longtext: 6rky-pdb

content
HEADER    HYDROLASE                               30-APR-19   6RKY
TITLE     STRUCTURE OF ESTER-HYDROLASE EH1AB1 FROM THE METAGENOME OF LAKE ARREO
TITLE    2 COMPLEXED WITH A DERIVATIVE OF BIPYRIDINE PHOSPHONATE
COMPND    MOL_ID: 1;
COMPND   2 MOLECULE: EH1AB1;
COMPND   3 CHAIN: A, B, C, D;
COMPND   4 ENGINEERED: YES
SOURCE    MOL_ID: 1;
SOURCE   2 ORGANISM_SCIENTIFIC: METAGENOME;
SOURCE   3 ORGANISM_TAXID: 256318;
SOURCE   4 EXPRESSION_SYSTEM: ESCHERICHIA COLI BL21;
SOURCE   5 EXPRESSION_SYSTEM_TAXID: 511693;
SOURCE   6 EXPRESSION_SYSTEM_VECTOR_TYPE: PET-46 EK/LIC
KEYWDS    ESTER HYDROLASE, COMPLEX, HYDROLASE
EXPDTA    X-RAY DIFFRACTION
AUTHOR    I.CEA-RAMA,J.SANZ-APARICIO
REVDAT   1   25-DEC-19 6RKY    0
JRNL        AUTH   S.ALONSO,G.SANTIAGO,I.CEA-RAMA,L.FERNANDEZ-LOPEZ,C.COSCOLIN,
JRNL        AUTH 2 J.MODREGGER,A.RESSMANN,M.MARTINEZ-MARTINEZ,H.MARRERO,
JRNL        AUTH 3 R.BARGIELA,M.PITA,J.L.GONZALEZ-ALFONSO,M.BRIAND,D.ROJO,
JRNL        AUTH 4 C.BARBAS,F.J.PLOU,P.N.GOLYSHIN,P.SHAHGALDIAN,
JRNL        AUTH 5 J.SANZ-APARICIO,V.GUALLAR,M.FERRER
JRNL        TITL   GENETICALLY ENGINEERED PROTEINS WITH TWO ACTIVE SITES FOR
JRNL        TITL 2 ENHANCED BIOCATALYSIS AND SYNERGISTIC CHEMO- AND
JRNL        TITL 3 BIOCATALYSIS
JRNL        REF    NAT CATAL                                  2019
JRNL        REFN                   ESSN 2520-1158
JRNL        DOI    10.1038/S41929-019-0394-4
REMARK   2
REMARK   2 RESOLUTION.    2.79 ANGSTROMS.
REMARK   3
REMARK   3 REFINEMENT.
REMARK   3   PROGRAM     : REFMAC 5.8.0238
REMARK   3   AUTHORS     : MURSHUDOV,SKUBAK,LEBEDEV,PANNU,STEINER,
REMARK   3               : NICHOLLS,WINN,LONG,VAGIN
REMARK   3
REMARK   3    REFINEMENT TARGET : NULL
REMARK   3
REMARK   3  DATA USED IN REFINEMENT.
REMARK   3   RESOLUTION RANGE HIGH (ANGSTROMS) : 2.79
REMARK   3   RESOLUTION RANGE LOW  (ANGSTROMS) : 49.08
REMARK   3   DATA CUTOFF            (SIGMA(F)) : NULL
REMARK   3   COMPLETENESS FOR RANGE        (%) : 99.1
REMARK   3   NUMBER OF REFLECTIONS             : 35315
REMARK   3
REMARK   3  FIT TO DATA USED IN REFINEMENT.
REMARK   3   CROSS-VALIDATION METHOD          : THROUGHOUT
REMARK   3   FREE R VALUE TEST SET SELECTION  : RANDOM
REMARK   3   R VALUE     (WORKING + TEST SET) : 0.241
REMARK   3   R VALUE            (WORKING SET) : 0.239
REMARK   3   FREE R VALUE                     : 0.276
REMARK   3   FREE R VALUE TEST SET SIZE   (%) : 4.900
REMARK   3   FREE R VALUE TEST SET COUNT      : 1823
REMARK   3
REMARK   3  FIT IN THE HIGHEST RESOLUTION BIN.
REMARK   3   TOTAL NUMBER OF BINS USED           : 20
REMARK   3   BIN RESOLUTION RANGE HIGH       (A) : 2.79
REMARK   3   BIN RESOLUTION RANGE LOW        (A) : 2.86
REMARK   3   REFLECTION IN BIN     (WORKING SET) : 2649
REMARK   3   BIN COMPLETENESS (WORKING+TEST) (%) : 99.28
REMARK   3   BIN R VALUE           (WORKING SET) : 0.2640
REMARK   3   BIN FREE R VALUE SET COUNT          : 119
REMARK   3   BIN FREE R VALUE                    : 0.3440
REMARK   3
REMARK   3  NUMBER OF NON-HYDROGEN ATOMS USED IN REFINEMENT.
REMARK   3   PROTEIN ATOMS            : 9628
REMARK   3   NUCLEIC ACID ATOMS       : 0
REMARK   3   HETEROGEN ATOMS          : 64
REMARK   3   SOLVENT ATOMS            : 72
REMARK   3
REMARK   3  B VALUES.
REMARK   3   FROM WILSON PLOT           (A**2) : 51.39
REMARK   3   MEAN B VALUE      (OVERALL, A**2) : 48.36
REMARK   3   OVERALL ANISOTROPIC B VALUE.
REMARK   3    B11 (A**2) : 2.00000
REMARK   3    B22 (A**2) : 1.60000
REMARK   3    B33 (A**2) : -1.47000
REMARK   3    B12 (A**2) : 0.00000
REMARK   3    B13 (A**2) : -2.00000
REMARK   3    B23 (A**2) : 0.00000
REMARK   3
REMARK   3  ESTIMATED OVERALL COORDINATE ERROR.
REMARK   3   ESU BASED ON R VALUE                            (A): NULL
REMARK   3   ESU BASED ON FREE R VALUE                       (A): 0.413
REMARK   3   ESU BASED ON MAXIMUM LIKELIHOOD                 (A): 0.382
REMARK   3   ESU FOR B VALUES BASED ON MAXIMUM LIKELIHOOD (A**2): 18.657
REMARK   3
REMARK   3 CORRELATION COEFFICIENTS.
