR THR THR
SEQRES  12 A  656  ALA ASP THR GLU ASP LYS ARG ASP GLU ARG GLY GLU ALA
SEQRES  13 A  656  ARG VAL LEU THR ARG PRO VAL TYR ARG ALA ASN GLY ALA
SEQRES  14 A  656  ASP TRP LEU PRO GLU ARG PRO ALA ALA LEU TRP LEU TYR
SEQRES  15 A  656  ASP VAL GLU ALA ASP LYS LEU ARG GLU TRP TYR ALA PRO
SEQRES  16 A  656  GLU ILE GLY ILE GLY ALA LEU SER TRP TRP PRO ASP SER
SEQRES  17 A  656  ARG GLY VAL LEU ILE VAL GLN SER GLU ASP GLU TRP GLN
SEQRES  18 A  656  ALA SER GLN TRP ARG GLN ASP VAL TYR ASP LEU PRO LEU
SEQRES  19 A  656  PRO THR ALA ASP ALA PRO ALA ALA PRO GLN LYS LEU LEU
SEQRES  20 A  656  ASP TRP ASN SER ALA ALA HIS GLY LEU ALA PRO HIS PRO
SEQRES  21 A  656  ASP GLY GLN ARG PHE ALA LEU ILE GLY ARG PRO ALA GLY
SEQRES  22 A  656  LYS GLY ASN THR GLU HIS ALA HIS LEU TYR LEU ILE GLU
SEQRES  23 A  656  ASN GLY GLN HIS ARG ARG LEU ASP THR GLY HIS ASP HIS
SEQRES  24 A  656  PRO VAL GLY ASP ALA VAL GLY GLY ASP CYS HIS VAL GLY
SEQRES  25 A  656  ALA PHE PRO GLU GLY PRO ARG TRP LEU ASP GLY ASP THR
SEQRES  26 A  656  LEU LEU PHE SER SER THR VAL ARG GLY SER VAL GLY LEU
SEQRES  27 A  656  PHE THR ALA HIS ILE GLY GLY GLY VAL LYS ALA TYR ASP
SEQRES  28 A  656  HIS ASP PRO GLN GLY VAL ILE SER ALA PHE THR ALA ASN
SEQRES  29 A  656  GLU HIS GLY VAL ALA LEU ILE ARG GLU SER ALA THR ARG
SEQRES  30 A  656  PHE PRO GLU VAL GLU LEU ASN GLY GLN ARG VAL THR ASP
SEQRES  31 A  656  LEU HIS ALA ARG PHE PRO PHE PRO VAL ARG GLU PRO GLN
SEQRES  32 A  656  ARG VAL THR PHE GLU THR GLU LEU GLY GLU GLY GLU GLY
SEQRES  33 A  656  TRP VAL LEU LEU PRO GLU GLY GLU GLN LYS VAL PRO ALA
SEQRES  34 A  656  LEU LEU ASN ILE HIS GLY GLY PRO HIS THR ASP TYR GLY
SEQRES  35 A  656  HIS GLY PHE THR HIS GLU PHE GLN LEU MET ALA ALA ARG
SEQRES  36 A  656  GLY TYR GLY VAL CYS TYR SER ASN PRO ARG GLY SER VAL
SEQRES  37 A  656  GLY TYR GLY GLN ALA TRP VAL ASP ALA ILE TYR GLY ARG
SEQRES  38 A  656  TRP GLY THR VAL ASP ALA ASP ASP LEU LEU ASN PHE PHE
SEQRES  39 A  656  ASP ARG CYS LEU GLU ALA VAL PRO ARG LEU ASP ALA ALA
SEQRES  40 A  656  LYS THR ALA VAL MET GLY GLY ALA TYR GLY GLY PHE MET
SEQRES  41 A  656  THR ASN TRP ILE THR GLY HIS THR THR ARG PHE GLN ALA
SEQRES  42 A  656  ALA ILE THR ASP ARG CYS ILE SER ASN LEU ILE SER PHE
SEQRES  43 A  656  GLY GLY THR SER ASP ILE GLY LEU ARG PHE TRP ASP ASP
SEQRES  44 A  656  GLU LEU GLY LEU ASP PHE SER ARG ARG ALA ASP ALA LEU
SEQRES  45 A  656  LYS LEU TRP ASP LEU SER PRO LEU GLN TYR VAL GLU ASN
SEQRES  46 A  656  VAL LYS THR PRO THR LEU ILE VAL HIS SER VAL LEU ASP
SEQRES  47 A  656  HIS ARG CYS PRO VAL GLU GLN ALA GLU GLN TRP TYR ALA
SEQRES  48 A  656  ALA LEU HIS LYS HIS GLN VAL PRO VAL ARG PHE VAL ARG
SEQRES  49 A  656  PHE PRO GLU GLU ASN HIS GLU LEU SER ARG SER GLY ARG
SEQRES  50 A  656  PRO ASP ARG ARG LEU THR ARG LEU ASN GLU TYR PHE ALA
SEQRES  51 A  656  TRP LEU GLU ARG TRP LEU
SEQRES   1 B  656  GLY SER ASN ASN SER GLU THR PRO ALA PRO GLY PRO ASP
SEQRES   2 B  656  SER LEU LEU ALA LEU ALA PHE PRO SER ASP PRO GLN VAL
SEQRES   3 B  656  SER PRO ASP GLY LYS GLN VAL ALA PHE VAL LEU ALA GLN
SEQRES   4 B  656  ILE SER GLU GLU ASP PRO ALA LYS PRO ASP LYS ASP PHE
SEQRES   5 B  656  ALA ARG PRO ARG TYR ARG SER GLY LEU TRP LEU SER GLU
SEQRES   6 B  656  GLY GLY ALA ALA ARG PRO LEU THR HIS ALA GLU THR GLY
SEQRES   7 B  656  ARG GLY ASP SER ALA PRO ARG TRP SER PRO ASP GLY GLN
SEQRES   8 B  656  ASN LEU ALA PHE VAL ARG SER ALA GLY GLU VAL LYS ALA
SEQRES   9 B  656  ALA LEU MET LEU LEU PRO LEU LYS GLY GLY GLU ALA ARG
SEQRES  10 B  656  ARG VAL THR HIS PHE LYS ASN GLY VAL SER GLY PRO GLN
