longtext: 7k4o-pdb

content
HEADER    HYDROLASE                               15-SEP-20   7K4O
TITLE     TANNIN ACYL HYDROLASE FROM ASPERGILLUS NIGER
COMPND    MOL_ID: 1;
COMPND   2 MOLECULE: CARBOXYLIC ESTER HYDROLASE;
COMPND   3 CHAIN: A;
COMPND   4 EC: 3.1.1.-;
COMPND   5 ENGINEERED: YES
SOURCE    MOL_ID: 1;
SOURCE   2 ORGANISM_SCIENTIFIC: ASPERGILLUS NIGER;
SOURCE   3 ORGANISM_TAXID: 5061;
SOURCE   4 EXPRESSION_SYSTEM: ASPERGILLUS NIGER;
SOURCE   5 EXPRESSION_SYSTEM_TAXID: 5061
KEYWDS    ESTERASE, TANNIN, SERINE HYDROLASE, HYDROLASE
EXPDTA    X-RAY DIFFRACTION
AUTHOR    B.REN
REVDAT   1   17-MAR-21 7K4O    0
JRNL        AUTH   L.DONG,W.J.MCKINSTRY,L.PAN,J.NEWMAN,B.REN
JRNL        TITL   CRYSTAL STRUCTURE OF FUNGAL TANNASE FROM ASPERGILLUS NIGER.
JRNL        REF    ACTA CRYSTALLOGR D STRUCT     V.  77   267 2021
JRNL        REF  2 BIOL
JRNL        REFN                   ISSN 2059-7983
JRNL        PMID   33559614
JRNL        DOI    10.1107/S2059798320016484
REMARK   2
REMARK   2 RESOLUTION.    1.65 ANGSTROMS.
REMARK   3
REMARK   3 REFINEMENT.
REMARK   3   PROGRAM     : REFMAC 5.8.0258
REMARK   3   AUTHORS     : MURSHUDOV,SKUBAK,LEBEDEV,PANNU,STEINER,
REMARK   3               : NICHOLLS,WINN,LONG,VAGIN
REMARK   3
REMARK   3    REFINEMENT TARGET : NULL
REMARK   3
REMARK   3  DATA USED IN REFINEMENT.
REMARK   3   RESOLUTION RANGE HIGH (ANGSTROMS) : 1.65
REMARK   3   RESOLUTION RANGE LOW  (ANGSTROMS) : 19.76
REMARK   3   DATA CUTOFF            (SIGMA(F)) : NULL
REMARK   3   COMPLETENESS FOR RANGE        (%) : 99.9
REMARK   3   NUMBER OF REFLECTIONS             : 114035
REMARK   3
REMARK   3  FIT TO DATA USED IN REFINEMENT.
REMARK   3   CROSS-VALIDATION METHOD          : FREE R-VALUE
REMARK   3   FREE R VALUE TEST SET SELECTION  : NULL
REMARK   3   R VALUE     (WORKING + TEST SET) : NULL
REMARK   3   R VALUE            (WORKING SET) : 0.152
REMARK   3   FREE R VALUE                     : 0.174
REMARK   3   FREE R VALUE TEST SET SIZE   (%) : 4.997
REMARK   3   FREE R VALUE TEST SET COUNT      : 5698
REMARK   3
REMARK   3  FIT IN THE HIGHEST RESOLUTION BIN.
REMARK   3   TOTAL NUMBER OF BINS USED           : NULL
REMARK   3   BIN RESOLUTION RANGE HIGH       (A) : 1.65
REMARK   3   BIN RESOLUTION RANGE LOW        (A) : 1.69
REMARK   3   REFLECTION IN BIN     (WORKING SET) : 7951
REMARK   3   BIN COMPLETENESS (WORKING+TEST) (%) : 100.0
REMARK   3   BIN R VALUE           (WORKING SET) : 0.2610
REMARK   3   BIN FREE R VALUE SET COUNT          : 410
REMARK   3   BIN FREE R VALUE                    : 0.2700
REMARK   3
REMARK   3  NUMBER OF NON-HYDROGEN ATOMS USED IN REFINEMENT.
REMARK   3   PROTEIN ATOMS            : 4280
REMARK   3   NUCLEIC ACID ATOMS       : 0
REMARK   3   HETEROGEN ATOMS          : 337
REMARK   3   SOLVENT ATOMS            : 775
REMARK   3
REMARK   3  B VALUES.
REMARK   3   FROM WILSON PLOT           (A**2) : NULL
REMARK   3   MEAN B VALUE      (OVERALL, A**2) : 30.72
REMARK   3   OVERALL ANISOTROPIC B VALUE.
REMARK   3    B11 (A**2) : -0.27200
REMARK   3    B22 (A**2) : -0.27200
REMARK   3    B33 (A**2) : 0.88100
REMARK   3    B12 (A**2) : -0.13600
REMARK   3    B13 (A**2) : 0.00000
REMARK   3    B23 (A**2) : 0.00000
REMARK   3
REMARK   3  ESTIMATED OVERALL COORDINATE ERROR.
REMARK   3   ESU BASED ON R VALUE                            (A): 0.064
REMARK   3   ESU BASED ON FREE R VALUE                       (A): 0.066
REMARK   3   ESU BASED ON MAXIMUM LIKELIHOOD                 (A): NULL
REMARK   3   ESU FOR B VALUES BASED ON MAXIMUM LIKELIHOOD (A**2): NULL
REMARK   3
REMARK   3 CORRELATION COEFFICIENTS.
