longtext: 7ebo-pdb

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HEADER    HYDROLASE                               10-MAR-21   7EBO
TITLE     CRYSTAL STRUCTURE OF A FERULOYL ESTERASE LP_0796 FROM LACTOBACILLUS
TITLE    2 PLANTARUM
COMPND    MOL_ID: 1;
COMPND   2 MOLECULE: CARBOXYLESTERASE;
COMPND   3 CHAIN: A, B;
COMPND   4 EC: 3.1.1.1;
COMPND   5 ENGINEERED: YES
SOURCE    MOL_ID: 1;
SOURCE   2 ORGANISM_SCIENTIFIC: LACTIPLANTIBACILLUS PLANTARUM WCFS1;
SOURCE   3 ORGANISM_TAXID: 220668;
SOURCE   4 STRAIN: ATCC BAA-793 / NCIMB 8826 / WCFS1;
SOURCE   5 GENE: LP_0796;
SOURCE   6 EXPRESSION_SYSTEM: ESCHERICHIA COLI BL21(DE3);
SOURCE   7 EXPRESSION_SYSTEM_TAXID: 469008
KEYWDS    FERULOYL ESTERASE, LACTOBACILLUS PLANTARUM, CARBOXYLESTERASE,
KEYWDS   2 CATALYTIC TRIAD, HYDROLASE
EXPDTA    X-RAY DIFFRACTION
AUTHOR    H.W.ZHANG,Y.L.WANG,F.J.XIN
REVDAT   1   03-AUG-22 7EBO    0
JRNL        AUTH   H.ZHANG,B.WEN,Y.LIU,G.DU,X.WEI,K.M.S.U.IMAM,H.ZHOU,S.FAN,
JRNL        AUTH 2 F.WANG,Y.WANG,F.XIN
JRNL        TITL   A REVERSE CATALYTIC TRIAD ASP CONTAINING LOOP SHAPING A WIDE
JRNL        TITL 2 SUBSTRATE BINDING POCKET OF A FERULOYL ESTERASE FROM
JRNL        TITL 3 LACTOBACILLUS PLANTARUM.
JRNL        REF    INT.J.BIOL.MACROMOL.          V. 184    92 2021
JRNL        REFN                   ISSN 0141-8130
JRNL        PMID   34116094
JRNL        DOI    10.1016/J.IJBIOMAC.2021.06.033
REMARK   2
REMARK   2 RESOLUTION.    2.50 ANGSTROMS.
REMARK   3
REMARK   3 REFINEMENT.
REMARK   3   PROGRAM     : PHENIX 1.12_2829
REMARK   3   AUTHORS     : PAUL ADAMS,PAVEL AFONINE,VINCENT CHEN,IAN
REMARK   3               : DAVIS,KRESHNA GOPAL,RALF GROSSE-KUNSTLEVE,
REMARK   3               : LI-WEI HUNG,ROBERT IMMORMINO,TOM IOERGER,
REMARK   3               : AIRLIE MCCOY,ERIK MCKEE,NIGEL MORIARTY,
REMARK   3               : REETAL PAI,RANDY READ,JANE RICHARDSON,
REMARK   3               : DAVID RICHARDSON,TOD ROMO,JIM SACCHETTINI,
REMARK   3               : NICHOLAS SAUTER,JACOB SMITH,LAURENT
REMARK   3               : STORONI,TOM TERWILLIGER,PETER ZWART
REMARK   3
REMARK   3    REFINEMENT TARGET : ML
REMARK   3
REMARK   3  DATA USED IN REFINEMENT.
REMARK   3   RESOLUTION RANGE HIGH (ANGSTROMS) : 2.50
REMARK   3   RESOLUTION RANGE LOW  (ANGSTROMS) : 49.18
REMARK   3   MIN(FOBS/SIGMA_FOBS)              : 1.350
REMARK   3   COMPLETENESS FOR RANGE        (%) : 99.4
REMARK   3   NUMBER OF REFLECTIONS             : 16162
REMARK   3
REMARK   3  FIT TO DATA USED IN REFINEMENT.