SEQRES  11 B  656  TRP SER PRO ASP GLY ARG PHE ILE ALA PHE THR THR THR
SEQRES  12 B  656  ALA ASP THR GLU ASP LYS ARG ASP GLU ARG GLY GLU ALA
SEQRES  13 B  656  ARG VAL LEU THR ARG PRO VAL TYR ARG ALA ASN GLY ALA
SEQRES  14 B  656  ASP TRP LEU PRO GLU ARG PRO ALA ALA LEU TRP LEU TYR
SEQRES  15 B  656  ASP VAL GLU ALA ASP LYS LEU ARG GLU TRP TYR ALA PRO
SEQRES  16 B  656  GLU ILE GLY ILE GLY ALA LEU SER TRP TRP PRO ASP SER
SEQRES  17 B  656  ARG GLY VAL LEU ILE VAL GLN SER GLU ASP GLU TRP GLN
SEQRES  18 B  656  ALA SER GLN TRP ARG GLN ASP VAL TYR ASP LEU PRO LEU
SEQRES  19 B  656  PRO THR ALA ASP ALA PRO ALA ALA PRO GLN LYS LEU LEU
SEQRES  20 B  656  ASP TRP ASN SER ALA ALA HIS GLY LEU ALA PRO HIS PRO
SEQRES  21 B  656  ASP GLY GLN ARG PHE ALA LEU ILE GLY ARG PRO ALA GLY
SEQRES  22 B  656  LYS GLY ASN THR GLU HIS ALA HIS LEU TYR LEU ILE GLU
SEQRES  23 B  656  ASN GLY GLN HIS ARG ARG LEU ASP THR GLY HIS ASP HIS
SEQRES  24 B  656  PRO VAL GLY ASP ALA VAL GLY GLY ASP CYS HIS VAL GLY
SEQRES  25 B  656  ALA PHE PRO GLU GLY PRO ARG TRP LEU ASP GLY ASP THR
SEQRES  26 B  656  LEU LEU PHE SER SER THR VAL ARG GLY SER VAL GLY LEU
SEQRES  27 B  656  PHE THR ALA HIS ILE GLY GLY GLY VAL LYS ALA TYR ASP
SEQRES  28 B  656  HIS ASP PRO GLN GLY VAL ILE SER ALA PHE THR ALA ASN
SEQRES  29 B  656  GLU HIS GLY VAL ALA LEU ILE ARG GLU SER ALA THR ARG
SEQRES  30 B  656  PHE PRO GLU VAL GLU LEU ASN GLY GLN ARG VAL THR ASP
SEQRES  31 B  656  LEU HIS ALA ARG PHE PRO PHE PRO VAL ARG GLU PRO GLN
SEQRES  32 B  656  ARG VAL THR PHE GLU THR GLU LEU GLY GLU GLY GLU GLY
SEQRES  33 B  656  TRP VAL LEU LEU PRO GLU GLY GLU GLN LYS VAL PRO ALA
SEQRES  34 B  656  LEU LEU ASN ILE HIS GLY GLY PRO HIS THR ASP TYR GLY
SEQRES  35 B  656  HIS GLY PHE THR HIS GLU PHE GLN LEU MET ALA ALA ARG
SEQRES  36 B  656  GLY TYR GLY VAL CYS TYR SER ASN PRO ARG GLY SER VAL
SEQRES  37 B  656  GLY TYR GLY GLN ALA TRP VAL ASP ALA ILE TYR GLY ARG
SEQRES  38 B  656  TRP GLY THR VAL ASP ALA ASP ASP LEU LEU ASN PHE PHE
SEQRES  39 B  656  ASP ARG CYS LEU GLU ALA VAL PRO ARG LEU ASP ALA ALA
SEQRES  40 B  656  LYS THR ALA VAL MET GLY GLY ALA TYR GLY GLY PHE MET
SEQRES  41 B  656  THR ASN TRP ILE THR GLY HIS THR THR ARG PHE GLN ALA
SEQRES  42 B  656  ALA ILE THR ASP ARG CYS ILE SER ASN LEU ILE SER PHE
SEQRES  43 B  656  GLY GLY THR SER ASP ILE GLY LEU ARG PHE TRP ASP ASP
SEQRES  44 B  656  GLU LEU GLY LEU ASP PHE SER ARG ARG ALA ASP ALA LEU
SEQRES  45 B  656  LYS LEU TRP ASP LEU SER PRO LEU GLN TYR VAL GLU ASN
SEQRES  46 B  656  VAL LYS THR PRO THR LEU ILE VAL HIS SER VAL LEU ASP
SEQRES  47 B  656  HIS ARG CYS PRO VAL GLU GLN ALA GLU GLN TRP TYR ALA
SEQRES  48 B  656  ALA LEU HIS LYS HIS GLN VAL PRO VAL ARG PHE VAL ARG
SEQRES  49 B  656  PHE PRO GLU GLU ASN HIS GLU LEU SER ARG SER GLY ARG
SEQRES  50 B  656  PRO ASP ARG ARG LEU THR ARG LEU ASN GLU TYR PHE ALA
SEQRES  51 B  656  TRP LEU GLU ARG TRP LEU
SEQRES   1 C  656  GLY SER ASN ASN SER GLU THR PRO ALA PRO GLY PRO ASP
SEQRES   2 C  656  SER LEU LEU ALA LEU ALA PHE PRO SER ASP PRO GLN VAL
SEQRES   3 C  656  SER PRO ASP GLY LYS GLN VAL ALA PHE VAL LEU ALA GLN
SEQRES   4 C  656  ILE SER GLU GLU ASP PRO ALA LYS PRO ASP LYS ASP PHE
SEQRES   5 C  656  ALA ARG PRO ARG TYR ARG SER GLY LEU TRP LEU SER GLU
SEQRES   6 C  656  GLY GLY ALA ALA ARG PRO LEU THR HIS ALA GLU THR GLY
SEQRES   7 C  656  ARG GLY ASP SER ALA PRO ARG TRP SER PRO ASP GLY GLN
SEQRES   8 C  656  ASN LEU ALA PHE VAL ARG SER ALA GLY GLU VAL LYS ALA
SEQRES   9 C  656  ALA LEU MET LEU LEU PRO LEU LYS GLY GLY GLU ALA ARG