REMARK   3   CORRELATION COEFFICIENT FO-FC      : 0.977
REMARK   3   CORRELATION COEFFICIENT FO-FC FREE : 0.970
REMARK   3
REMARK   3  RMS DEVIATIONS FROM IDEAL VALUES        COUNT    RMS    WEIGHT
REMARK   3   BOND LENGTHS REFINED ATOMS        (A):  4856 ; 0.014 ; 0.013
REMARK   3   BOND LENGTHS OTHERS               (A):  4103 ; 0.035 ; 0.018
REMARK   3   BOND ANGLES REFINED ATOMS   (DEGREES):  6706 ; 1.880 ; 1.745
REMARK   3   BOND ANGLES OTHERS          (DEGREES):  9653 ; 3.165 ; 1.661
REMARK   3   TORSION ANGLES, PERIOD 1    (DEGREES):   594 ; 6.247 ; 5.000
REMARK   3   TORSION ANGLES, PERIOD 2    (DEGREES):   228 ;33.105 ;24.035
REMARK   3   TORSION ANGLES, PERIOD 3    (DEGREES):   676 ;11.745 ;15.000
REMARK   3   TORSION ANGLES, PERIOD 4    (DEGREES):    16 ;19.133 ;15.000
REMARK   3   CHIRAL-CENTER RESTRAINTS       (A**3):   712 ; 0.096 ; 0.200
REMARK   3   GENERAL PLANES REFINED ATOMS      (A):  5368 ; 0.011 ; 0.020
REMARK   3   GENERAL PLANES OTHERS             (A):   975 ; 0.019 ; 0.020
REMARK   3   NON-BONDED CONTACTS REFINED ATOMS (A):   927 ; 0.219 ; 0.200
REMARK   3   NON-BONDED CONTACTS OTHERS        (A):    34 ; 0.187 ; 0.200
REMARK   3   NON-BONDED TORSION REFINED ATOMS  (A):  2478 ; 0.178 ; 0.200
REMARK   3   NON-BONDED TORSION OTHERS         (A):  NULL ;  NULL ;  NULL
REMARK   3   H-BOND (X...Y) REFINED ATOMS      (A):   570 ; 0.232 ; 0.200
REMARK   3   H-BOND (X...Y) OTHERS             (A):  NULL ;  NULL ;  NULL
REMARK   3   POTENTIAL METAL-ION REFINED ATOMS (A):     7 ; 0.123 ; 0.200
REMARK   3   POTENTIAL METAL-ION OTHERS        (A):  NULL ;  NULL ;  NULL
REMARK   3   SYMMETRY VDW REFINED ATOMS        (A):  NULL ;  NULL ;  NULL
REMARK   3   SYMMETRY VDW OTHERS               (A):  NULL ;  NULL ;  NULL
REMARK   3   SYMMETRY H-BOND REFINED ATOMS     (A):  NULL ;  NULL ;  NULL
REMARK   3   SYMMETRY H-BOND OTHERS            (A):  NULL ;  NULL ;  NULL
REMARK   3   SYMMETRY METAL-ION REFINED ATOMS  (A):     2 ; 0.112 ; 0.200
REMARK   3   SYMMETRY METAL-ION OTHERS         (A):  NULL ;  NULL ;  NULL
REMARK   3
REMARK   3  ISOTROPIC THERMAL FACTOR RESTRAINTS.     COUNT   RMS    WEIGHT
REMARK   3   MAIN-CHAIN BOND REFINED ATOMS  (A**2):  2257 ; 2.562 ; 2.954
REMARK   3   MAIN-CHAIN BOND OTHER ATOMS    (A**2):  2256 ; 2.562 ; 2.954
REMARK   3   MAIN-CHAIN ANGLE REFINED ATOMS (A**2):  2830 ; 3.464 ; 4.423
REMARK   3   MAIN-CHAIN ANGLE OTHER ATOMS   (A**2):  2831 ; 3.464 ; 4.423
REMARK   3   SIDE-CHAIN BOND REFINED ATOMS  (A**2):  2597 ; 3.683 ; 3.489
REMARK   3   SIDE-CHAIN BOND OTHER ATOMS    (A**2):  2598 ; 3.900 ; 3.487
REMARK   3   SIDE-CHAIN ANGLE REFINED ATOMS (A**2):  3855 ; 5.469 ; 5.139
REMARK   3   SIDE-CHAIN ANGLE OTHER ATOMS   (A**2):  3856 ; 5.593 ; 5.138
REMARK   3   LONG RANGE B REFINED ATOMS     (A**2):  NULL ;  NULL ;  NULL
REMARK   3   LONG RANGE B OTHER ATOMS       (A**2):  NULL ;  NULL ;  NULL
REMARK   3
REMARK   3 ANISOTROPIC THERMAL FACTOR RESTRAINTS.    COUNT   RMS   WEIGHT
REMARK   3   RIGID-BOND RESTRAINTS          (A**2):  NULL ;  NULL ;  NULL
REMARK   3   SPHERICITY; FREE ATOMS         (A**2):  NULL ;  NULL ;  NULL
REMARK   3   SPHERICITY; BONDED ATOMS       (A**2):  NULL ;  NULL ;  NULL
REMARK   3
REMARK   3  NCS RESTRAINTS STATISTICS
REMARK   3   NUMBER OF DIFFERENT NCS GROUPS : NULL
REMARK   3
REMARK   3  TLS DETAILS
REMARK   3   NUMBER OF TLS GROUPS  : NULL
REMARK   3
REMARK   3  BULK SOLVENT MODELLING.
REMARK   3   METHOD USED : MASK BULK SOLVENT
REMARK   3   PARAMETERS FOR MASK CALCULATION
REMARK   3   VDW PROBE RADIUS   : 1.20
REMARK   3   ION PROBE RADIUS   : 0.80
REMARK   3   SHRINKAGE RADIUS   : 0.80
REMARK   3
REMARK   3  OTHER REFINEMENT REMARKS: HYDROGENS HAVE BEEN ADDED IN THEIR
REMARK   3  RIDING POSITIONS
REMARK   4
REMARK   4 7K4O COMPLIES WITH FORMAT V. 3.30, 13-JUL-11
REMARK 100
REMARK 100 THIS ENTRY HAS BEEN PROCESSED BY RCSB ON 16-SEP-20.
REMARK 100 THE DEPOSITION ID IS D_1000251864.