REMARK   3   R VALUE     (WORKING + TEST SET) : 0.203
REMARK   3   R VALUE            (WORKING SET) : 0.201
REMARK   3   FREE R VALUE                     : 0.239
REMARK   3   FREE R VALUE TEST SET SIZE   (%) : 5.190
REMARK   3   FREE R VALUE TEST SET COUNT      : 839
REMARK   3
REMARK   3  FIT TO DATA USED IN REFINEMENT (IN BINS).
REMARK   3   BIN  RESOLUTION RANGE  COMPL.    NWORK NFREE   RWORK  RFREE
REMARK   3     1  4.5420 -  3.6055    1.00     2599   128  0.1745 0.1961
REMARK   3     2  3.6055 -  3.1498    1.00     2553   147  0.1983 0.2283
REMARK   3     3  3.1498 -  2.8619    1.00     2553   112  0.2269 0.2982
REMARK   3     4  2.8619 -  2.6567    1.00     2516   143  0.2249 0.2781
REMARK   3     5  2.6567 -  2.5001    0.97     2405   153  0.2268 0.3082
REMARK   3
REMARK   3  BULK SOLVENT MODELLING.
REMARK   3   METHOD USED        : FLAT BULK SOLVENT MODEL
REMARK   3   SOLVENT RADIUS     : 1.11
REMARK   3   SHRINKAGE RADIUS   : 0.90
REMARK   3   K_SOL              : NULL
REMARK   3   B_SOL              : NULL
REMARK   3
REMARK   3  ERROR ESTIMATES.
REMARK   3   COORDINATE ERROR (MAXIMUM-LIKELIHOOD BASED)     : 0.270
REMARK   3   PHASE ERROR (DEGREES, MAXIMUM-LIKELIHOOD BASED) : 24.810
REMARK   3
REMARK   3  B VALUES.
REMARK   3   FROM WILSON PLOT           (A**2) : 36.88
REMARK   3   MEAN B VALUE      (OVERALL, A**2) : 40.07
REMARK   3   OVERALL ANISOTROPIC B VALUE.
REMARK   3    B11 (A**2) : NULL
REMARK   3    B22 (A**2) : NULL
REMARK   3    B33 (A**2) : NULL
REMARK   3    B12 (A**2) : NULL
REMARK   3    B13 (A**2) : NULL
REMARK   3    B23 (A**2) : NULL
REMARK   3
REMARK   3  TWINNING INFORMATION.
REMARK   3   FRACTION: NULL
REMARK   3   OPERATOR: NULL
REMARK   3
REMARK   3  DEVIATIONS FROM IDEAL VALUES.
REMARK   3                 RMSD          COUNT
REMARK   3   BOND      :  0.003           3875
REMARK   3   ANGLE     :  0.725           5282
REMARK   3   CHIRALITY :  0.043            591
REMARK   3   PLANARITY :  0.004            693
REMARK   3   DIHEDRAL  : 22.965           1348
REMARK   3
REMARK   3  TLS DETAILS
REMARK   3   NUMBER OF TLS GROUPS  : NULL
REMARK   3
REMARK   3  NCS DETAILS
REMARK   3   NUMBER OF NCS GROUPS : NULL
REMARK   3
REMARK   3  OTHER REFINEMENT REMARKS: NULL
REMARK   4
REMARK   4 7EBO COMPLIES WITH FORMAT V. 3.30, 13-JUL-11
REMARK 100
REMARK 100 THIS ENTRY HAS BEEN PROCESSED BY PDBJ ON 11-MAR-21.
REMARK 100 THE DEPOSITION ID IS D_1300021111.