REMARK   3   CORRELATION COEFFICIENT FO-FC      : 0.910
REMARK   3   CORRELATION COEFFICIENT FO-FC FREE : 0.888
REMARK   3
REMARK   3  RMS DEVIATIONS FROM IDEAL VALUES        COUNT    RMS    WEIGHT
REMARK   3   BOND LENGTHS REFINED ATOMS        (A):  9922 ; 0.007 ; 0.013
REMARK   3   BOND LENGTHS OTHERS               (A):  9028 ; 0.003 ; 0.017
REMARK   3   BOND ANGLES REFINED ATOMS   (DEGREES): 13462 ; 1.476 ; 1.664
REMARK   3   BOND ANGLES OTHERS          (DEGREES): 20824 ; 1.251 ; 1.589
REMARK   3   TORSION ANGLES, PERIOD 1    (DEGREES):  1256 ; 6.533 ; 5.000
REMARK   3   TORSION ANGLES, PERIOD 2    (DEGREES):   544 ;28.698 ;20.515
REMARK   3   TORSION ANGLES, PERIOD 3    (DEGREES):  1432 ;14.826 ;15.000
REMARK   3   TORSION ANGLES, PERIOD 4    (DEGREES):    92 ;18.196 ;15.000
REMARK   3   CHIRAL-CENTER RESTRAINTS       (A**3):  1260 ; 0.076 ; 0.200
REMARK   3   GENERAL PLANES REFINED ATOMS      (A): 11440 ; 0.005 ; 0.020
REMARK   3   GENERAL PLANES OTHERS             (A):  2268 ; 0.001 ; 0.020
REMARK   3   NON-BONDED CONTACTS REFINED ATOMS (A):  NULL ;  NULL ;  NULL
REMARK   3   NON-BONDED CONTACTS OTHERS        (A):  NULL ;  NULL ;  NULL
REMARK   3   NON-BONDED TORSION REFINED ATOMS  (A):  NULL ;  NULL ;  NULL
REMARK   3   NON-BONDED TORSION OTHERS         (A):  NULL ;  NULL ;  NULL
REMARK   3   H-BOND (X...Y) REFINED ATOMS      (A):  NULL ;  NULL ;  NULL
REMARK   3   H-BOND (X...Y) OTHERS             (A):  NULL ;  NULL ;  NULL
REMARK   3   POTENTIAL METAL-ION REFINED ATOMS (A):  NULL ;  NULL ;  NULL
REMARK   3   POTENTIAL METAL-ION OTHERS        (A):  NULL ;  NULL ;  NULL
REMARK   3   SYMMETRY VDW REFINED ATOMS        (A):  NULL ;  NULL ;  NULL
REMARK   3   SYMMETRY VDW OTHERS               (A):  NULL ;  NULL ;  NULL
REMARK   3   SYMMETRY H-BOND REFINED ATOMS     (A):  NULL ;  NULL ;  NULL
REMARK   3   SYMMETRY H-BOND OTHERS            (A):  NULL ;  NULL ;  NULL
REMARK   3   SYMMETRY METAL-ION REFINED ATOMS  (A):  NULL ;  NULL ;  NULL
REMARK   3   SYMMETRY METAL-ION OTHERS         (A):  NULL ;  NULL ;  NULL
REMARK   3
REMARK   3  ISOTROPIC THERMAL FACTOR RESTRAINTS.     COUNT   RMS    WEIGHT
REMARK   3   MAIN-CHAIN BOND REFINED ATOMS  (A**2):  5036 ; 3.846 ; 4.902
REMARK   3   MAIN-CHAIN BOND OTHER ATOMS    (A**2):  5035 ; 3.842 ; 4.901
REMARK   3   MAIN-CHAIN ANGLE REFINED ATOMS (A**2):  6288 ; 5.862 ; 7.355
REMARK   3   MAIN-CHAIN ANGLE OTHER ATOMS   (A**2):  6289 ; 5.863 ; 7.355
REMARK   3   SIDE-CHAIN BOND REFINED ATOMS  (A**2):  4886 ; 4.639 ; 5.498
REMARK   3   SIDE-CHAIN BOND OTHER ATOMS    (A**2):  4887 ; 4.639 ; 5.499
REMARK   3   SIDE-CHAIN ANGLE REFINED ATOMS (A**2):  NULL ;  NULL ;  NULL
REMARK   3   SIDE-CHAIN ANGLE OTHER ATOMS   (A**2):  7175 ; 7.299 ; 8.034
REMARK   3   LONG RANGE B REFINED ATOMS     (A**2): 10513 ; 9.923 ;58.300
REMARK   3   LONG RANGE B OTHER ATOMS       (A**2): 10512 ; 9.919 ;58.303
REMARK   3
REMARK   3 ANISOTROPIC THERMAL FACTOR RESTRAINTS.    COUNT   RMS   WEIGHT
REMARK   3   RIGID-BOND RESTRAINTS          (A**2):  NULL ;  NULL ;  NULL
REMARK   3   SPHERICITY; FREE ATOMS         (A**2):  NULL ;  NULL ;  NULL
REMARK   3   SPHERICITY; BONDED ATOMS       (A**2):  NULL ;  NULL ;  NULL
REMARK   3
REMARK   3  NCS RESTRAINTS STATISTICS
REMARK   3   NCS TYPE: LOCAL
REMARK   3   NUMBER OF DIFFERENT NCS PAIRS  : 6
REMARK   3  GROUP  CHAIN1    RANGE     CHAIN2     RANGE    COUNT RMS  WEIGHT
REMARK   3    1     A     1    315       B     1    315   10234  0.02  0.05
REMARK   3    2     A     1    315       C     1    315   10160  0.02  0.05
REMARK   3    3     A     1    315       D     1    315   10163  0.03  0.05
REMARK   3    4     B     1    315       C     1    315   10176  0.02  0.05
REMARK   3    5     B     1    315       D     1    315   10178  0.03  0.05
REMARK   3    6     C     1    315       D     1    315   10180  0.03  0.05
REMARK   3
REMARK   3  TLS DETAILS
REMARK   3   NUMBER OF TLS GROUPS  : NULL
REMARK   3
REMARK   3  BULK SOLVENT MODELLING.
REMARK   3   METHOD USED : NULL
REMARK   3   PARAMETERS FOR MASK CALCULATION
REMARK   3   VDW PROBE RADIUS   : 1.20
REMARK   3   ION PROBE RADIUS   : 0.80
REMARK   3   SHRINKAGE RADIUS   : 0.80
REMARK   3
REMARK   3  OTHER REFINEMENT REMARKS: HYDROGENS HAVE BEEN ADDED IN THE RIDING
REMARK   3  POSITIONS
REMARK   4
REMARK   4 6RKY COMPLIES WITH FORMAT V. 3.30, 13-JUL-11
REMARK 100
REMARK 100 THIS ENTRY HAS BEEN PROCESSED BY PDBE ON 01-MAY-19.
REMARK 100 THE DEPOSITION ID IS D_1292102071.