REMARK 200
REMARK 200 EXPERIMENTAL DETAILS
REMARK 200  EXPERIMENT TYPE                : X-RAY DIFFRACTION
REMARK 200  DATE OF DATA COLLECTION        : 21-MAR-19
REMARK 200  TEMPERATURE           (KELVIN) : 100
REMARK 200  PH                             : 6.5
REMARK 200  NUMBER OF CRYSTALS USED        : 1
REMARK 200
REMARK 200  SYNCHROTRON              (Y/N) : Y
REMARK 200  RADIATION SOURCE               : AUSTRALIAN SYNCHROTRON
REMARK 200  BEAMLINE                       : MX2
REMARK 200  X-RAY GENERATOR MODEL          : NULL
REMARK 200  MONOCHROMATIC OR LAUE    (M/L) : M
REMARK 200  WAVELENGTH OR RANGE        (A) : 0.9792
REMARK 200  MONOCHROMATOR                  : NULL
REMARK 200  OPTICS                         : NULL
REMARK 200
REMARK 200  DETECTOR TYPE                  : PIXEL
REMARK 200  DETECTOR MANUFACTURER          : DECTRIS EIGER X 16M
REMARK 200  INTENSITY-INTEGRATION SOFTWARE : XDS
REMARK 200  DATA SCALING SOFTWARE          : AIMLESS
REMARK 200
REMARK 200  NUMBER OF UNIQUE REFLECTIONS   : 114035
REMARK 200  RESOLUTION RANGE HIGH      (A) : 1.650
REMARK 200  RESOLUTION RANGE LOW       (A) : 19.760
REMARK 200  REJECTION CRITERIA  (SIGMA(I)) : NULL
REMARK 200
REMARK 200 OVERALL.
REMARK 200  COMPLETENESS FOR RANGE     (%) : 99.9
REMARK 200  DATA REDUNDANCY                : 13.40
REMARK 200  R MERGE                    (I) : 0.07900
REMARK 200  R SYM                      (I) : NULL
REMARK 200   FOR THE DATA SET  : 20.9000
REMARK 200
REMARK 200 IN THE HIGHEST RESOLUTION SHELL.
REMARK 200  HIGHEST RESOLUTION SHELL, RANGE HIGH (A) : 1.65
REMARK 200  HIGHEST RESOLUTION SHELL, RANGE LOW  (A) : 1.71
REMARK 200  COMPLETENESS FOR SHELL     (%) : NULL
REMARK 200  DATA REDUNDANCY IN SHELL       : NULL
REMARK 200  R MERGE FOR SHELL          (I) : 1.39600
REMARK 200  R SYM FOR SHELL            (I) : NULL
REMARK 200   FOR SHELL         : 1.800
REMARK 200
REMARK 200 DIFFRACTION PROTOCOL: SINGLE WAVELENGTH
REMARK 200 METHOD USED TO DETERMINE THE STRUCTURE: MOLECULAR REPLACEMENT
REMARK 200 SOFTWARE USED: PHASER
REMARK 200 STARTING MODEL: 3WMT
REMARK 200
REMARK 200 REMARK: NULL
REMARK 280
REMARK 280 CRYSTAL
REMARK 280 SOLVENT CONTENT, VS   (%): 68.06
REMARK 280 MATTHEWS COEFFICIENT, VM (ANGSTROMS**3/DA): 3.85
REMARK 280
REMARK 280 CRYSTALLIZATION CONDITIONS: ZINC SULFATE, POLYETHYLENE GLYCOL
REMARK 280  MONOMETHYL ETHER 500 AND 0.1 M SODIUM MES AT PH 6.5, VAPOR
REMARK 280  DIFFUSION, SITTING DROP, TEMPERATURE 281K
REMARK 290
REMARK 290 CRYSTALLOGRAPHIC SYMMETRY
REMARK 290 SYMMETRY OPERATORS FOR SPACE GROUP: P 65 2 2
REMARK 290
REMARK 290      SYMOP   SYMMETRY
REMARK 290     NNNMMM   OPERATOR
REMARK 290       1555   X,Y,Z
REMARK 290       2555   -Y,X-Y,Z+2/3
REMARK 290       3555   -X+Y,-X,Z+1/3
REMARK 290       4555   -X,-Y,Z+1/2
REMARK 290       5555   Y,-X+Y,Z+1/6
REMARK 290       6555   X-Y,X,Z+5/6
REMARK 290       7555   Y,X,-Z+2/3
REMARK 290       8555   X-Y,-Y,-Z
REMARK 290       9555   -X,-X+Y,-Z+1/3
REMARK 290      10555   -Y,-X,-Z+1/6
REMARK 290      11555   -X+Y,Y,-Z+1/2
REMARK 290      12555   X,X-Y,-Z+5/6
REMARK 290
REMARK 290     WHERE NNN -> OPERATOR NUMBER
REMARK 290           MMM -> TRANSLATION VECTOR
REMARK 290
REMARK 290 CRYSTALLOGRAPHIC SYMMETRY TRANSFORMATIONS
REMARK 290 THE FOLLOWING TRANSFORMATIONS OPERATE ON THE ATOM/HETATM
REMARK 290 RECORDS IN THIS ENTRY TO PRODUCE CRYSTALLOGRAPHICALLY
REMARK 290 RELATED MOLECULES.