SEQRES  10 C  656  ARG VAL THR HIS PHE LYS ASN GLY VAL SER GLY PRO GLN
SEQRES  11 C  656  TRP SER PRO ASP GLY ARG PHE ILE ALA PHE THR THR THR
SEQRES  12 C  656  ALA ASP THR GLU ASP LYS ARG ASP GLU ARG GLY GLU ALA
SEQRES  13 C  656  ARG VAL LEU THR ARG PRO VAL TYR ARG ALA ASN GLY ALA
SEQRES  14 C  656  ASP TRP LEU PRO GLU ARG PRO ALA ALA LEU TRP LEU TYR
SEQRES  15 C  656  ASP VAL GLU ALA ASP LYS LEU ARG GLU TRP TYR ALA PRO
SEQRES  16 C  656  GLU ILE GLY ILE GLY ALA LEU SER TRP TRP PRO ASP SER
SEQRES  17 C  656  ARG GLY VAL LEU ILE VAL GLN SER GLU ASP GLU TRP GLN
SEQRES  18 C  656  ALA SER GLN TRP ARG GLN ASP VAL TYR ASP LEU PRO LEU
SEQRES  19 C  656  PRO THR ALA ASP ALA PRO ALA ALA PRO GLN LYS LEU LEU
SEQRES  20 C  656  ASP TRP ASN SER ALA ALA HIS GLY LEU ALA PRO HIS PRO
SEQRES  21 C  656  ASP GLY GLN ARG PHE ALA LEU ILE GLY ARG PRO ALA GLY
SEQRES  22 C  656  LYS GLY ASN THR GLU HIS ALA HIS LEU TYR LEU ILE GLU
SEQRES  23 C  656  ASN GLY GLN HIS ARG ARG LEU ASP THR GLY HIS ASP HIS
SEQRES  24 C  656  PRO VAL GLY ASP ALA VAL GLY GLY ASP CYS HIS VAL GLY
SEQRES  25 C  656  ALA PHE PRO GLU GLY PRO ARG TRP LEU ASP GLY ASP THR
SEQRES  26 C  656  LEU LEU PHE SER SER THR VAL ARG GLY SER VAL GLY LEU
SEQRES  27 C  656  PHE THR ALA HIS ILE GLY GLY GLY VAL LYS ALA TYR ASP
SEQRES  28 C  656  HIS ASP PRO GLN GLY VAL ILE SER ALA PHE THR ALA ASN
SEQRES  29 C  656  GLU HIS GLY VAL ALA LEU ILE ARG GLU SER ALA THR ARG
SEQRES  30 C  656  PHE PRO GLU VAL GLU LEU ASN GLY GLN ARG VAL THR ASP
SEQRES  31 C  656  LEU HIS ALA ARG PHE PRO PHE PRO VAL ARG GLU PRO GLN
SEQRES  32 C  656  ARG VAL THR PHE GLU THR GLU LEU GLY GLU GLY GLU GLY
SEQRES  33 C  656  TRP VAL LEU LEU PRO GLU GLY GLU GLN LYS VAL PRO ALA
SEQRES  34 C  656  LEU LEU ASN ILE HIS GLY GLY PRO HIS THR ASP TYR GLY
SEQRES  35 C  656  HIS GLY PHE THR HIS GLU PHE GLN LEU MET ALA ALA ARG
SEQRES  36 C  656  GLY TYR GLY VAL CYS TYR SER ASN PRO ARG GLY SER VAL
SEQRES  37 C  656  GLY TYR GLY GLN ALA TRP VAL ASP ALA ILE TYR GLY ARG
SEQRES  38 C  656  TRP GLY THR VAL ASP ALA ASP ASP LEU LEU ASN PHE PHE
SEQRES  39 C  656  ASP ARG CYS LEU GLU ALA VAL PRO ARG LEU ASP ALA ALA
SEQRES  40 C  656  LYS THR ALA VAL MET GLY GLY ALA TYR GLY GLY PHE MET
SEQRES  41 C  656  THR ASN TRP ILE THR GLY HIS THR THR ARG PHE GLN ALA
SEQRES  42 C  656  ALA ILE THR ASP ARG CYS ILE SER ASN LEU ILE SER PHE
SEQRES  43 C  656  GLY GLY THR SER ASP ILE GLY LEU ARG PHE TRP ASP ASP
SEQRES  44 C  656  GLU LEU GLY LEU ASP PHE SER ARG ARG ALA ASP ALA LEU
SEQRES  45 C  656  LYS LEU TRP ASP LEU SER PRO LEU GLN TYR VAL GLU ASN
SEQRES  46 C  656  VAL LYS THR PRO THR LEU ILE VAL HIS SER VAL LEU ASP
SEQRES  47 C  656  HIS ARG CYS PRO VAL GLU GLN ALA GLU GLN TRP TYR ALA
SEQRES  48 C  656  ALA LEU HIS LYS HIS GLN VAL PRO VAL ARG PHE VAL ARG
SEQRES  49 C  656  PHE PRO GLU GLU ASN HIS GLU LEU SER ARG SER GLY ARG
SEQRES  50 C  656  PRO ASP ARG ARG LEU THR ARG LEU ASN GLU TYR PHE ALA
SEQRES  51 C  656  TRP LEU GLU ARG TRP LEU
SEQRES   1 D  656  GLY SER ASN ASN SER GLU THR PRO ALA PRO GLY PRO ASP
SEQRES   2 D  656  SER LEU LEU ALA LEU ALA PHE PRO SER ASP PRO GLN VAL
SEQRES   3 D  656  SER PRO ASP GLY LYS GLN VAL ALA PHE VAL LEU ALA GLN
SEQRES   4 D  656  ILE SER GLU GLU ASP PRO ALA LYS PRO ASP LYS ASP PHE
SEQRES   5 D  656  ALA ARG PRO ARG TYR ARG SER GLY LEU TRP LEU SER GLU
SEQRES   6 D  656  GLY GLY ALA ALA ARG PRO LEU THR HIS ALA GLU THR GLY
SEQRES   7 D  656  ARG GLY ASP SER ALA PRO ARG TRP SER PRO ASP GLY GLN
SEQRES   8 D  656  ASN LEU ALA PHE VAL ARG SER ALA GLY GLU VAL LYS ALA