REMARK 200
REMARK 200 EXPERIMENTAL DETAILS
REMARK 200  EXPERIMENT TYPE                : X-RAY DIFFRACTION
REMARK 200  DATE OF DATA COLLECTION        : 28-FEB-19
REMARK 200  TEMPERATURE           (KELVIN) : 100
REMARK 200  PH                             : 7.5
REMARK 200  NUMBER OF CRYSTALS USED        : 1
REMARK 200
REMARK 200  SYNCHROTRON              (Y/N) : Y
REMARK 200  RADIATION SOURCE               : ALBA
REMARK 200  BEAMLINE                       : XALOC
REMARK 200  X-RAY GENERATOR MODEL          : NULL
REMARK 200  MONOCHROMATIC OR LAUE    (M/L) : M
REMARK 200  WAVELENGTH OR RANGE        (A) : 0.97926
REMARK 200  MONOCHROMATOR                  : SI(111) CHANNEL-CUT, CRYOCOOLED
REMARK 200  OPTICS                         : KB FOCUSING MIRRORS
REMARK 200
REMARK 200  DETECTOR TYPE                  : PIXEL
REMARK 200  DETECTOR MANUFACTURER          : DECTRIS PILATUS3 S 6M
REMARK 200  INTENSITY-INTEGRATION SOFTWARE : XDS
REMARK 200  DATA SCALING SOFTWARE          : AIMLESS 1.11.17
REMARK 200
REMARK 200  NUMBER OF UNIQUE REFLECTIONS   : 37139
REMARK 200  RESOLUTION RANGE HIGH      (A) : 2.790
REMARK 200  RESOLUTION RANGE LOW       (A) : 49.080
REMARK 200  REJECTION CRITERIA  (SIGMA(I)) : NULL
REMARK 200
REMARK 200 OVERALL.
REMARK 200  COMPLETENESS FOR RANGE     (%) : 99.1
REMARK 200  DATA REDUNDANCY                : 3.800
REMARK 200  R MERGE                    (I) : 0.27700
REMARK 200  R SYM                      (I) : NULL
REMARK 200   FOR THE DATA SET  : 2.7000
REMARK 200
REMARK 200 IN THE HIGHEST RESOLUTION SHELL.
REMARK 200  HIGHEST RESOLUTION SHELL, RANGE HIGH (A) : 2.79
REMARK 200  HIGHEST RESOLUTION SHELL, RANGE LOW  (A) : 2.91
REMARK 200  COMPLETENESS FOR SHELL     (%) : 99.3
REMARK 200  DATA REDUNDANCY IN SHELL       : 3.90
REMARK 200  R MERGE FOR SHELL          (I) : 0.57200
REMARK 200  R SYM FOR SHELL            (I) : NULL
REMARK 200   FOR SHELL         : 1.600
REMARK 200
REMARK 200 DIFFRACTION PROTOCOL: SINGLE WAVELENGTH
REMARK 200 METHOD USED TO DETERMINE THE STRUCTURE: MOLECULAR REPLACEMENT
REMARK 200 SOFTWARE USED: MOLREP 11.6.04
REMARK 200 STARTING MODEL: 6I8F
REMARK 200
REMARK 200 REMARK: PRISM
REMARK 280
REMARK 280 CRYSTAL
REMARK 280 SOLVENT CONTENT, VS   (%): 56.78
REMARK 280 MATTHEWS COEFFICIENT, VM (ANGSTROMS**3/DA): 2.85
REMARK 280
REMARK 280 CRYSTALLIZATION CONDITIONS: 20% PEG 3350, 0.1M BIS-TRIS PROPANE PH
REMARK 280  7.5, 0.2 M NAF, VAPOR DIFFUSION, SITTING DROP, TEMPERATURE 291K
REMARK 290
REMARK 290 CRYSTALLOGRAPHIC SYMMETRY
REMARK 290 SYMMETRY OPERATORS FOR SPACE GROUP: C 1 2 1
REMARK 290
REMARK 290      SYMOP   SYMMETRY
REMARK 290     NNNMMM   OPERATOR
REMARK 290       1555   X,Y,Z
REMARK 290       2555   -X,Y,-Z
REMARK 290       3555   X+1/2,Y+1/2,Z
REMARK 290       4555   -X+1/2,Y+1/2,-Z
REMARK 290
REMARK 290     WHERE NNN -> OPERATOR NUMBER
REMARK 290           MMM -> TRANSLATION VECTOR
REMARK 290
REMARK 290 CRYSTALLOGRAPHIC SYMMETRY TRANSFORMATIONS
REMARK 290 THE FOLLOWING TRANSFORMATIONS OPERATE ON THE ATOM/HETATM
REMARK 290 RECORDS IN THIS ENTRY TO PRODUCE CRYSTALLOGRAPHICALLY
REMARK 290 RELATED MOLECULES.
REMARK 290   SMTRY1   1  1.000000  0.000000  0.000000        0.00000
REMARK 290   SMTRY2   1  0.000000  1.000000  0.000000        0.00000
REMARK 290   SMTRY3   1  0.000000  0.000000  1.000000        0.00000
REMARK 290   SMTRY1   2 -1.000000  0.000000  0.000000        0.00000
REMARK 290   SMTRY2   2  0.000000  1.000000  0.000000        0.00000
REMARK 290   SMTRY3   2  0.000000  0.000000 -1.000000        0.00000
REMARK 290   SMTRY1   3  1.000000  0.000000  0.000000       45.38300
REMARK 290   SMTRY2   3  0.000000  1.000000  0.000000      100.96000
REMARK 290   SMTRY3   3  0.000000  0.000000  1.000000        0.00000
REMARK 290   SMTRY1   4 -1.000000  0.000000  0.000000       45.38300
REMARK 290   SMTRY2   4  0.000000  1.000000  0.000000      100.96000
REMARK 290   SMTRY3   4  0.000000  0.000000 -1.000000        0.00000
REMARK 290
REMARK 290 REMARK: NULL
REMARK 300
REMARK 300 BIOMOLECULE: 1, 2
REMARK 300 SEE REMARK 350 FOR THE AUTHOR PROVIDED AND/OR PROGRAM
REMARK 300 GENERATED ASSEMBLY INFORMATION FOR THE STRUCTURE IN
REMARK 300 THIS ENTRY. THE REMARK MAY ALSO PROVIDE INFORMATION ON
REMARK 300 BURIED SURFACE AREA.
REMARK 350
REMARK 350 COORDINATES FOR A COMPLETE MULTIMER REPRESENTING THE KNOWN
REMARK 350 BIOLOGICALLY SIGNIFICANT OLIGOMERIZATION STATE OF THE
REMARK 350 MOLECULE CAN BE GENERATED BY APPLYING BIOMT TRANSFORMATIONS
REMARK 350 GIVEN BELOW.  BOTH NON-CRYSTALLOGRAPHIC AND
REMARK 350 CRYSTALLOGRAPHIC OPERATIONS ARE GIVEN.