REMARK 290   SMTRY1   1  1.000000  0.000000  0.000000        0.00000
REMARK 290   SMTRY2   1  0.000000  1.000000  0.000000        0.00000
REMARK 290   SMTRY3   1  0.000000  0.000000  1.000000        0.00000
REMARK 290   SMTRY1   2 -0.500000 -0.866025  0.000000        0.00000
REMARK 290   SMTRY2   2  0.866025 -0.500000  0.000000        0.00000
REMARK 290   SMTRY3   2  0.000000  0.000000  1.000000       74.04067
REMARK 290   SMTRY1   3 -0.500000  0.866025  0.000000        0.00000
REMARK 290   SMTRY2   3 -0.866025 -0.500000  0.000000        0.00000
REMARK 290   SMTRY3   3  0.000000  0.000000  1.000000       37.02033
REMARK 290   SMTRY1   4 -1.000000  0.000000  0.000000        0.00000
REMARK 290   SMTRY2   4  0.000000 -1.000000  0.000000        0.00000
REMARK 290   SMTRY3   4  0.000000  0.000000  1.000000       55.53050
REMARK 290   SMTRY1   5  0.500000  0.866025  0.000000        0.00000
REMARK 290   SMTRY2   5 -0.866025  0.500000  0.000000        0.00000
REMARK 290   SMTRY3   5  0.000000  0.000000  1.000000       18.51017
REMARK 290   SMTRY1   6  0.500000 -0.866025  0.000000        0.00000
REMARK 290   SMTRY2   6  0.866025  0.500000  0.000000        0.00000
REMARK 290   SMTRY3   6  0.000000  0.000000  1.000000       92.55083
REMARK 290   SMTRY1   7 -0.500000  0.866025  0.000000        0.00000
REMARK 290   SMTRY2   7  0.866025  0.500000  0.000000        0.00000
REMARK 290   SMTRY3   7  0.000000  0.000000 -1.000000       74.04067
REMARK 290   SMTRY1   8  1.000000  0.000000  0.000000        0.00000
REMARK 290   SMTRY2   8  0.000000 -1.000000  0.000000        0.00000
REMARK 290   SMTRY3   8  0.000000  0.000000 -1.000000        0.00000
REMARK 290   SMTRY1   9 -0.500000 -0.866025  0.000000        0.00000
REMARK 290   SMTRY2   9 -0.866025  0.500000  0.000000        0.00000
REMARK 290   SMTRY3   9  0.000000  0.000000 -1.000000       37.02033
REMARK 290   SMTRY1  10  0.500000 -0.866025  0.000000        0.00000
REMARK 290   SMTRY2  10 -0.866025 -0.500000  0.000000        0.00000
REMARK 290   SMTRY3  10  0.000000  0.000000 -1.000000       18.51017
REMARK 290   SMTRY1  11 -1.000000  0.000000  0.000000        0.00000
REMARK 290   SMTRY2  11  0.000000  1.000000  0.000000        0.00000
REMARK 290   SMTRY3  11  0.000000  0.000000 -1.000000       55.53050
REMARK 290   SMTRY1  12  0.500000  0.866025  0.000000        0.00000
REMARK 290   SMTRY2  12  0.866025 -0.500000  0.000000        0.00000
REMARK 290   SMTRY3  12  0.000000  0.000000 -1.000000       92.55083
REMARK 290
REMARK 290 REMARK: NULL
REMARK 300
REMARK 300 BIOMOLECULE: 1
REMARK 300 SEE REMARK 350 FOR THE AUTHOR PROVIDED AND/OR PROGRAM
REMARK 300 GENERATED ASSEMBLY INFORMATION FOR THE STRUCTURE IN
REMARK 300 THIS ENTRY. THE REMARK MAY ALSO PROVIDE INFORMATION ON
REMARK 300 BURIED SURFACE AREA.
REMARK 350
REMARK 350 COORDINATES FOR A COMPLETE MULTIMER REPRESENTING THE KNOWN
REMARK 350 BIOLOGICALLY SIGNIFICANT OLIGOMERIZATION STATE OF THE
REMARK 350 MOLECULE CAN BE GENERATED BY APPLYING BIOMT TRANSFORMATIONS
REMARK 350 GIVEN BELOW.  BOTH NON-CRYSTALLOGRAPHIC AND
REMARK 350 CRYSTALLOGRAPHIC OPERATIONS ARE GIVEN.
REMARK 350
REMARK 350 BIOMOLECULE: 1
REMARK 350 AUTHOR DETERMINED BIOLOGICAL UNIT: MONOMERIC
REMARK 350 APPLY THE FOLLOWING TO CHAINS: A, B, C, D, E, F, G
REMARK 350   BIOMT1   1  1.000000  0.000000  0.000000        0.00000
REMARK 350   BIOMT2   1  0.000000  1.000000  0.000000        0.00000
REMARK 350   BIOMT3   1  0.000000  0.000000  1.000000        0.00000
REMARK 375
REMARK 375 SPECIAL POSITION
REMARK 375 THE FOLLOWING ATOMS ARE FOUND TO BE WITHIN 0.15 ANGSTROMS
REMARK 375 OF A SYMMETRY RELATED ATOM AND ARE ASSUMED TO BE ON SPECIAL
REMARK 375 POSITIONS.
REMARK 375
REMARK 375 ATOM RES CSSEQI
REMARK 375 ZN    ZN A 605  LIES ON A SPECIAL POSITION.
REMARK 375 ZN    ZN A 606  LIES ON A SPECIAL POSITION.
REMARK 375 ZN    ZN A 607  LIES ON A SPECIAL POSITION.
REMARK 375      HOH A 740  LIES ON A SPECIAL POSITION.
REMARK 375      HOH A 842  LIES ON A SPECIAL POSITION.
REMARK 375      HOH A 873  LIES ON A SPECIAL POSITION.
REMARK 375      HOH A 945  LIES ON A SPECIAL POSITION.
REMARK 375      HOH A 971  LIES ON A SPECIAL POSITION.
REMARK 375      HOH A1304  LIES ON A SPECIAL POSITION.
REMARK 375      HOH A1371  LIES ON A SPECIAL POSITION.
REMARK 375      HOH A1389  LIES ON A SPECIAL POSITION.
REMARK 375      HOH A1421  LIES ON A SPECIAL POSITION.
REMARK 375      HOH A1461  LIES ON A SPECIAL POSITION.
REMARK 500
REMARK 500 GEOMETRY AND STEREOCHEMISTRY
REMARK 500 SUBTOPIC: CLOSE CONTACTS IN SAME ASYMMETRIC UNIT
REMARK 500
REMARK 500 THE FOLLOWING ATOMS ARE IN CLOSE CONTACT.