SEQRES   9 D  656  ALA LEU MET LEU LEU PRO LEU LYS GLY GLY GLU ALA ARG
SEQRES  10 D  656  ARG VAL THR HIS PHE LYS ASN GLY VAL SER GLY PRO GLN
SEQRES  11 D  656  TRP SER PRO ASP GLY ARG PHE ILE ALA PHE THR THR THR
SEQRES  12 D  656  ALA ASP THR GLU ASP LYS ARG ASP GLU ARG GLY GLU ALA
SEQRES  13 D  656  ARG VAL LEU THR ARG PRO VAL TYR ARG ALA ASN GLY ALA
SEQRES  14 D  656  ASP TRP LEU PRO GLU ARG PRO ALA ALA LEU TRP LEU TYR
SEQRES  15 D  656  ASP VAL GLU ALA ASP LYS LEU ARG GLU TRP TYR ALA PRO
SEQRES  16 D  656  GLU ILE GLY ILE GLY ALA LEU SER TRP TRP PRO ASP SER
SEQRES  17 D  656  ARG GLY VAL LEU ILE VAL GLN SER GLU ASP GLU TRP GLN
SEQRES  18 D  656  ALA SER GLN TRP ARG GLN ASP VAL TYR ASP LEU PRO LEU
SEQRES  19 D  656  PRO THR ALA ASP ALA PRO ALA ALA PRO GLN LYS LEU LEU
SEQRES  20 D  656  ASP TRP ASN SER ALA ALA HIS GLY LEU ALA PRO HIS PRO
SEQRES  21 D  656  ASP GLY GLN ARG PHE ALA LEU ILE GLY ARG PRO ALA GLY
SEQRES  22 D  656  LYS GLY ASN THR GLU HIS ALA HIS LEU TYR LEU ILE GLU
SEQRES  23 D  656  ASN GLY GLN HIS ARG ARG LEU ASP THR GLY HIS ASP HIS
SEQRES  24 D  656  PRO VAL GLY ASP ALA VAL GLY GLY ASP CYS HIS VAL GLY
SEQRES  25 D  656  ALA PHE PRO GLU GLY PRO ARG TRP LEU ASP GLY ASP THR
SEQRES  26 D  656  LEU LEU PHE SER SER THR VAL ARG GLY SER VAL GLY LEU
SEQRES  27 D  656  PHE THR ALA HIS ILE GLY GLY GLY VAL LYS ALA TYR ASP
SEQRES  28 D  656  HIS ASP PRO GLN GLY VAL ILE SER ALA PHE THR ALA ASN
SEQRES  29 D  656  GLU HIS GLY VAL ALA LEU ILE ARG GLU SER ALA THR ARG
SEQRES  30 D  656  PHE PRO GLU VAL GLU LEU ASN GLY GLN ARG VAL THR ASP
SEQRES  31 D  656  LEU HIS ALA ARG PHE PRO PHE PRO VAL ARG GLU PRO GLN
SEQRES  32 D  656  ARG VAL THR PHE GLU THR GLU LEU GLY GLU GLY GLU GLY
SEQRES  33 D  656  TRP VAL LEU LEU PRO GLU GLY GLU GLN LYS VAL PRO ALA
SEQRES  34 D  656  LEU LEU ASN ILE HIS GLY GLY PRO HIS THR ASP TYR GLY
SEQRES  35 D  656  HIS GLY PHE THR HIS GLU PHE GLN LEU MET ALA ALA ARG
SEQRES  36 D  656  GLY TYR GLY VAL CYS TYR SER ASN PRO ARG GLY SER VAL
SEQRES  37 D  656  GLY TYR GLY GLN ALA TRP VAL ASP ALA ILE TYR GLY ARG
SEQRES  38 D  656  TRP GLY THR VAL ASP ALA ASP ASP LEU LEU ASN PHE PHE
SEQRES  39 D  656  ASP ARG CYS LEU GLU ALA VAL PRO ARG LEU ASP ALA ALA
SEQRES  40 D  656  LYS THR ALA VAL MET GLY GLY ALA TYR GLY GLY PHE MET
SEQRES  41 D  656  THR ASN TRP ILE THR GLY HIS THR THR ARG PHE GLN ALA
SEQRES  42 D  656  ALA ILE THR ASP ARG CYS ILE SER ASN LEU ILE SER PHE
SEQRES  43 D  656  GLY GLY THR SER ASP ILE GLY LEU ARG PHE TRP ASP ASP
SEQRES  44 D  656  GLU LEU GLY LEU ASP PHE SER ARG ARG ALA ASP ALA LEU
SEQRES  45 D  656  LYS LEU TRP ASP LEU SER PRO LEU GLN TYR VAL GLU ASN
SEQRES  46 D  656  VAL LYS THR PRO THR LEU ILE VAL HIS SER VAL LEU ASP
SEQRES  47 D  656  HIS ARG CYS PRO VAL GLU GLN ALA GLU GLN TRP TYR ALA
SEQRES  48 D  656  ALA LEU HIS LYS HIS GLN VAL PRO VAL ARG PHE VAL ARG
SEQRES  49 D  656  PHE PRO GLU GLU ASN HIS GLU LEU SER ARG SER GLY ARG
SEQRES  50 D  656  PRO ASP ARG ARG LEU THR ARG LEU ASN GLU TYR PHE ALA
SEQRES  51 D  656  TRP LEU GLU ARG TRP LEU
HET    GOL  A 701       6
HET    GOL  A 702       6
HETNAM     GOL GLYCEROL
HETSYN     GOL GLYCERIN; PROPANE-1,2,3-TRIOL
FORMUL   5  GOL    2(C3 H8 O3)
FORMUL   7  HOH   *369(H2 O)
HELIX    1 AA1 GLY A   10  LEU A   17  5                                   8
HELIX    2 AA2 ASP A  217  GLN A  223  1                                   7
HELIX    3 AA3 LEU A  390  PHE A  394  5                                   5
HELIX    4 AA4 THR A  445  ARG A  454  1                                  10