REMARK 350
REMARK 350 BIOMOLECULE: 1
REMARK 350 AUTHOR DETERMINED BIOLOGICAL UNIT: DIMERIC
REMARK 350 SOFTWARE DETERMINED QUATERNARY STRUCTURE: DIMERIC
REMARK 350 SOFTWARE USED: PISA
REMARK 350 TOTAL BURIED SURFACE AREA: 3000 ANGSTROM**2
REMARK 350 SURFACE AREA OF THE COMPLEX: 23260 ANGSTROM**2
REMARK 350 CHANGE IN SOLVENT FREE ENERGY: -1.0 KCAL/MOL
REMARK 350 APPLY THE FOLLOWING TO CHAINS: A, C
REMARK 350   BIOMT1   1  1.000000  0.000000  0.000000        0.00000
REMARK 350   BIOMT2   1  0.000000  1.000000  0.000000        0.00000
REMARK 350   BIOMT3   1  0.000000  0.000000  1.000000        0.00000
REMARK 350
REMARK 350 BIOMOLECULE: 2
REMARK 350 AUTHOR DETERMINED BIOLOGICAL UNIT: DIMERIC
REMARK 350 SOFTWARE DETERMINED QUATERNARY STRUCTURE: DIMERIC
REMARK 350 SOFTWARE USED: PISA
REMARK 350 TOTAL BURIED SURFACE AREA: 2660 ANGSTROM**2
REMARK 350 SURFACE AREA OF THE COMPLEX: 23090 ANGSTROM**2
REMARK 350 CHANGE IN SOLVENT FREE ENERGY: -4.0 KCAL/MOL
REMARK 350 APPLY THE FOLLOWING TO CHAINS: B, D
REMARK 350   BIOMT1   1  1.000000  0.000000  0.000000        0.00000
REMARK 350   BIOMT2   1  0.000000  1.000000  0.000000        0.00000
REMARK 350   BIOMT3   1  0.000000  0.000000  1.000000        0.00000
REMARK 465
REMARK 465 MISSING RESIDUES
REMARK 465 THE FOLLOWING RESIDUES WERE NOT LOCATED IN THE
REMARK 465 EXPERIMENT. (M=MODEL NUMBER; RES=RESIDUE NAME; C=CHAIN
REMARK 465 IDENTIFIER; SSSEQ=SEQUENCE NUMBER; I=INSERTION CODE.)
REMARK 465
REMARK 465   M RES C SSSEQI
REMARK 465     SER A   160A
REMARK 465     SER B   160A
REMARK 465     SER C   160A
REMARK 465     SER D   160A
REMARK 500
REMARK 500 GEOMETRY AND STEREOCHEMISTRY
REMARK 500 SUBTOPIC: TORSION ANGLES
REMARK 500
REMARK 500 TORSION ANGLES OUTSIDE THE EXPECTED RAMACHANDRAN REGIONS:
REMARK 500 (M=MODEL NUMBER; RES=RESIDUE NAME; C=CHAIN IDENTIFIER;
REMARK 500 SSEQ=SEQUENCE NUMBER; I=INSERTION CODE).
REMARK 500
REMARK 500 STANDARD TABLE:
REMARK 500 FORMAT:(10X,I3,1X,A3,1X,A1,I4,A1,4X,F7.2,3X,F7.2)
REMARK 500
REMARK 500 EXPECTED VALUES: GJ KLEYWEGT AND TA JONES (1996). PHI/PSI-
REMARK 500 CHOLOGY: RAMACHANDRAN REVISITED. STRUCTURE 4, 1395 - 1400
REMARK 500
REMARK 500  M RES CSSEQI        PSI       PHI
REMARK 500    ALA A  62       28.35   -154.81
REMARK 500    SER A  63      173.40    172.54
REMARK 500    VAL A  92      -50.46   -126.34
REMARK 500    ASN A  95     -177.06   -172.14
REMARK 500    PHE A 184      145.50   -171.35
REMARK 500    TYR A 189       58.93     34.29
REMARK 500    PHE A 209      -70.34     68.18
REMARK 500    ASP A 228      107.68    -58.16
REMARK 500    TYR A 255       46.41   -108.08
REMARK 500    PRO A 257      -37.01    -39.97
REMARK 500    LEU A 291       47.96    -98.09
REMARK 500    ALA B  62       25.64   -151.38
REMARK 500    SER B  63      173.31    171.56
REMARK 500    VAL B  92      -50.38   -126.58
REMARK 500    ASN B  95     -176.60   -171.90
REMARK 500    PHE B 184      145.30   -170.28
REMARK 500    TYR B 189       60.31     34.43
REMARK 500    PHE B 209      -70.19     69.52
REMARK 500    ASP B 228      108.18    -59.82
REMARK 500    TYR B 255       46.79   -108.05
REMARK 500    LEU B 291       48.38    -98.44
REMARK 500    ALA C  62       34.25   -156.46
REMARK 500    SER C  63      175.29    170.88
REMARK 500    VAL C  92      -50.76   -126.66
REMARK 500    ASN C  95     -176.60   -173.12
REMARK 500    TYR C 189       59.91     34.05
REMARK 500    PHE C 209      -70.47     69.78
REMARK 500    ASP C 228      107.90    -58.71
REMARK 500    TYR C 255       47.48   -108.68
REMARK 500    LEU C 291       48.11    -97.26
REMARK 500    ALA D  62       34.02   -155.53
REMARK 500    SER D  63      175.98    171.24
REMARK 500    VAL D  92      -51.01   -126.42
REMARK 500    ASN D  95     -176.57   -173.07
REMARK 500    TYR D 189       58.87     35.18
REMARK 500    PHE D 209      -70.67     68.11
REMARK 500    ASP D 228      108.34    -58.72
REMARK 500    TYR D 255       48.02   -108.50
REMARK 500    LEU D 291       48.11    -97.96
REMARK 500
REMARK 500 REMARK: NULL
REMARK 800
REMARK 800 SITE
REMARK 800 SITE_IDENTIFIER: AC1
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: binding site for residue GOL A 401
REMARK 800
REMARK 800 SITE_IDENTIFIER: AC2
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: binding site for residue GOL B 401
REMARK 800
REMARK 800 SITE_IDENTIFIER: AC3
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: binding site for residue GOL C 401
REMARK 800
REMARK 800 SITE_IDENTIFIER: AC4
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: binding site for residue GOL C 402
REMARK 800
REMARK 800 SITE_IDENTIFIER: AC5
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: binding site for residue PEG C 403
REMARK 800
REMARK 800 SITE_IDENTIFIER: AC6
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: binding site for residue PEG C 404
REMARK 800