REMARK 200
REMARK 200 EXPERIMENTAL DETAILS
REMARK 200  EXPERIMENT TYPE                : X-RAY DIFFRACTION
REMARK 200  DATE OF DATA COLLECTION        : 07-NOV-19
REMARK 200  TEMPERATURE           (KELVIN) : 100
REMARK 200  PH                             : NULL
REMARK 200  NUMBER OF CRYSTALS USED        : 1
REMARK 200
REMARK 200  SYNCHROTRON              (Y/N) : Y
REMARK 200  RADIATION SOURCE               : SSRF
REMARK 200  BEAMLINE                       : BL17U1
REMARK 200  X-RAY GENERATOR MODEL          : NULL
REMARK 200  MONOCHROMATIC OR LAUE    (M/L) : M
REMARK 200  WAVELENGTH OR RANGE        (A) : 0.9792
REMARK 200  MONOCHROMATOR                  : NULL
REMARK 200  OPTICS                         : NULL
REMARK 200
REMARK 200  DETECTOR TYPE                  : CCD
REMARK 200  DETECTOR MANUFACTURER          : ADSC QUANTUM 315R
REMARK 200  INTENSITY-INTEGRATION SOFTWARE : NULL
REMARK 200  DATA SCALING SOFTWARE          : HKL-2000
REMARK 200
REMARK 200  NUMBER OF UNIQUE REFLECTIONS   : 21091
REMARK 200  RESOLUTION RANGE HIGH      (A) : 2.200
REMARK 200  RESOLUTION RANGE LOW       (A) : 50.000
REMARK 200  REJECTION CRITERIA  (SIGMA(I)) : NULL
REMARK 200
REMARK 200 OVERALL.
REMARK 200  COMPLETENESS FOR RANGE     (%) : 96.2
REMARK 200  DATA REDUNDANCY                : 10.60
REMARK 200  R MERGE                    (I) : 0.11200
REMARK 200  R SYM                      (I) : NULL
REMARK 200   FOR THE DATA SET  : 9.0000
REMARK 200
REMARK 200 IN THE HIGHEST RESOLUTION SHELL.
REMARK 200  HIGHEST RESOLUTION SHELL, RANGE HIGH (A) : 2.20
REMARK 200  HIGHEST RESOLUTION SHELL, RANGE LOW  (A) : 2.28
REMARK 200  COMPLETENESS FOR SHELL     (%) : 100.0
REMARK 200  DATA REDUNDANCY IN SHELL       : 7.60
REMARK 200  R MERGE FOR SHELL          (I) : 0.48600
REMARK 200  R SYM FOR SHELL            (I) : NULL
REMARK 200   FOR SHELL         : NULL
REMARK 200
REMARK 200 DIFFRACTION PROTOCOL: SINGLE WAVELENGTH
REMARK 200 METHOD USED TO DETERMINE THE STRUCTURE: MOLECULAR REPLACEMENT
REMARK 200 SOFTWARE USED: PHASER
REMARK 200 STARTING MODEL: 1TQH
REMARK 200
REMARK 200 REMARK: NULL
REMARK 280
REMARK 280 CRYSTAL
REMARK 280 SOLVENT CONTENT, VS   (%): 39.12
REMARK 280 MATTHEWS COEFFICIENT, VM (ANGSTROMS**3/DA): 2.02
REMARK 280
REMARK 280 CRYSTALLIZATION CONDITIONS: 0.2 M AMMONIUM SULFATE, 0.1 M MES PH
REMARK 280  6.5 AND 25% POLYETHYLENE GLYCOL 8000, VAPOR DIFFUSION, HANGING
REMARK 280  DROP, TEMPERATURE 298K
REMARK 290
REMARK 290 CRYSTALLOGRAPHIC SYMMETRY
REMARK 290 SYMMETRY OPERATORS FOR SPACE GROUP: P 21 21 21
REMARK 290
REMARK 290      SYMOP   SYMMETRY
REMARK 290     NNNMMM   OPERATOR
REMARK 290       1555   X,Y,Z
REMARK 290       2555   -X+1/2,-Y,Z+1/2
REMARK 290       3555   -X,Y+1/2,-Z+1/2
REMARK 290       4555   X+1/2,-Y+1/2,-Z
REMARK 290
REMARK 290     WHERE NNN -> OPERATOR NUMBER
REMARK 290           MMM -> TRANSLATION VECTOR
REMARK 290
REMARK 290 CRYSTALLOGRAPHIC SYMMETRY TRANSFORMATIONS
REMARK 290 THE FOLLOWING TRANSFORMATIONS OPERATE ON THE ATOM/HETATM
REMARK 290 RECORDS IN THIS ENTRY TO PRODUCE CRYSTALLOGRAPHICALLY
REMARK 290 RELATED MOLECULES.