REMARK 500
REMARK 500  ATM1  RES C  SSEQI   ATM2  RES C  SSEQI           DISTANCE
REMARK 500   O2   MAN C     4     H1   MAN C     5              1.08
REMARK 500   O3   MAN B     4     H1   MAN B     7              1.12
REMARK 500   O4   NAG D     1     H1   NAG D     2              1.19
REMARK 500   O3   BMA C     3     H1   MAN C     4              1.20
REMARK 500   O4   NAG B     1     H1   NAG B     2              1.20
REMARK 500  HH21  ARG A   285     HG   SER A   558              1.21
REMARK 500   O4   NAG C     1     H1   NAG C     2              1.24
REMARK 500   O4   NAG B     2     H1   BMA B     3              1.24
REMARK 500   O4   NAG F     1     H1   NAG F     2              1.26
REMARK 500   O2   MAN B     5     H1   MAN B     6              1.27
REMARK 500   HG   SER A    54     H    ALA A    83              1.28
REMARK 500   O4   NAG G     1     H1   NAG G     2              1.29
REMARK 500   O    HOH A   713     O    HOH A  1212              1.43
REMARK 500   C4   NAG F     1     H1   NAG F     2              1.48
REMARK 500   C4   NAG D     1     H1   NAG D     2              1.48
REMARK 500   C4   NAG B     1     H1   NAG B     2              1.50
REMARK 500   C4   NAG G     1     H1   NAG G     2              1.52
REMARK 500   C4   NAG C     1     H1   NAG C     2              1.54
REMARK 500   C2   MAN B     5     H1   MAN B     6              1.57
REMARK 500   C3   BMA C     3     H1   MAN C     4              1.58
REMARK 500   C4   NAG B     2     H1   BMA B     3              1.59
REMARK 500   O    HOH A  1314     O    HOH A  1362              1.72
REMARK 500   O    HOH A  1252     O    HOH A  1280              1.81
REMARK 500   O    HOH A  1407     O    HOH A  1434              1.84
REMARK 500   O    HOH A  1284     O    HOH A  1385              1.85
REMARK 500   O    HOH A  1260     O    HOH A  1376              1.88
REMARK 500   O    HOH A  1285     O    HOH A  1306              1.89
REMARK 500   O    HOH A  1436     O    HOH A  1442              1.92
REMARK 500   O    HOH A  1236     O    HOH A  1270              1.93
REMARK 500   O    HOH A  1235     O    HOH A  1362              1.94
REMARK 500   O    HOH A   832     O    HOH A   935              1.94
REMARK 500   O    HOH A  1048     O    HOH A  1224              1.98
REMARK 500   O    HOH A  1283     O    HOH A  1307              1.99
REMARK 500   O    HOH A  1283     O    HOH A  1357              2.03
REMARK 500   O    HOH A  1207     O    HOH A  1368              2.05
REMARK 500   O    HOH A   705     O    HOH A  1090              2.07
REMARK 500   O    HOH A  1135     O    HOH A  1232              2.15
REMARK 500   O    HOH A  1112     O    HOH A  1217              2.15
REMARK 500   O    HOH A  1217     O    HOH A  1318              2.17
REMARK 500   O    HOH A   701     O    HOH A  1106              2.17
REMARK 500   O    HOH A  1018     O    HOH A  1410              2.18
REMARK 500   O    HOH A  1186     O    HOH A  1345              2.18
REMARK 500
REMARK 500 REMARK: NULL
REMARK 500
REMARK 500 GEOMETRY AND STEREOCHEMISTRY
REMARK 500 SUBTOPIC: CLOSE CONTACTS
REMARK 500
REMARK 500 THE FOLLOWING ATOMS THAT ARE RELATED BY CRYSTALLOGRAPHIC
REMARK 500 SYMMETRY ARE IN CLOSE CONTACT.  AN ATOM LOCATED WITHIN 0.15
REMARK 500 ANGSTROMS OF A SYMMETRY RELATED ATOM IS ASSUMED TO BE ON A
REMARK 500 SPECIAL POSITION AND IS, THEREFORE, LISTED IN REMARK 375
REMARK 500 INSTEAD OF REMARK 500.  ATOMS WITH NON-BLANK ALTERNATE
REMARK 500 LOCATION INDICATORS ARE NOT INCLUDED IN THE CALCULATIONS.
REMARK 500
REMARK 500 DISTANCE CUTOFF:
REMARK 500 2.2 ANGSTROMS FOR CONTACTS NOT INVOLVING HYDROGEN ATOMS
REMARK 500 1.6 ANGSTROMS FOR CONTACTS INVOLVING HYDROGEN ATOMS
REMARK 500
REMARK 500  ATM1  RES C  SSEQI   ATM2  RES C  SSEQI  SSYMOP   DISTANCE
REMARK 500   O    HOH A  1075     O    HOH A  1075    10555     2.13
REMARK 500   O    HOH A  1208     O    HOH A  1433     9555     2.19
REMARK 500
REMARK 500 REMARK: NULL
REMARK 500
REMARK 500 GEOMETRY AND STEREOCHEMISTRY
REMARK 500 SUBTOPIC: TORSION ANGLES
REMARK 500
REMARK 500 TORSION ANGLES OUTSIDE THE EXPECTED RAMACHANDRAN REGIONS:
REMARK 500 (M=MODEL NUMBER; RES=RESIDUE NAME; C=CHAIN IDENTIFIER;
REMARK 500 SSEQ=SEQUENCE NUMBER; I=INSERTION CODE).