REMARK 800 SITE_IDENTIFIER: AC7
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: binding site for residue PEG C 405
REMARK 800
REMARK 800 SITE_IDENTIFIER: AC8
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: binding site for residue GOL D 401
REMARK 800
REMARK 800 SITE_IDENTIFIER: AC9
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: binding site for residue GOL D 402
REMARK 800
REMARK 800 SITE_IDENTIFIER: AD1
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: binding site for residue PEG D 403
REMARK 800
REMARK 800 SITE_IDENTIFIER: AD2
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: binding site for Di-peptide ASP B 160 and K7K B
REMARK 800  161
REMARK 800
REMARK 800 SITE_IDENTIFIER: AD3
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: binding site for Di-peptide K7K B 161 and ALA B
REMARK 800  162
REMARK 800
REMARK 800 SITE_IDENTIFIER: AD4
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: binding site for Di-peptide ASP C 160 and K7K C
REMARK 800  161
REMARK 800
REMARK 800 SITE_IDENTIFIER: AD5
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: binding site for Di-peptide K7K C 161 and ALA C
REMARK 800  162
REMARK 800
REMARK 800 SITE_IDENTIFIER: AD6
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: binding site for Di-peptide ASP D 160 and K7K D
REMARK 800  161
REMARK 800
REMARK 800 SITE_IDENTIFIER: AD7
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: binding site for Di-peptide K7K D 161 and ALA D
REMARK 800  162
DBREF  6RKY A    1   315  PDB    6RKY     6RKY             1    315
DBREF  6RKY B    1   315  PDB    6RKY     6RKY             1    315
DBREF  6RKY C    1   315  PDB    6RKY     6RKY             1    315
DBREF  6RKY D    1   315  PDB    6RKY     6RKY             1    315
SEQRES   1 A  316  MET LEU LEU PRO GLU THR ARG ASN LEU LEU ASP LEU MET
SEQRES   2 A  316  ASP ALA ALA THR ARG GLY GLY ARG PRO GLY LEU ASP THR
SEQRES   3 A  316  LEU PRO HIS ALA VAL GLY ARG LYS ALA VAL ASP LYS MET
SEQRES   4 A  316  SER GLU ASP GLY GLU ALA ASP PRO PRO GLU VAL ALA GLU
SEQRES   5 A  316  VAL ALA ASN GLY GLY PHE ALA GLY PRO ALA SER GLU ILE
SEQRES   6 A  316  ARG PHE ARG ARG TYR ARG PRO LEU GLY GLU ALA ALA GLY
SEQRES   7 A  316  LEU LEU PRO THR LEU ILE TYR TYR HIS GLY GLY GLY PHE
SEQRES   8 A  316  VAL ILE GLY ASN ILE GLU THR HIS ASP SER THR CYS ARG
SEQRES   9 A  316  ARG LEU ALA ASN LYS SER ARG CYS GLN VAL ILE SER ILE
SEQRES  10 A  316  ASP TYR ARG LEU ALA PRO GLU HIS PRO PHE PRO ALA PRO
SEQRES  11 A  316  ILE ASP ASP GLY ILE ALA ALA PHE ARG HIS ILE ARG ASP
SEQRES  12 A  316  ASN ALA GLU SER PHE GLY ALA ASP ALA ALA ARG LEU ALA
SEQRES  13 A  316  VAL GLY GLY ASP SER K7K ALA GLY GLY ALA MET ALA ALA
SEQRES  14 A  316  VAL VAL CYS GLN ALA CYS ARG ASP ALA GLY GLU THR GLY
SEQRES  15 A  316  PRO ALA PHE GLN MET LEU ILE TYR PRO ALA THR ASP SER
SEQRES  16 A  316  SER ARG GLU SER ALA SER ARG VAL ALA PHE ALA GLU GLY
SEQRES  17 A  316  TYR PHE LEU SER LYS ALA HIS MET ASP TRP PHE TRP GLU
SEQRES  18 A  316  ALA TYR VAL PRO GLU ASP THR ASP LEU THR ASP LEU ARG
SEQRES  19 A  316  LEU SER PRO LEU LEU ALA THR ASP PHE THR GLY LEU PRO
SEQRES  20 A  316  PRO ALA PHE VAL LEU THR ALA GLY TYR ASP PRO LEU ARG
SEQRES  21 A  316  ASP GLU GLY ARG ALA TYR ALA ASP ARG LEU ILE GLU ALA
SEQRES  22 A  316  GLY ILE LYS THR THR TYR VAL ASN TYR PRO GLY THR ILE
SEQRES  23 A  316  HIS GLY PHE PHE SER LEU THR ARG PHE LEU SER GLN GLY
SEQRES  24 A  316  LEU LYS ALA ASN ASP GLU ALA ALA ALA VAL MET GLY ALA
SEQRES  25 A  316  HIS PHE GLY THR
SEQRES   1 B  316  MET LEU LEU PRO GLU THR ARG ASN LEU LEU ASP LEU MET
SEQRES   2 B  316  ASP ALA ALA THR ARG GLY GLY ARG PRO GLY LEU ASP THR
SEQRES   3 B  316  LEU PRO HIS ALA VAL GLY ARG LYS ALA VAL ASP LYS MET
SEQRES   4 B  316  SER GLU ASP GLY GLU ALA ASP PRO PRO GLU VAL ALA GLU
SEQRES   5 B  316  VAL ALA ASN GLY GLY PHE ALA GLY PRO ALA SER GLU ILE
SEQRES   6 B  316  ARG PHE ARG ARG TYR ARG PRO LEU GLY GLU ALA ALA GLY
SEQRES   7 B  316  LEU LEU PRO THR LEU ILE TYR TYR HIS GLY GLY GLY PHE
SEQRES   8 B  316  VAL ILE GLY ASN ILE GLU THR HIS ASP SER THR CYS ARG
SEQRES   9 B  316  ARG LEU ALA ASN LYS SER ARG CYS GLN VAL ILE SER ILE
SEQRES  10 B  316  ASP TYR ARG LEU ALA PRO GLU HIS PRO PHE PRO ALA PRO
SEQRES  11 B  316  ILE ASP ASP GLY ILE ALA ALA PHE ARG HIS ILE ARG ASP
SEQRES  12 B  316  ASN ALA GLU SER PHE GLY ALA ASP ALA ALA ARG LEU ALA
SEQRES  13 B  316  VAL GLY GLY ASP SER K7K ALA GLY GLY ALA MET ALA ALA
SEQRES  14 B  316  VAL VAL CYS GLN ALA CYS ARG ASP ALA GLY GLU THR GLY
SEQRES  15 B  316  PRO ALA PHE GLN MET LEU ILE TYR PRO ALA THR ASP SER
SEQRES  16 B  316  SER ARG GLU SER ALA SER ARG VAL ALA PHE ALA GLU GLY
SEQRES  17 B  316  TYR PHE LEU SER LYS ALA HIS MET ASP TRP PHE TRP GLU
SEQRES  18 B  316  ALA TYR VAL PRO GLU ASP THR ASP LEU THR ASP LEU ARG
SEQRES  19 B  316  LEU SER PRO LEU LEU ALA THR ASP PHE THR GLY LEU PRO