REMARK 290   SMTRY1   1  1.000000  0.000000  0.000000        0.00000
REMARK 290   SMTRY2   1  0.000000  1.000000  0.000000        0.00000
REMARK 290   SMTRY3   1  0.000000  0.000000  1.000000        0.00000
REMARK 290   SMTRY1   2 -1.000000  0.000000  0.000000       27.44550
REMARK 290   SMTRY2   2  0.000000 -1.000000  0.000000        0.00000
REMARK 290   SMTRY3   2  0.000000  0.000000  1.000000       55.36300
REMARK 290   SMTRY1   3 -1.000000  0.000000  0.000000        0.00000
REMARK 290   SMTRY2   3  0.000000  1.000000  0.000000       37.16950
REMARK 290   SMTRY3   3  0.000000  0.000000 -1.000000       55.36300
REMARK 290   SMTRY1   4  1.000000  0.000000  0.000000       27.44550
REMARK 290   SMTRY2   4  0.000000 -1.000000  0.000000       37.16950
REMARK 290   SMTRY3   4  0.000000  0.000000 -1.000000        0.00000
REMARK 290
REMARK 290 REMARK: NULL
REMARK 300
REMARK 300 BIOMOLECULE: 1
REMARK 300 SEE REMARK 350 FOR THE AUTHOR PROVIDED AND/OR PROGRAM
REMARK 300 GENERATED ASSEMBLY INFORMATION FOR THE STRUCTURE IN
REMARK 300 THIS ENTRY. THE REMARK MAY ALSO PROVIDE INFORMATION ON
REMARK 300 BURIED SURFACE AREA.
REMARK 350
REMARK 350 COORDINATES FOR A COMPLETE MULTIMER REPRESENTING THE KNOWN
REMARK 350 BIOLOGICALLY SIGNIFICANT OLIGOMERIZATION STATE OF THE
REMARK 350 MOLECULE CAN BE GENERATED BY APPLYING BIOMT TRANSFORMATIONS
REMARK 350 GIVEN BELOW.  BOTH NON-CRYSTALLOGRAPHIC AND
REMARK 350 CRYSTALLOGRAPHIC OPERATIONS ARE GIVEN.
REMARK 350
REMARK 350 BIOMOLECULE: 1
REMARK 350 AUTHOR DETERMINED BIOLOGICAL UNIT: DIMERIC
REMARK 350 SOFTWARE DETERMINED QUATERNARY STRUCTURE: DIMERIC
REMARK 350 SOFTWARE USED: PISA
REMARK 350 TOTAL BURIED SURFACE AREA: 3280 ANGSTROM**2
REMARK 350 SURFACE AREA OF THE COMPLEX: 18600 ANGSTROM**2
REMARK 350 CHANGE IN SOLVENT FREE ENERGY: -22.0 KCAL/MOL
REMARK 350 APPLY THE FOLLOWING TO CHAINS: A, B
REMARK 350   BIOMT1   1  1.000000  0.000000  0.000000        0.00000
REMARK 350   BIOMT2   1  0.000000  1.000000  0.000000        0.00000
REMARK 350   BIOMT3   1  0.000000  0.000000  1.000000        0.00000
REMARK 465
REMARK 465 MISSING RESIDUES
REMARK 465 THE FOLLOWING RESIDUES WERE NOT LOCATED IN THE
REMARK 465 EXPERIMENT. (M=MODEL NUMBER; RES=RESIDUE NAME; C=CHAIN
REMARK 465 IDENTIFIER; SSSEQ=SEQUENCE NUMBER; I=INSERTION CODE.)