REMARK 500
REMARK 500 STANDARD TABLE:
REMARK 500 FORMAT:(10X,I3,1X,A3,1X,A1,I4,A1,4X,F7.2,3X,F7.2)
REMARK 500
REMARK 500 EXPECTED VALUES: GJ KLEYWEGT AND TA JONES (1996). PHI/PSI-
REMARK 500 CHOLOGY: RAMACHANDRAN REVISITED. STRUCTURE 4, 1395 - 1400
REMARK 500
REMARK 500  M RES CSSEQI        PSI       PHI
REMARK 500    TYR A 172      -18.03   -161.95
REMARK 500    SER A 206     -120.86     69.47
REMARK 500    SER A 206     -121.91     70.88
REMARK 500    ALA A 230       69.16     24.28
REMARK 500    ALA A 232       45.12    -80.54
REMARK 500    ASP A 280       12.03   -148.16
REMARK 500    THR A 348      -14.01     91.35
REMARK 500    VAL A 381      -60.62   -103.27
REMARK 500    ASN A 384       26.56   -149.63
REMARK 500    THR A 413      -77.29   -126.42
REMARK 500    TRP A 474      -15.20   -143.61
REMARK 500
REMARK 500 REMARK: NULL
REMARK 525
REMARK 525 SOLVENT
REMARK 525
REMARK 525 THE SOLVENT MOLECULES HAVE CHAIN IDENTIFIERS THAT
REMARK 525 INDICATE THE POLYMER CHAIN WITH WHICH THEY ARE MOST
REMARK 525 CLOSELY ASSOCIATED. THE REMARK LISTS ALL THE SOLVENT
REMARK 525 MOLECULES WHICH ARE MORE THAN 5A AWAY FROM THE
REMARK 525 NEAREST POLYMER CHAIN (M = MODEL NUMBER;
REMARK 525 RES=RESIDUE NAME; C=CHAIN IDENTIFIER; SSEQ=SEQUENCE
REMARK 525 NUMBER; I=INSERTION CODE):
REMARK 525
REMARK 525  M RES CSSEQI
REMARK 525    HOH A1459        DISTANCE =  5.85 ANGSTROMS
REMARK 525    HOH A1461        DISTANCE =  5.92 ANGSTROMS
REMARK 525    HOH A1462        DISTANCE =  5.95 ANGSTROMS
REMARK 525    HOH A1465        DISTANCE =  6.56 ANGSTROMS
REMARK 525    HOH A1467        DISTANCE =  7.02 ANGSTROMS
REMARK 610
REMARK 610 MISSING HETEROATOM
REMARK 610 THE FOLLOWING RESIDUES HAVE MISSING ATOMS (M=MODEL NUMBER;
REMARK 610 RES=RESIDUE NAME; C=CHAIN IDENTIFIER; SSEQ=SEQUENCE NUMBER;
REMARK 610 I=INSERTION CODE):
REMARK 610   M RES C SSEQI
REMARK 610     MAN B    7
REMARK 620
REMARK 620 METAL COORDINATION
REMARK 620 (M=MODEL NUMBER; RES=RESIDUE NAME; C=CHAIN IDENTIFIER;
REMARK 620 SSEQ=SEQUENCE NUMBER; I=INSERTION CODE):
REMARK 620
REMARK 620 COORDINATION ANGLES FOR:  M RES CSSEQI METAL
REMARK 620                              NA A 611  NA
REMARK 620 N RES CSSEQI ATOM
REMARK 620 1 THR A  57   O
REMARK 620 2 THR A  57   OG1  70.5
REMARK 620 3 HOH A 823   O   106.4 157.3
REMARK 620 4 HOH A 907   O    75.1  73.2  84.2
REMARK 620 5 HOH A1077   O    71.5  85.8 115.0 144.9
REMARK 620 6 HOH A1145   O   151.1  80.7 101.1  99.4 104.6
REMARK 620 N                    1     2     3     4     5
REMARK 620
REMARK 620 COORDINATION ANGLES FOR:  M RES CSSEQI METAL
REMARK 620                              ZN A 607  ZN
REMARK 620 N RES CSSEQI ATOM
REMARK 620 1 GLU A  58   OE2
REMARK 620 2 GLU A  58   OE2   0.0
REMARK 620 3 HOH A 948   O    92.2  92.2
REMARK 620 4 HOH A 948   O   171.1 171.1  87.9
REMARK 620 5 HOH A1087   O    85.4  85.4  78.9 103.4
REMARK 620 6 HOH A1087   O    92.4  92.4 103.4  78.8 177.0
REMARK 620 N                    1     2     3     4     5
REMARK 620
REMARK 620 COORDINATION ANGLES FOR:  M RES CSSEQI METAL
REMARK 620                              ZN A 606  ZN
REMARK 620 N RES CSSEQI ATOM
REMARK 620 1 ASP A 196   OD2
REMARK 620 2 ASP A 196   OD2   0.0
REMARK 620 3 HOH A 925   O    87.2  87.2
REMARK 620 4 HOH A 925   O   168.1 168.1  83.6
REMARK 620 5 HOH A1066   O    86.0  86.0  92.3  86.8
REMARK 620 6 HOH A1066   O    94.7  94.7  86.8  92.3 178.8
REMARK 620 N                    1     2     3     4     5
REMARK 620
REMARK 620 COORDINATION ANGLES FOR:  M RES CSSEQI METAL
REMARK 620                              CA A 604  CA
REMARK 620 N RES CSSEQI ATOM
REMARK 620 1 ASP A 273   O
REMARK 620 2 ASP A 273   OD1  72.1
REMARK 620 3 ASP A 276   OD1  75.6 140.4
REMARK 620 4 ASP A 276   OD2  75.2 133.0  55.4
REMARK 620 5 LYS A 278   O    88.3  82.3  74.5 129.6
REMARK 620 6 ASP A 280   OD1 142.7  71.2 133.4 137.6  80.6
REMARK 620 7 VAL A 282   O    97.6  78.7 128.3  73.1 157.2  81.5
REMARK 620 8 HOH A 813   O   145.8 141.5  75.2  73.7 100.6  71.5  86.9
REMARK 620 N                    1     2     3     4     5     6     7
REMARK 620
REMARK 620 COORDINATION ANGLES FOR:  M RES CSSEQI METAL
REMARK 620                              ZN A 608  ZN
REMARK 620 N RES CSSEQI ATOM
REMARK 620 1 HIS A 425   NE2
REMARK 620 2 HOH A 935   O    89.4
REMARK 620 3 HOH A1250   O   104.8 165.5