SEQRES  20 B  316  PRO ALA PHE VAL LEU THR ALA GLY TYR ASP PRO LEU ARG
SEQRES  21 B  316  ASP GLU GLY ARG ALA TYR ALA ASP ARG LEU ILE GLU ALA
SEQRES  22 B  316  GLY ILE LYS THR THR TYR VAL ASN TYR PRO GLY THR ILE
SEQRES  23 B  316  HIS GLY PHE PHE SER LEU THR ARG PHE LEU SER GLN GLY
SEQRES  24 B  316  LEU LYS ALA ASN ASP GLU ALA ALA ALA VAL MET GLY ALA
SEQRES  25 B  316  HIS PHE GLY THR
SEQRES   1 C  316  MET LEU LEU PRO GLU THR ARG ASN LEU LEU ASP LEU MET
SEQRES   2 C  316  ASP ALA ALA THR ARG GLY GLY ARG PRO GLY LEU ASP THR
SEQRES   3 C  316  LEU PRO HIS ALA VAL GLY ARG LYS ALA VAL ASP LYS MET
SEQRES   4 C  316  SER GLU ASP GLY GLU ALA ASP PRO PRO GLU VAL ALA GLU
SEQRES   5 C  316  VAL ALA ASN GLY GLY PHE ALA GLY PRO ALA SER GLU ILE
SEQRES   6 C  316  ARG PHE ARG ARG TYR ARG PRO LEU GLY GLU ALA ALA GLY
SEQRES   7 C  316  LEU LEU PRO THR LEU ILE TYR TYR HIS GLY GLY GLY PHE
SEQRES   8 C  316  VAL ILE GLY ASN ILE GLU THR HIS ASP SER THR CYS ARG
SEQRES   9 C  316  ARG LEU ALA ASN LYS SER ARG CYS GLN VAL ILE SER ILE
SEQRES  10 C  316  ASP TYR ARG LEU ALA PRO GLU HIS PRO PHE PRO ALA PRO
SEQRES  11 C  316  ILE ASP ASP GLY ILE ALA ALA PHE ARG HIS ILE ARG ASP
SEQRES  12 C  316  ASN ALA GLU SER PHE GLY ALA ASP ALA ALA ARG LEU ALA
SEQRES  13 C  316  VAL GLY GLY ASP SER K7K ALA GLY GLY ALA MET ALA ALA
SEQRES  14 C  316  VAL VAL CYS GLN ALA CYS ARG ASP ALA GLY GLU THR GLY
SEQRES  15 C  316  PRO ALA PHE GLN MET LEU ILE TYR PRO ALA THR ASP SER
SEQRES  16 C  316  SER ARG GLU SER ALA SER ARG VAL ALA PHE ALA GLU GLY
SEQRES  17 C  316  TYR PHE LEU SER LYS ALA HIS MET ASP TRP PHE TRP GLU
SEQRES  18 C  316  ALA TYR VAL PRO GLU ASP THR ASP LEU THR ASP LEU ARG
SEQRES  19 C  316  LEU SER PRO LEU LEU ALA THR ASP PHE THR GLY LEU PRO
SEQRES  20 C  316  PRO ALA PHE VAL LEU THR ALA GLY TYR ASP PRO LEU ARG
SEQRES  21 C  316  ASP GLU GLY ARG ALA TYR ALA ASP ARG LEU ILE GLU ALA
SEQRES  22 C  316  GLY ILE LYS THR THR TYR VAL ASN TYR PRO GLY THR ILE
SEQRES  23 C  316  HIS GLY PHE PHE SER LEU THR ARG PHE LEU SER GLN GLY
SEQRES  24 C  316  LEU LYS ALA ASN ASP GLU ALA ALA ALA VAL MET GLY ALA
SEQRES  25 C  316  HIS PHE GLY THR
SEQRES   1 D  316  MET LEU LEU PRO GLU THR ARG ASN LEU LEU ASP LEU MET
SEQRES   2 D  316  ASP ALA ALA THR ARG GLY GLY ARG PRO GLY LEU ASP THR
SEQRES   3 D  316  LEU PRO HIS ALA VAL GLY ARG LYS ALA VAL ASP LYS MET
SEQRES   4 D  316  SER GLU ASP GLY GLU ALA ASP PRO PRO GLU VAL ALA GLU
SEQRES   5 D  316  VAL ALA ASN GLY GLY PHE ALA GLY PRO ALA SER GLU ILE
SEQRES   6 D  316  ARG PHE ARG ARG TYR ARG PRO LEU GLY GLU ALA ALA GLY
SEQRES   7 D  316  LEU LEU PRO THR LEU ILE TYR TYR HIS GLY GLY GLY PHE
SEQRES   8 D  316  VAL ILE GLY ASN ILE GLU THR HIS ASP SER THR CYS ARG
SEQRES   9 D  316  ARG LEU ALA ASN LYS SER ARG CYS GLN VAL ILE SER ILE
SEQRES  10 D  316  ASP TYR ARG LEU ALA PRO GLU HIS PRO PHE PRO ALA PRO
SEQRES  11 D  316  ILE ASP ASP GLY ILE ALA ALA PHE ARG HIS ILE ARG ASP
SEQRES  12 D  316  ASN ALA GLU SER PHE GLY ALA ASP ALA ALA ARG LEU ALA
SEQRES  13 D  316  VAL GLY GLY ASP SER K7K ALA GLY GLY ALA MET ALA ALA
SEQRES  14 D  316  VAL VAL CYS GLN ALA CYS ARG ASP ALA GLY GLU THR GLY
SEQRES  15 D  316  PRO ALA PHE GLN MET LEU ILE TYR PRO ALA THR ASP SER
SEQRES  16 D  316  SER ARG GLU SER ALA SER ARG VAL ALA PHE ALA GLU GLY
SEQRES  17 D  316  TYR PHE LEU SER LYS ALA HIS MET ASP TRP PHE TRP GLU
SEQRES  18 D  316  ALA TYR VAL PRO GLU ASP THR ASP LEU THR ASP LEU ARG
SEQRES  19 D  316  LEU SER PRO LEU LEU ALA THR ASP PHE THR GLY LEU PRO
SEQRES  20 D  316  PRO ALA PHE VAL LEU THR ALA GLY TYR ASP PRO LEU ARG
SEQRES  21 D  316  ASP GLU GLY ARG ALA TYR ALA ASP ARG LEU ILE GLU ALA
SEQRES  22 D  316  GLY ILE LYS THR THR TYR VAL ASN TYR PRO GLY THR ILE
SEQRES  23 D  316  HIS GLY PHE PHE SER LEU THR ARG PHE LEU SER GLN GLY
SEQRES  24 D  316  LEU LYS ALA ASN ASP GLU ALA ALA ALA VAL MET GLY ALA
SEQRES  25 D  316  HIS PHE GLY THR
HET    K7K  A 161      28
HET    K7K  B 161      28
HET    K7K  C 161      28
HET    K7K  D 161      28
HET    GOL  A 401       6
HET    GOL  B 401       6
HET    GOL  C 401       6
HET    GOL  C 402       6
HET    PEG  C 403       7
HET    PEG  C 404       7
HET    PEG  C 405       7
HET    GOL  D 401       6
HET    GOL  D 402       6
HET    PEG  D 403       7
HETNAM     K7K 2-AZANYL-3-[HEXYL-[2-(3-OXIDANYLPYRIDIN-2-YL)PYRIDIN-3-
HETNAM   2 K7K  YL]OXY-PHOSPHORYL]OXY-PROPANAL
HETNAM     GOL GLYCEROL
HETNAM     PEG DI(HYDROXYETHYL)ETHER
HETSYN     GOL GLYCERIN; PROPANE-1,2,3-TRIOL
FORMUL   1  K7K    4(C19 H26 N3 O5 P)
FORMUL   5  GOL    6(C3 H8 O3)
FORMUL   9  PEG    4(C4 H10 O3)
FORMUL  15  HOH   *72(H2 O)
HELIX    1 AA1 LEU A    3  GLY A   20  1                                  18
HELIX    2 AA2 GLY A   23  LEU A   27  5                                   5
HELIX    3 AA3 PRO A   28  ASP A   42  1                                  15