REMARK 465
REMARK 465   M RES C SSSEQI
REMARK 465     MET A     1
REMARK 465     MET A     2
REMARK 465     LEU A     3
REMARK 465     LYS A     4
REMARK 465     GLN A     5
REMARK 465     PRO A     6
REMARK 465     LYS A   249
REMARK 465     MET B     1
REMARK 465     MET B     2
REMARK 465     LEU B     3
REMARK 465     ASN B   124
REMARK 465     ARG B   125
REMARK 465     TYR B   248
REMARK 465     LYS B   249
REMARK 470
REMARK 470 MISSING ATOM
REMARK 470 THE FOLLOWING RESIDUES HAVE MISSING ATOMS (M=MODEL NUMBER;
REMARK 470 RES=RESIDUE NAME; C=CHAIN IDENTIFIER; SSEQ=SEQUENCE NUMBER;
REMARK 470 I=INSERTION CODE):
REMARK 470   M RES CSSEQI  ATOMS
REMARK 470     GLU A   7    CG   CD   OE1  OE2
REMARK 470     ASP A  56    CG   OD1  OD2
REMARK 470     MET A 131    CG   SD   CE
REMARK 470     ARG A 163    CG   CD   NE   CZ   NH1  NH2
REMARK 470     LYS B   4    CG   CD   CE   NZ
REMARK 470     GLN B  82    CG   CD   OE1  NE2
REMARK 470     HIS B 142    CG   ND1  CD2  CE1  NE2
REMARK 470     SER B 143    OG
REMARK 470     GLN B 144    CG   CD   OE1  NE2
REMARK 470     ARG B 204    CG   CD   NE   CZ   NH1  NH2
REMARK 470     GLN B 205    CG   CD   OE1  NE2
REMARK 470     GLN B 238    CG   CD   OE1  NE2
REMARK 500
REMARK 500 GEOMETRY AND STEREOCHEMISTRY
REMARK 500 SUBTOPIC: TORSION ANGLES
REMARK 500
REMARK 500 TORSION ANGLES OUTSIDE THE EXPECTED RAMACHANDRAN REGIONS:
REMARK 500 (M=MODEL NUMBER; RES=RESIDUE NAME; C=CHAIN IDENTIFIER;
REMARK 500 SSEQ=SEQUENCE NUMBER; I=INSERTION CODE).
REMARK 500
REMARK 500 STANDARD TABLE:
REMARK 500 FORMAT:(10X,I3,1X,A3,1X,A1,I4,A1,4X,F7.2,3X,F7.2)
REMARK 500
REMARK 500 EXPECTED VALUES: GJ KLEYWEGT AND TA JONES (1996). PHI/PSI-
REMARK 500 CHOLOGY: RAMACHANDRAN REVISITED. STRUCTURE 4, 1395 - 1400
REMARK 500
REMARK 500  M RES CSSEQI        PSI       PHI
REMARK 500    HIS A  13      -79.00   -138.08
REMARK 500    SER A  94     -113.14     51.66
REMARK 500    HIS B  13      -79.90   -140.80
REMARK 500    SER B  94     -113.81     51.68
REMARK 500
REMARK 500 REMARK: NULL
REMARK 800
REMARK 800 SITE
REMARK 800 SITE_IDENTIFIER: AC1
REMARK 800 EVIDENCE_CODE: SOFTWARE
REMARK 800 SITE_DESCRIPTION: binding site for residue SO4 A 300
DBREF  7EBO A    1   249  UNP    F9UM18   F9UM18_LACPL     1    249
DBREF  7EBO B    1   249  UNP    F9UM18   F9UM18_LACPL     1    249
SEQRES   1 A  249  MET MET LEU LYS GLN PRO GLU PRO PHE PHE PHE GLU HIS
SEQRES   2 A  249  GLY GLN HIS ALA VAL ILE LEU LEU HIS ALA TYR ALA GLY
SEQRES   3 A  249  SER ALA ASN ASP VAL ARG MET LEU ALA ARG ALA LEU GLU
SEQRES   4 A  249  ARG GLU ASP TYR THR VAL TYR GLY PRO GLN PHE SER GLY
SEQRES   5 A  249  HIS ALA THR ASP ASP PRO ARG ASP ILE LEU ALA GLN THR
SEQRES   6 A  249  PRO ALA GLN TRP TRP GLN ASP THR GLN GLN ALA ILE SER