HELIX    5 AA5 GLY A  470  ALA A  476  1                                   7
HELIX    6 AA6 THR A  483  VAL A  500  1                                  18
HELIX    7 AA7 ALA A  514  GLY A  525  1                                  12
HELIX    8 AA8 ASN A  541  SER A  549  1                                   9
HELIX    9 AA9 ARG A  554  GLY A  561  1                                   8
HELIX   10 AB1 ARG A  566  LEU A  576  1                                  11
HELIX   11 AB2 SER A  577  VAL A  585  5                                   9
HELIX   12 AB3 VAL A  602  HIS A  615  1                                  14
HELIX   13 AB4 HIS A  629  GLY A  635  1                                   7
HELIX   14 AB5 PRO A  637  LEU A  655  1                                  19
HELIX   15 AB6 GLY B   10  LEU B   17  5                                   8
HELIX   16 AB7 ASP B  217  GLN B  223  1                                   7
HELIX   17 AB8 LEU B  390  PHE B  394  5                                   5
HELIX   18 AB9 THR B  445  ARG B  454  1                                  10
HELIX   19 AC1 GLY B  470  ALA B  476  1                                   7
HELIX   20 AC2 THR B  483  VAL B  500  1                                  18
HELIX   21 AC3 ALA B  514  GLY B  525  1                                  12
HELIX   22 AC4 ASN B  541  SER B  549  1                                   9
HELIX   23 AC5 ARG B  554  GLY B  561  1                                   8
HELIX   24 AC6 ARG B  566  LEU B  576  1                                  11
HELIX   25 AC7 SER B  577  VAL B  585  5                                   9
HELIX   26 AC8 VAL B  602  HIS B  615  1                                  14
HELIX   27 AC9 HIS B  629  GLY B  635  1                                   7
HELIX   28 AD1 PRO B  637  LEU B  655  1                                  19
HELIX   29 AD2 GLY C   10  LEU C   17  5                                   8
HELIX   30 AD3 TRP C  219  GLN C  223  1                                   5
HELIX   31 AD4 LEU C  390  PHE C  394  5                                   5
HELIX   32 AD5 THR C  445  ARG C  454  1                                  10
HELIX   33 AD6 GLY C  470  ALA C  476  1                                   7
HELIX   34 AD7 THR C  483  VAL C  500  1                                  18
HELIX   35 AD8 ALA C  514  GLY C  525  1                                  12
HELIX   36 AD9 ASN C  541  SER C  549  1                                   9
HELIX   37 AE1 ILE C  551  GLY C  561  1                                  11
HELIX   38 AE2 ARG C  566  LEU C  576  1                                  11
HELIX   39 AE3 SER C  577  VAL C  585  5                                   9
HELIX   40 AE4 VAL C  602  HIS C  615  1                                  14
HELIX   41 AE5 HIS C  629  GLY C  635  1                                   7
HELIX   42 AE6 PRO C  637  LEU C  655  1                                  19
HELIX   43 AE7 GLY D   10  LEU D   17  5                                   8
HELIX   44 AE8 TRP D  219  GLN D  223  1                                   5
HELIX   45 AE9 LEU D  390  PHE D  394  5                                   5
HELIX   46 AF1 THR D  445  ARG D  454  1                                  10
HELIX   47 AF2 GLY D  470  ALA D  476  1                                   7
HELIX   48 AF3 THR D  483  VAL D  500  1                                  18
HELIX   49 AF4 ALA D  514  GLY D  525  1                                  12
HELIX   50 AF5 ASN D  541  SER D  549  1                                   9