HELIX    4 AA4 ASN A   95  THR A   98  5                                   4
HELIX    5 AA5 HIS A   99  ARG A  111  1                                  13
HELIX    6 AA6 PRO A  128  ASP A  143  1                                  16
HELIX    7 AA7 ASN A  144  PHE A  148  5                                   5
HELIX    8 AA8 K7K A  161  ALA A  177  1                                  17
HELIX    9 AA9 SER A  198  PHE A  204  1                                   7
HELIX   10 AB1 SER A  211  VAL A  223  1                                  13
HELIX   11 AB2 SER A  235  ALA A  239  5                                   5
HELIX   12 AB3 LEU A  258  ALA A  272  1                                  15
HELIX   13 AB4 SER A  296  GLY A  314  1                                  19
HELIX   14 AB5 LEU B    3  GLY B   20  1                                  18
HELIX   15 AB6 GLY B   23  LEU B   27  5                                   5
HELIX   16 AB7 PRO B   28  ASP B   42  1                                  15
HELIX   17 AB8 ASN B   95  THR B   98  5                                   4
HELIX   18 AB9 HIS B   99  ARG B  111  1                                  13
HELIX   19 AC1 PRO B  128  ASP B  143  1                                  16
HELIX   20 AC2 ASN B  144  PHE B  148  5                                   5
HELIX   21 AC3 K7K B  161  ALA B  177  1                                  17
HELIX   22 AC4 SER B  198  PHE B  204  1                                   7
HELIX   23 AC5 SER B  211  VAL B  223  1                                  13
HELIX   24 AC6 SER B  235  ALA B  239  5                                   5
HELIX   25 AC7 LEU B  258  ALA B  272  1                                  15
HELIX   26 AC8 SER B  296  GLY B  314  1                                  19
HELIX   27 AC9 LEU C    3  GLY C   20  1                                  18
HELIX   28 AD1 GLY C   23  LEU C   27  5                                   5
HELIX   29 AD2 PRO C   28  GLU C   44  1                                  17
HELIX   30 AD3 ASN C   95  THR C   98  5                                   4
HELIX   31 AD4 HIS C   99  ARG C  111  1                                  13
HELIX   32 AD5 PRO C  128  ASP C  143  1                                  16
HELIX   33 AD6 ASN C  144  PHE C  148  5                                   5
HELIX   34 AD7 K7K C  161  ALA C  177  1                                  17
HELIX   35 AD8 SER C  198  PHE C  204  1                                   7
HELIX   36 AD9 SER C  211  VAL C  223  1                                  13
HELIX   37 AE1 SER C  235  ALA C  239  5                                   5
HELIX   38 AE2 LEU C  258  ALA C  272  1                                  15
HELIX   39 AE3 SER C  296  GLY C  314  1                                  19
HELIX   40 AE4 LEU D    3  GLY D   20  1                                  18
HELIX   41 AE5 GLY D   23  LEU D   27  5                                   5
HELIX   42 AE6 PRO D   28  GLU D   44  1                                  17
HELIX   43 AE7 ASN D   95  THR D   98  5                                   4
HELIX   44 AE8 HIS D   99  ARG D  111  1                                  13
HELIX   45 AE9 PRO D  128  ASP D  143  1                                  16
HELIX   46 AF1 ASN D  144  PHE D  148  5                                   5
HELIX   47 AF2 K7K D  161  ALA D  177  1                                  17
HELIX   48 AF3 SER D  198  PHE D  204  1                                   7
HELIX   49 AF4 SER D  211  VAL D  223  1                                  13
HELIX   50 AF5 SER D  235  ALA D  239  5                                   5
HELIX   51 AF6 LEU D  258  ALA D  272  1                                  15
HELIX   52 AF7 SER D  296  GLY D  314  1                                  19
SHEET    1 AA116 GLU A  52  ALA A  59  0
SHEET    2 AA116 GLU A  64  ARG A  71 -1  O  ARG A  71   N  GLU A  52
SHEET    3 AA116 GLN A 113  ASP A 118 -1  O  ASP A 118   N  ARG A  66
SHEET    4 AA116 LEU A  80  TYR A  86  1  N  PRO A  81   O  GLN A 113
SHEET    5 AA116 ALA A 150  ASP A 160  1  O  ALA A 156   N  ILE A  84
SHEET    6 AA116 GLN A 185  ILE A 188  1  O  ILE A 188   N  GLY A 159
SHEET    7 AA116 ALA A 248  TYR A 255  1  O  PHE A 249   N  LEU A 187
SHEET    8 AA116 THR A 276  ILE A 285  1  O  TYR A 281   N  THR A 252
SHEET    9 AA116 THR C 276  ILE C 285 -1  O  TYR C 278   N  TYR A 278
SHEET   10 AA116 ALA C 248  TYR C 255  1  N  THR C 252   O  TYR C 281
SHEET   11 AA116 GLN C 185  ILE C 188  1  N  LEU C 187   O  PHE C 249
SHEET   12 AA116 ALA C 150  ASP C 160  1  N  GLY C 159   O  ILE C 188
SHEET   13 AA116 LEU C  80  TYR C  86  1  N  ILE C  84   O  ALA C 156
SHEET   14 AA116 GLN C 113  ASP C 118  1  O  GLN C 113   N  PRO C  81
SHEET   15 AA116 GLU C  64  ARG C  71 -1  N  ARG C  66   O  ASP C 118
SHEET   16 AA116 GLU C  52  ALA C  59 -1  N  GLU C  52   O  ARG C  71