SEQRES   7 A  249  PHE MET ARG GLN LYS GLY TYR THR LYS ILE SER ILE PHE
SEQRES   8 A  249  GLY LEU SER LEU GLY GLY ILE PHE ALA THR ALA ALA LEU
SEQRES   9 A  249  GLU ARG ASP PRO GLN LEU LEU GLY GLY GLY THR PHE SER
SEQRES  10 A  249  SER PRO LEU PHE ALA GLY ASN ARG SER ASP VAL ALA GLU
SEQRES  11 A  249  MET PHE ILE THR LEU SER HIS HIS GLN LEU ALA HIS SER
SEQRES  12 A  249  GLN PHE SER ILE ALA GLU ARG GLU GLN ILE LEU MET THR
SEQRES  13 A  249  LEU PRO GLU LEU VAL GLN ARG GLN LEU GLN ALA VAL ASN
SEQRES  14 A  249  THR PHE THR THR THR GLU VAL THR SER HIS LEU SER ALA
SEQRES  15 A  249  VAL THR GLN PRO PHE PHE ILE GLY GLN GLY GLY GLN ASP
SEQRES  16 A  249  GLU LEU ILE ASP ALA THR VAL ALA ARG GLN LEU ARG ASP
SEQRES  17 A  249  GLN LEU PRO GLN VAL PRO VAL ASP PHE HIS TRP TYR ALA
SEQRES  18 A  249  ASP ALA GLY HIS VAL ILE THR VAL ASN SER ALA HIS HIS
SEQRES  19 A  249  GLN LEU GLU GLN ASP VAL LEU THR TYR LEU LYS THR ILE
SEQRES  20 A  249  TYR LYS
SEQRES   1 B  249  MET MET LEU LYS GLN PRO GLU PRO PHE PHE PHE GLU HIS
SEQRES   2 B  249  GLY GLN HIS ALA VAL ILE LEU LEU HIS ALA TYR ALA GLY
SEQRES   3 B  249  SER ALA ASN ASP VAL ARG MET LEU ALA ARG ALA LEU GLU
SEQRES   4 B  249  ARG GLU ASP TYR THR VAL TYR GLY PRO GLN PHE SER GLY
SEQRES   5 B  249  HIS ALA THR ASP ASP PRO ARG ASP ILE LEU ALA GLN THR
SEQRES   6 B  249  PRO ALA GLN TRP TRP GLN ASP THR GLN GLN ALA ILE SER
SEQRES   7 B  249  PHE MET ARG GLN LYS GLY TYR THR LYS ILE SER ILE PHE
SEQRES   8 B  249  GLY LEU SER LEU GLY GLY ILE PHE ALA THR ALA ALA LEU
SEQRES   9 B  249  GLU ARG ASP PRO GLN LEU LEU GLY GLY GLY THR PHE SER
SEQRES  10 B  249  SER PRO LEU PHE ALA GLY ASN ARG SER ASP VAL ALA GLU
SEQRES  11 B  249  MET PHE ILE THR LEU SER HIS HIS GLN LEU ALA HIS SER
SEQRES  12 B  249  GLN PHE SER ILE ALA GLU ARG GLU GLN ILE LEU MET THR
SEQRES  13 B  249  LEU PRO GLU LEU VAL GLN ARG GLN LEU GLN ALA VAL ASN
SEQRES  14 B  249  THR PHE THR THR THR GLU VAL THR SER HIS LEU SER ALA
SEQRES  15 B  249  VAL THR GLN PRO PHE PHE ILE GLY GLN GLY GLY GLN ASP
SEQRES  16 B  249  GLU LEU ILE ASP ALA THR VAL ALA ARG GLN LEU ARG ASP
SEQRES  17 B  249  GLN LEU PRO GLN VAL PRO VAL ASP PHE HIS TRP TYR ALA
SEQRES  18 B  249  ASP ALA GLY HIS VAL ILE THR VAL ASN SER ALA HIS HIS
SEQRES  19 B  249  GLN LEU GLU GLN ASP VAL LEU THR TYR LEU LYS THR ILE
SEQRES  20 B  249  TYR LYS
HET    SO4  A 300       5
HETNAM     SO4 SULFATE ION
FORMUL   3  SO4    O4 S 2-
FORMUL   4  HOH   *96(H2 O)
HELIX    1 AA1 SER A   27  ASP A   30  5                                   4
HELIX    2 AA2 VAL A   31  GLU A   41  1                                  11
HELIX    3 AA3 PRO A   58  GLN A   64  1                                   7
HELIX    4 AA4 THR A   65  LYS A   83  1                                  19
HELIX    5 AA5 SER A   94  ASP A  107  1                                  14