HELIX   51 AF6 ILE D  551  GLY D  561  1                                  11
HELIX   52 AF7 ARG D  566  LEU D  576  1                                  11
HELIX   53 AF8 SER D  577  VAL D  585  5                                   9
HELIX   54 AF9 VAL D  602  HIS D  615  1                                  14
HELIX   55 AG1 HIS D  629  GLY D  635  1                                   7
HELIX   56 AG2 PRO D  637  LEU D  655  1                                  19
SHEET    1 AA1 4 PHE A  19  VAL A  25  0
SHEET    2 AA1 4 VAL A  32  GLN A  38 -1  O  ALA A  33   N  GLN A  24
SHEET    3 AA1 4 ARG A  57  SER A  63 -1  O  TRP A  61   N  PHE A  34
SHEET    4 AA1 4 ARG A  69  PRO A  70 -1  O  ARG A  69   N  LEU A  62
SHEET    1 AA2 4 GLY A  79  TRP A  85  0
SHEET    2 AA2 4 ASN A  91  SER A  97 -1  O  ALA A  93   N  ARG A  84
SHEET    3 AA2 4 ALA A 104  PRO A 109 -1  O  MET A 106   N  PHE A  94
SHEET    4 AA2 4 ARG A 116  ARG A 117 -1  O  ARG A 116   N  LEU A 107
SHEET    1 AA3 4 VAL A 125  TRP A 130  0
SHEET    2 AA3 4 PHE A 136  THR A 141 -1  O  ALA A 138   N  GLN A 129
SHEET    3 AA3 4 ALA A 177  ASP A 182 -1  O  TRP A 179   N  PHE A 139
SHEET    4 AA3 4 LYS A 187  TYR A 192 -1  O  TYR A 192   N  LEU A 178
SHEET    1 AA4 4 LEU A 201  TRP A 203  0
SHEET    2 AA4 4 GLY A 209  GLN A 214 -1  O  LEU A 211   N  SER A 202
SHEET    3 AA4 4 GLN A 226  PRO A 232 -1  O  TYR A 229   N  ILE A 212
SHEET    4 AA4 4 GLN A 243  SER A 250 -1  O  GLN A 243   N  ASP A 230
SHEET    1 AA5 4 ALA A 252  PRO A 257  0
SHEET    2 AA5 4 PHE A 264  GLY A 268 -1  O  ILE A 267   N  HIS A 253
SHEET    3 AA5 4 HIS A 280  GLU A 285 -1  O  ILE A 284   N  PHE A 264
SHEET    4 AA5 4 GLN A 288  ARG A 291 -1  O  ARG A 290   N  LEU A 283
SHEET    1 AA6 4 ARG A 318  TRP A 319  0
SHEET    2 AA6 4 THR A 324  VAL A 331 -1  O  LEU A 326   N  ARG A 318
SHEET    3 AA6 4 SER A 334  HIS A 341 -1  O  ALA A 340   N  LEU A 325
SHEET    4 AA6 4 VAL A 346  ASP A 350 -1  O  ASP A 350   N  LEU A 337
SHEET    1 AA7 4 GLY A 355  ALA A 362  0
SHEET    2 AA7 4 VAL A 367  SER A 373 -1  O  GLU A 372   N  VAL A 356
SHEET    3 AA7 4 ARG A 376  LEU A 382 -1  O  GLU A 381   N  LEU A 369
SHEET    4 AA7 4 GLN A 385  ARG A 386 -1  O  GLN A 385   N  LEU A 382
SHEET    1 AA8 8 GLN A 402  THR A 408  0
SHEET    2 AA8 8 GLY A 411  LEU A 418 -1  O  GLY A 413   N  PHE A 406
SHEET    3 AA8 8 GLY A 457  SER A 461 -1  O  TYR A 460   N  TRP A 416
SHEET    4 AA8 8 VAL A 426  ILE A 432  1  N  LEU A 429   O  GLY A 457
SHEET    5 AA8 8 LEU A 503  GLY A 513  1  O  ASP A 504   N  VAL A 426
SHEET    6 AA8 8 ALA A 532  ASP A 536  1  O  ASP A 536   N  GLY A 512
SHEET    7 AA8 8 THR A 589  SER A 594  1  O  LEU A 590   N  THR A 535
SHEET    8 AA8 8 VAL A 619  PHE A 624  1  O  ARG A 620   N  ILE A 591
SHEET    1 AA9 4 PHE B  19  VAL B  25  0
SHEET    2 AA9 4 VAL B  32  GLN B  38 -1  O  ALA B  33   N  GLN B  24
SHEET    3 AA9 4 ARG B  57  SER B  63 -1  O  TRP B  61   N  PHE B  34
SHEET    4 AA9 4 ARG B  69  PRO B  70 -1  O  ARG B  69   N  LEU B  62
SHEET    1 AB1 4 GLY B  79  TRP B  85  0
SHEET    2 AB1 4 ASN B  91  SER B  97 -1  O  ALA B  93   N  ARG B  84
SHEET    3 AB1 4 ALA B 104  PRO B 109 -1  O  MET B 106   N  PHE B  94
SHEET    4 AB1 4 ARG B 116  ARG B 117 -1  O  ARG B 116   N  LEU B 107
SHEET    1 AB2 4 SER B 126  TRP B 130  0
SHEET    2 AB2 4 PHE B 136  THR B 141 -1  O  ALA B 138   N  GLN B 129
SHEET    3 AB2 4 ALA B 177  ASP B 182 -1  O  TRP B 179   N  PHE B 139
SHEET    4 AB2 4 LYS B 187  TYR B 192 -1  O  TYR B 192   N  LEU B 178
SHEET    1 AB3 4 LEU B 201  TRP B 203  0