SHEET    1 AA216 GLU B  52  ALA B  59  0
SHEET    2 AA216 GLU B  64  ARG B  71 -1  O  ARG B  71   N  GLU B  52
SHEET    3 AA216 GLN B 113  ASP B 118 -1  O  ASP B 118   N  ARG B  66
SHEET    4 AA216 LEU B  80  TYR B  86  1  N  PRO B  81   O  GLN B 113
SHEET    5 AA216 ALA B 150  ASP B 160  1  O  ALA B 156   N  ILE B  84
SHEET    6 AA216 GLN B 185  ILE B 188  1  O  ILE B 188   N  GLY B 159
SHEET    7 AA216 ALA B 248  TYR B 255  1  O  PHE B 249   N  LEU B 187
SHEET    8 AA216 THR B 276  ILE B 285  1  O  TYR B 281   N  THR B 252
SHEET    9 AA216 THR D 276  ILE D 285 -1  O  TYR D 278   N  TYR B 278
SHEET   10 AA216 ALA D 248  TYR D 255  1  N  THR D 252   O  TYR D 281
SHEET   11 AA216 GLN D 185  ILE D 188  1  N  LEU D 187   O  PHE D 249
SHEET   12 AA216 ALA D 150  ASP D 160  1  N  GLY D 159   O  ILE D 188
SHEET   13 AA216 LEU D  80  TYR D  86  1  N  ILE D  84   O  ALA D 156
SHEET   14 AA216 GLN D 113  ASP D 118  1  O  GLN D 113   N  PRO D  81
SHEET   15 AA216 GLU D  64  ARG D  71 -1  N  ARG D  66   O  ASP D 118
SHEET   16 AA216 GLU D  52  ALA D  59 -1  N  GLU D  52   O  ARG D  71
LINK         C   ASP A 160                 N   K7K A 161     1555   1555  1.33
LINK         C   K7K A 161                 N   ALA A 162     1555   1555  1.33
LINK         C   ASP B 160                 N   K7K B 161     1555   1555  1.34
LINK         C   K7K B 161                 N   ALA B 162     1555   1555  1.33
LINK         C   ASP C 160                 N   K7K C 161     1555   1555  1.34
LINK         C   K7K C 161                 N   ALA C 162     1555   1555  1.34
LINK         C   ASP D 160                 N   K7K D 161     1555   1555  1.33
LINK         C   K7K D 161                 N   ALA D 162     1555   1555  1.34
CISPEP   1 ALA A  122    PRO A  123          0         7.06
CISPEP   2 PHE A  127    PRO A  128          0         5.97
CISPEP   3 ALA B  122    PRO B  123          0         6.06
CISPEP   4 PHE B  127    PRO B  128          0         5.83
CISPEP   5 ALA C  122    PRO C  123          0         7.11
CISPEP   6 PHE C  127    PRO C  128          0         5.78
CISPEP   7 ALA D  122    PRO D  123          0         6.78
CISPEP   8 PHE D  127    PRO D  128          0         5.55
SITE     1 AC1  3 ARG A 259  ASP A 260  ARG A 263
SITE     1 AC2  5 GLU B  49  VAL B  50  ASN B  55  GLY B  56
SITE     2 AC2  5 ARG B 104
SITE     1 AC3  1 GLY C 207
SITE     1 AC4  1 GLY C  60
SITE     1 AC5  1 ASP C 176
SITE     1 AC6  2 PRO C  61  SER C  63
SITE     1 AC7  2 ARG C 139  GLU C 179
SITE     1 AC8  4 ARG B 111  LYS D 109  ARG D 111  HOH D 505
SITE     1 AC9  2 ALA D 153  ALA D 183
SITE     1 AD1  3 GLY D 178  THR D 180  HOH D 508
SITE     1 AD2 19 TYR B  85  TYR B  86  HIS B  87  GLY B  88
SITE     2 AD2 19 GLY B  89  GLY B  90  HIS B  99  GLY B 159
SITE     3 AD2 19 ALA B 162  GLY B 163  GLY B 164  ALA B 165
SITE     4 AD2 19 ILE B 188  TYR B 189  PRO B 190  ALA B 191
SITE     5 AD2 19 PHE B 209  PHE B 218  HIS B 286
SITE     1 AD3 16 GLY B  88  GLY B  89  GLY B  90  PHE B  91
SITE     2 AD3 16 ASP B 160  GLY B 163  GLY B 164  ALA B 165
SITE     3 AD3 16 MET B 166  ILE B 188  TYR B 189  PRO B 190
SITE     4 AD3 16 ALA B 191  PHE B 209  PHE B 218  HIS B 286
SITE     1 AD4 19 TYR C  85  TYR C  86  HIS C  87  GLY C  88
SITE     2 AD4 19 GLY C  89  GLY C  90  HIS C  99  GLY C 159
SITE     3 AD4 19 ALA C 162  GLY C 163  GLY C 164  ALA C 165
SITE     4 AD4 19 ILE C 188  TYR C 189  PRO C 190  ALA C 191
SITE     5 AD4 19 PHE C 209  PHE C 218  HIS C 286
SITE     1 AD5 16 GLY C  88  GLY C  89  GLY C  90  PHE C  91
SITE     2 AD5 16 ASP C 160  GLY C 163  GLY C 164  ALA C 165
SITE     3 AD5 16 MET C 166  ILE C 188  TYR C 189  PRO C 190
SITE     4 AD5 16 ALA C 191  PHE C 209  PHE C 218  HIS C 286
SITE     1 AD6 19 TYR D  85  TYR D  86  HIS D  87  GLY D  88
SITE     2 AD6 19 GLY D  89  GLY D  90  HIS D  99  GLY D 159
SITE     3 AD6 19 ALA D 162  GLY D 163  GLY D 164  ALA D 165
SITE     4 AD6 19 ILE D 188  TYR D 189  PRO D 190  ALA D 191
SITE     5 AD6 19 PHE D 209  PHE D 218  HIS D 286
SITE     1 AD7 16 GLY D  88  GLY D  89  GLY D  90  PHE D  91
SITE     2 AD7 16 ASP D 160  GLY D 163  GLY D 164  ALA D 165
SITE     3 AD7 16 MET D 166  ILE D 188  TYR D 189  PRO D 190
SITE     4 AD7 16 ALA D 191  PHE D 209  PHE D 218  HIS D 286
CRYST1   90.766  201.920   90.637  90.00 112.19  90.00 C 1 2 1      16
ORIGX1      1.000000  0.000000  0.000000        0.00000
ORIGX2      0.000000  1.000000  0.000000        0.00000
ORIGX3      0.000000  0.000000  1.000000        0.00000
SCALE1      0.011017  0.000000  0.004494        0.00000
SCALE2      0.000000  0.004952  0.000000        0.00000
SCALE3      0.000000  0.000000  0.011916        0.00000
TER    2408      THR A 315
TER    4816      THR B 315
TER    7224      THR C 315
TER    9632      THR D 315
MASTER      397    0   14   52   32    0   38    6 9764    4  184  100
END