HELIX    6 AA6 ARG A  125  ALA A  141  1                                  17
HELIX    7 AA7 SER A  146  VAL A  176  1                                  31
HELIX    8 AA8 THR A  177  VAL A  183  5                                   7
HELIX    9 AA9 ILE A  198  GLN A  209  1                                  12
HELIX   10 AB1 ALA A  232  TYR A  248  1                                  17
HELIX   11 AB2 SER B   27  ASP B   30  5                                   4
HELIX   12 AB3 VAL B   31  GLU B   41  1                                  11
HELIX   13 AB4 ASP B   57  GLN B   64  1                                   8
HELIX   14 AB5 THR B   65  LYS B   83  1                                  19
HELIX   15 AB6 SER B   94  ASP B  107  1                                  14
HELIX   16 AB7 ASP B  127  HIS B  142  1                                  16
HELIX   17 AB8 SER B  146  MET B  155  1                                  10
HELIX   18 AB9 THR B  156  VAL B  176  1                                  21
HELIX   19 AC1 THR B  177  VAL B  183  5                                   7
HELIX   20 AC2 THR B  201  GLN B  209  1                                   9
HELIX   21 AC3 ALA B  232  ILE B  247  1                                  16
SHEET    1 AA1 7 PHE A   9  PHE A  11  0
SHEET    2 AA1 7 THR A  44  GLY A  47 -1  O  VAL A  45   N  PHE A  11
SHEET    3 AA1 7 HIS A  16  LEU A  21  1  N  VAL A  18   O  THR A  44
SHEET    4 AA1 7 LYS A  87  LEU A  93  1  O  SER A  89   N  ILE A  19
SHEET    5 AA1 7 GLY A 112  PHE A 116  1  O  PHE A 116   N  GLY A  92
SHEET    6 AA1 7 PHE A 187  GLY A 192  1  O  PHE A 188   N  GLY A 113
SHEET    7 AA1 7 VAL A 215  TYR A 220  1  O  ASP A 216   N  PHE A 187
SHEET    1 AA2 7 PHE B   9  PHE B  11  0
SHEET    2 AA2 7 THR B  44  GLY B  47 -1  O  VAL B  45   N  PHE B  11
SHEET    3 AA2 7 ALA B  17  LEU B  21  1  N  VAL B  18   O  THR B  44
SHEET    4 AA2 7 ILE B  88  LEU B  93  1  O  PHE B  91   N  ILE B  19
SHEET    5 AA2 7 GLY B 112  PHE B 116  1  O  PHE B 116   N  GLY B  92
SHEET    6 AA2 7 PHE B 187  GLY B 192  1  O  PHE B 188   N  GLY B 113
SHEET    7 AA2 7 VAL B 215  TYR B 220  1  O  TYR B 220   N  GLN B 191
SITE     1 AC1  3 ARG A  40  ARG B  32  ARG B  36
CRYST1   54.891   74.339  110.726  90.00  90.00  90.00 P 21 21 21    8
ORIGX1      1.000000  0.000000  0.000000        0.00000
ORIGX2      0.000000  1.000000  0.000000        0.00000
ORIGX3      0.000000  0.000000  1.000000        0.00000
SCALE1      0.018218  0.000000  0.000000        0.00000
SCALE2      0.000000  0.013452  0.000000        0.00000
SCALE3      0.000000  0.000000  0.009031        0.00000
TER    1900      TYR A 248
TER    3778      ILE B 247
MASTER      262    0    1   21   14    0    1    6 3877    2    5   40
END