SHEET    2 AB3 4 GLY B 209  GLN B 214 -1  O  LEU B 211   N  SER B 202
SHEET    3 AB3 4 GLN B 226  PRO B 232 -1  O  TYR B 229   N  ILE B 212
SHEET    4 AB3 4 GLN B 243  SER B 250 -1  O  GLN B 243   N  ASP B 230
SHEET    1 AB4 4 ALA B 252  PRO B 257  0
SHEET    2 AB4 4 PHE B 264  GLY B 268 -1  O  ILE B 267   N  HIS B 253
SHEET    3 AB4 4 HIS B 280  GLU B 285 -1  O  ILE B 284   N  PHE B 264
SHEET    4 AB4 4 GLN B 288  ARG B 291 -1  O  ARG B 290   N  LEU B 283
SHEET    1 AB5 4 ARG B 318  TRP B 319  0
SHEET    2 AB5 4 THR B 324  VAL B 331 -1  O  LEU B 326   N  ARG B 318
SHEET    3 AB5 4 SER B 334  HIS B 341 -1  O  ALA B 340   N  LEU B 325
SHEET    4 AB5 4 VAL B 346  ASP B 350 -1  O  LYS B 347   N  THR B 339
SHEET    1 AB6 4 GLY B 355  ALA B 362  0
SHEET    2 AB6 4 VAL B 367  SER B 373 -1  O  GLU B 372   N  VAL B 356
SHEET    3 AB6 4 GLU B 379  LEU B 382 -1  O  GLU B 381   N  LEU B 369
SHEET    4 AB6 4 GLN B 385  ARG B 386 -1  O  GLN B 385   N  LEU B 382
SHEET    1 AB7 8 GLN B 402  THR B 408  0
SHEET    2 AB7 8 GLY B 411  LEU B 418 -1  O  GLY B 413   N  PHE B 406
SHEET    3 AB7 8 GLY B 457  SER B 461 -1  O  TYR B 460   N  TRP B 416
SHEET    4 AB7 8 VAL B 426  ILE B 432  1  N  LEU B 429   O  GLY B 457
SHEET    5 AB7 8 LEU B 503  GLY B 513  1  O  ASP B 504   N  VAL B 426
SHEET    6 AB7 8 ALA B 532  ASP B 536  1  O  ASP B 536   N  GLY B 512
SHEET    7 AB7 8 THR B 589  SER B 594  1  O  LEU B 590   N  THR B 535
SHEET    8 AB7 8 VAL B 619  PHE B 624  1  O  ARG B 620   N  ILE B 591
SHEET    1 AB8 4 PHE C  19  VAL C  25  0
SHEET    2 AB8 4 VAL C  32  GLN C  38 -1  O  ALA C  33   N  GLN C  24
SHEET    3 AB8 4 ARG C  57  SER C  63 -1  O  TRP C  61   N  PHE C  34
SHEET    4 AB8 4 ARG C  69  PRO C  70 -1  O  ARG C  69   N  LEU C  62
SHEET    1 AB9 4 GLY C  79  TRP C  85  0
SHEET    2 AB9 4 ASN C  91  SER C  97 -1  O  VAL C  95   N  SER C  81
SHEET    3 AB9 4 ALA C 104  PRO C 109 -1  O  MET C 106   N  PHE C  94
SHEET    4 AB9 4 ARG C 116  ARG C 117 -1  O  ARG C 116   N  LEU C 107
SHEET    1 AC1 4 SER C 126  TRP C 130  0
SHEET    2 AC1 4 PHE C 136  THR C 141 -1  O  ALA C 138   N  GLN C 129
SHEET    3 AC1 4 ALA C 177  ASP C 182 -1  O  TRP C 179   N  PHE C 139
SHEET    4 AC1 4 LYS C 187  TYR C 192 -1  O  LYS C 187   N  ASP C 182
SHEET    1 AC2 4 LEU C 201  TRP C 203  0
SHEET    2 AC2 4 GLY C 209  GLN C 214 -1  O  LEU C 211   N  SER C 202
SHEET    3 AC2 4 GLN C 226  PRO C 232 -1  O  ASP C 227   N  GLN C 214
SHEET    4 AC2 4 GLN C 243  SER C 250 -1  O  LEU C 245   N  VAL C 228
SHEET    1 AC3 4 ALA C 252  PRO C 257  0
SHEET    2 AC3 4 PHE C 264  GLY C 268 -1  O  ILE C 267   N  HIS C 253
SHEET    3 AC3 4 HIS C 280  GLU C 285 -1  O  ILE C 284   N  PHE C 264
SHEET    4 AC3 4 GLN C 288  ARG C 291 -1  O  GLN C 288   N  GLU C 285
SHEET    1 AC4 4 ARG C 318  TRP C 319  0
SHEET    2 AC4 4 THR C 324  VAL C 331 -1  O  LEU C 326   N  ARG C 318
SHEET    3 AC4 4 SER C 334  HIS C 341 -1  O  ALA C 340   N  LEU C 325
SHEET    4 AC4 4 VAL C 346  ASP C 350 -1  O  LYS C 347   N  THR C 339
SHEET    1 AC5 4 GLY C 355  ALA C 362  0
SHEET    2 AC5 4 VAL C 367  SER C 373 -1  O  GLU C 372   N  VAL C 356
SHEET    3 AC5 4 GLU C 379  LEU C 382 -1  O  GLU C 381   N  LEU C 369
SHEET    4 AC5 4 GLN C 385  ARG C 386 -1  O  GLN C 385   N  LEU C 382
SHEET    1 AC6 8 GLN C 402  THR C 408  0
SHEET    2 AC6 8 GLY C 411  LEU C 418 -1  O  GLY C 413   N  PHE C 406
SHEET    3 AC6 8 GLY C 457  SER C 461 -1  O  TYR C 460   N  TRP C 416
SHEET    4 AC6 8 VAL C 426  ILE C 432  1  N  LEU C 429   O  GLY C 457