REMARK 620 4 HOH A1275   O   111.1  88.8  88.7
REMARK 620 5 HOH A1300   O   114.0  94.3  77.5 134.8
REMARK 620 N                    1     2     3     4
REMARK 620
REMARK 620 COORDINATION ANGLES FOR:  M RES CSSEQI METAL
REMARK 620                              ZN A 605  ZN
REMARK 620 N RES CSSEQI ATOM
REMARK 620 1 GLU A 469   OE1
REMARK 620 2 GLU A 469   OE2  55.9
REMARK 620 3 GLU A 469   OE1   0.0  55.9
REMARK 620 4 GLU A 469   OE2  55.9   0.0  55.9
REMARK 620 5 GLU A 473   OE1  99.6 121.7  99.6 121.7
REMARK 620 6 GLU A 473   OE1  99.6 121.7  99.6 121.7   0.0
REMARK 620 N                    1     2     3     4     5
DBREF  7K4O A   21   574  UNP    A2QIR3   A2QIR3_ASPNC    21    574
SEQRES   1 A  554  ALA THR PRO SER THR LEU ALA GLU LEU CYS THR ASP SER
SEQRES   2 A  554  ILE VAL LYS ALA ALA LEU PRO PRO SER GLU PHE ILE GLN
SEQRES   3 A  554  GLY ILE THR ILE ASP SER ASP SER VAL THR THR GLU VAL
SEQRES   4 A  554  VAL THR ASN SER SER VAL SER SER GLU PHE TYR PRO SER
SEQRES   5 A  554  ALA THR ILE ASN TYR CYS ASN VAL THR PHE ALA TYR SER
SEQRES   6 A  554  HIS ASP GLY ILE ASP GLY ASP GLN VAL LEU LEU GLU ILE
SEQRES   7 A  554  TRP LEU PRO ALA PRO THR ASP PHE GLN ASN ARG TRP LEU
SEQRES   8 A  554  SER THR GLY GLY GLY GLY TYR ALA ILE ASN SER GLY ASP
SEQRES   9 A  554  GLN SER LEU PRO GLY GLY VAL MET TYR GLY ALA ALA SER
SEQRES  10 A  554  GLY MET THR ASP GLY GLY PHE GLY GLY PHE SER ASN ASN
SEQRES  11 A  554  ALA ASP THR ALA MET LEU LEU ALA ASN GLY THR LEU ASP
SEQRES  12 A  554  TYR GLU THR LEU TYR MET PHE ALA TYR LYS ALA HIS ARG
SEQRES  13 A  554  GLU LEU SER LEU ILE GLY LYS ALA LEU THR ARG ASN VAL
SEQRES  14 A  554  TYR GLY MET SER ASP SER ASP LYS LEU TYR ALA TYR TYR
SEQRES  15 A  554  GLN GLY CYS SER GLU GLY GLY ARG GLU GLY TRP SER GLN
SEQRES  16 A  554  VAL GLN ARG PHE GLY ASP GLU TRP ASP GLY ALA ILE ILE
SEQRES  17 A  554  GLY ALA PRO ALA PHE ARG TRP SER PHE GLN GLN THR GLN
SEQRES  18 A  554  HIS LEU TYR SER ASN VAL VAL GLU LYS THR LEU ASP TYR
SEQRES  19 A  554  TYR PRO PRO PRO CYS GLU LEU ASP LYS ILE VAL ASN GLU
SEQRES  20 A  554  THR ILE ALA ALA CYS ASP ALA MET ASP GLY LYS VAL ASP
SEQRES  21 A  554  TRP VAL VAL ALA ARG THR ASP LEU CYS LEU LEU ASP PHE
SEQRES  22 A  554  ASP ILE SER THR ILE GLU GLY LYS PRO TYR SER CYS ALA
SEQRES  23 A  554  ALA SER ARG GLY THR PRO ALA GLN ASN GLY THR VAL SER
SEQRES  24 A  554  ALA LYS GLY ILE GLU VAL ALA LYS THR ILE ILE ASN GLY
SEQRES  25 A  554  LEU HIS ASP SER GLN GLY ARG ARG VAL TYR PHE SER TYR
SEQRES  26 A  554  GLN PRO THR ALA ALA PHE ASP ASP ALA GLU THR GLN TYR
SEQRES  27 A  554  ASN SER THR THR GLY GLN TRP GLY LEU ASP ILE ASP GLN
SEQRES  28 A  554  LEU GLY GLY GLU TYR ILE ALA LEU LEU VAL ASP LYS ASN
SEQRES  29 A  554  GLY THR THR LEU ASP SER LEU ASP GLY VAL THR TYR ASP
SEQRES  30 A  554  THR LEU LYS ASP TRP MET ILE SER GLY LEU GLN GLU TYR
SEQRES  31 A  554  TYR SER THR LEU GLN THR THR TRP PRO ASP LEU THR PRO
SEQRES  32 A  554  PHE HIS GLU ALA GLY GLY LYS VAL ILE HIS PHE HIS GLY
SEQRES  33 A  554  ASP ALA ASP PHE SER ILE PRO THR ALA ALA SER ILE ARG
SEQRES  34 A  554  TYR TRP GLU SER VAL ARG SER ILE MET TYR PRO ASN GLN
SEQRES  35 A  554  ASP TYR ASN SER SER ALA GLU ALA LEU ASN GLU TRP TYR
SEQRES  36 A  554  ARG LEU TYR THR VAL PRO GLY ALA GLY HIS CYS ALA THR
SEQRES  37 A  554  ASN ASP ALA MET PRO ASN GLY PRO PHE PRO GLN THR ASN
SEQRES  38 A  554  MET ALA VAL MET ILE ASP TRP VAL GLU ASN GLY VAL VAL
SEQRES  39 A  554  PRO THR THR LEU ASN ALA THR VAL LEU GLN GLY GLU ASN
SEQRES  40 A  554  GLU GLY GLN ASN GLN GLN LEU CYS ALA TRP PRO LEU ARG
SEQRES  41 A  554  PRO LEU TRP THR ASN ASN GLY THR THR MET GLU CYS VAL
SEQRES  42 A  554  TYR ASN GLN ARG SER ILE ASP SER TRP HIS TYR ASP LEU
SEQRES  43 A  554  ASP ALA VAL PRO MET PRO VAL TYR
HET    NAG  B   1      27
HET    NAG  B   2      27
HET    BMA  B   3      20
HET    MAN  B   4      20
HET    MAN  B   5      21
HET    MAN  B   6      22
HET    MAN  B   7      20
HET    MAN  B   8      22
HET    NAG  C   1      27
HET    NAG  C   2      27
HET    BMA  C   3      20
HET    MAN  C   4      21
HET    MAN  C   5      22
HET    MAN  C   6      22
HET    NAG  D   1      27
HET    NAG  D   2      28
HET    NAG  E   1      27
HET    NAG  E   2      28
HET    NAG  F   1      27
HET    NAG  F   2      28
HET    NAG  G   1      27
HET    NAG  G   2      28
HET    NAG  A 601      28