SHEET    5 AC6 8 LEU C 503  GLY C 513  1  O  ALA C 509   N  LEU C 430
SHEET    6 AC6 8 ALA C 532  ASP C 536  1  O  ASP C 536   N  GLY C 512
SHEET    7 AC6 8 THR C 589  SER C 594  1  O  LEU C 590   N  ALA C 533
SHEET    8 AC6 8 VAL C 619  PHE C 624  1  O  ARG C 620   N  ILE C 591
SHEET    1 AC7 4 PHE D  19  VAL D  25  0
SHEET    2 AC7 4 VAL D  32  GLN D  38 -1  O  ALA D  33   N  GLN D  24
SHEET    3 AC7 4 ARG D  57  SER D  63 -1  O  TRP D  61   N  PHE D  34
SHEET    4 AC7 4 ARG D  69  PRO D  70 -1  O  ARG D  69   N  LEU D  62
SHEET    1 AC8 4 GLY D  79  TRP D  85  0
SHEET    2 AC8 4 ASN D  91  SER D  97 -1  O  VAL D  95   N  SER D  81
SHEET    3 AC8 4 ALA D 104  PRO D 109 -1  O  MET D 106   N  PHE D  94
SHEET    4 AC8 4 ARG D 116  ARG D 117 -1  O  ARG D 116   N  LEU D 107
SHEET    1 AC9 4 SER D 126  TRP D 130  0
SHEET    2 AC9 4 PHE D 136  THR D 141 -1  O  ALA D 138   N  GLN D 129
SHEET    3 AC9 4 ALA D 177  ASP D 182 -1  O  TRP D 179   N  PHE D 139
SHEET    4 AC9 4 LYS D 187  TYR D 192 -1  O  LYS D 187   N  ASP D 182
SHEET    1 AD1 4 ILE D 198  TRP D 203  0
SHEET    2 AD1 4 GLY D 209  GLN D 214 -1  O  VAL D 213   N  GLY D 199
SHEET    3 AD1 4 GLN D 226  PRO D 232 -1  O  ASP D 227   N  GLN D 214
SHEET    4 AD1 4 GLN D 243  SER D 250 -1  O  LEU D 245   N  VAL D 228
SHEET    1 AD2 4 ALA D 252  PRO D 257  0
SHEET    2 AD2 4 PHE D 264  GLY D 268 -1  O  ILE D 267   N  HIS D 253
SHEET    3 AD2 4 HIS D 280  GLU D 285 -1  O  ILE D 284   N  PHE D 264
SHEET    4 AD2 4 GLN D 288  ARG D 291 -1  O  GLN D 288   N  GLU D 285
SHEET    1 AD3 4 ARG D 318  TRP D 319  0
SHEET    2 AD3 4 THR D 324  VAL D 331 -1  O  LEU D 326   N  ARG D 318
SHEET    3 AD3 4 SER D 334  HIS D 341 -1  O  PHE D 338   N  PHE D 327
SHEET    4 AD3 4 VAL D 346  ASP D 350 -1  O  LYS D 347   N  THR D 339
SHEET    1 AD4 4 GLY D 355  ALA D 362  0
SHEET    2 AD4 4 VAL D 367  SER D 373 -1  O  GLU D 372   N  VAL D 356
SHEET    3 AD4 4 GLU D 379  LEU D 382 -1  O  GLU D 381   N  LEU D 369
SHEET    4 AD4 4 GLN D 385  ARG D 386 -1  O  GLN D 385   N  LEU D 382
SHEET    1 AD5 8 GLN D 402  THR D 408  0
SHEET    2 AD5 8 GLY D 411  LEU D 418 -1  O  GLY D 413   N  PHE D 406
SHEET    3 AD5 8 GLY D 457  SER D 461 -1  O  TYR D 460   N  TRP D 416
SHEET    4 AD5 8 VAL D 426  ILE D 432  1  N  LEU D 429   O  GLY D 457
SHEET    5 AD5 8 LEU D 503  GLY D 513  1  O  ASP D 504   N  VAL D 426
SHEET    6 AD5 8 ALA D 532  ASP D 536  1  O  ASP D 536   N  GLY D 512
SHEET    7 AD5 8 THR D 589  SER D 594  1  O  LEU D 590   N  ALA D 533
SHEET    8 AD5 8 VAL D 619  PHE D 624  1  O  ARG D 620   N  ILE D 591
CISPEP   1 GLY A  435    PRO A  436          0         2.01
CISPEP   2 GLY B  435    PRO B  436          0         2.70
CISPEP   3 GLY C  435    PRO C  436          0         2.83
CISPEP   4 GLY D  435    PRO D  436          0         2.53
SITE     1 AC1  3 TRP A  85  TRP A 130  HOH A 841
SITE     1 AC2  5 GLY A 434  GLY A 435  ALA A 514  TYR A 515
SITE     2 AC2  5 ARG A 599
CRYST1   77.415  189.200  121.030  90.00 108.59  90.00 P 1 21 1      8
ORIGX1      1.000000  0.000000  0.000000        0.00000
ORIGX2      0.000000  1.000000  0.000000        0.00000
ORIGX3      0.000000  0.000000  1.000000        0.00000
SCALE1      0.012917  0.000000  0.004345        0.00000
SCALE2      0.000000  0.005285  0.000000        0.00000
SCALE3      0.000000  0.000000  0.008717        0.00000
TER    4607      LEU A 655
TER    9192      LEU B 655
TER   13756      LEU C 655
TER   18288      LEU D 655
MASTER      645    0    2   56  144    0    3    618665    4   12  204
END