HET    NAG  A 602      28
HET    GDE  A 603      17
HET     CA  A 604       1
HET     ZN  A 605       1
HET     ZN  A 606       1
HET     ZN  A 607       1
HET     ZN  A 608       1
HET     CL  A 609       1
HET     CL  A 610       1
HET     NA  A 611       1
HET    FWN  A 612      29
HETNAM     NAG 2-ACETAMIDO-2-DEOXY-BETA-D-GLUCOPYRANOSE
HETNAM     BMA BETA-D-MANNOPYRANOSE
HETNAM     MAN ALPHA-D-MANNOPYRANOSE
HETNAM     GDE 3,4,5-TRIHYDROXYBENZOIC ACID
HETNAM      CA CALCIUM ION
HETNAM      ZN ZINC ION
HETNAM      CL CHLORIDE ION
HETNAM      NA SODIUM ION
HETNAM     FWN 2-[2-(2-ETHOXYETHOXY)ETHOXY]ETHANOL
HETSYN     NAG N-ACETYL-BETA-D-GLUCOSAMINE; 2-ACETAMIDO-2-DEOXY-BETA-
HETSYN   2 NAG  D-GLUCOSE; 2-ACETAMIDO-2-DEOXY-D-GLUCOSE; 2-ACETAMIDO-
HETSYN   3 NAG  2-DEOXY-GLUCOSE; N-ACETYL-D-GLUCOSAMINE
HETSYN     BMA BETA-D-MANNOSE; D-MANNOSE; MANNOSE
HETSYN     MAN ALPHA-D-MANNOSE; D-MANNOSE; MANNOSE
HETSYN     GDE GALLATE
FORMUL   2  NAG    14(C8 H15 N O6)
FORMUL   2  BMA    2(C6 H12 O6)
FORMUL   2  MAN    8(C6 H12 O6)
FORMUL  10  GDE    C7 H6 O5
FORMUL  11   CA    CA 2+
FORMUL  12   ZN    4(ZN 2+)
FORMUL  16   CL    2(CL 1-)
FORMUL  18   NA    NA 1+
FORMUL  19  FWN    C8 H18 O4
FORMUL  20  HOH   *775(H2 O)
HELIX    1 AA1 THR A   25  CYS A   30  1                                   6
HELIX    2 AA2 THR A   31  LEU A   39  1                                   9
HELIX    3 AA3 PRO A  103  PHE A  106  5                                   4
HELIX    4 AA4 LEU A  127  MET A  132  1                                   6
HELIX    5 AA5 ALA A  151  ALA A  154  5                                   4
HELIX    6 AA6 ASP A  163  TYR A  172  1                                  10
HELIX    7 AA7 TYR A  172  TYR A  190  1                                  19
HELIX    8 AA8 SER A  206  GLN A  217  1                                  12
HELIX    9 AA9 ARG A  234  HIS A  242  1                                   9
HELIX   10 AB1 LEU A  243  ASP A  253  1                                  11
HELIX   11 AB2 PRO A  257  ASP A  273  1                                  17
HELIX   12 AB3 ALA A  274  GLY A  277  5                                   4
HELIX   13 AB4 ARG A  285  PHE A  293  1                                   9
HELIX   14 AB5 ASP A  294  GLU A  299  5                                   6
HELIX   15 AB6 SER A  319  ASN A  331  1                                  13
HELIX   16 AB7 ASP A  370  VAL A  381  1                                  12
HELIX   17 AB8 THR A  395  TYR A  411  1                                  17
HELIX   18 AB9 LEU A  421  ALA A  427  1                                   7
HELIX   19 AC1 THR A  444  TYR A  459  1                                  16
HELIX   20 AC2 ASP A  463  GLU A  473  1                                  11
HELIX   21 AC3 THR A  500  GLY A  512  1                                  13
HELIX   22 AC4 ASN A  555  TRP A  562  1                                   8
SHEET    1 AA1 9 ILE A  48  SER A  67  0
SHEET    2 AA1 9 TYR A  70  HIS A  86 -1  O  ASN A  79   N  GLU A  58
SHEET    3 AA1 9 VAL A  94  PRO A 101 -1  O  VAL A  94   N  TYR A  84
SHEET    4 AA1 9 ALA A 135  THR A 140 -1  O  SER A 137   N  TRP A  99
SHEET    5 AA1 9 ARG A 109  THR A 113  1  N  LEU A 111   O  GLY A 138
SHEET    6 AA1 9 TYR A 199  CYS A 205  1  O  TYR A 201   N  SER A 112
SHEET    7 AA1 9 GLY A 225  GLY A 229  1  O  ILE A 227   N  TYR A 202
SHEET    8 AA1 9 LYS A 430  GLY A 436  1  O  ILE A 432   N  ILE A 228
SHEET    9 AA1 9 TYR A 475  VAL A 480  1  O  ARG A 476   N  HIS A 433
SHEET    1 AA2 2 LEU A 156  ALA A 158  0
SHEET    2 AA2 2 THR A 161  LEU A 162 -1  O  THR A 161   N  LEU A 157
SHEET    1 AA3 2 PRO A 302  CYS A 305  0
SHEET    2 AA3 2 GLN A 314  THR A 317 -1  O  GLN A 314   N  CYS A 305
SHEET    1 AA4 2 GLN A 357  ASN A 359  0
SHEET    2 AA4 2 GLN A 364  GLY A 366 -1  O  GLY A 366   N  GLN A 357
SHEET    1 AA5 2 LEU A 518  THR A 521  0
SHEET    2 AA5 2 ASN A 531  LEU A 534 -1  O  LEU A 534   N  LEU A 518
SHEET    1 AA6 2 ARG A 540  THR A 544  0
SHEET    2 AA6 2 THR A 549  VAL A 553 -1  O  VAL A 553   N  ARG A 540
SSBOND   1 CYS A   30    CYS A   78                          1555   1555  2.24
SSBOND   2 CYS A  205    CYS A  486                          1555   1555  2.07
SSBOND   3 CYS A  259    CYS A  305                          1555   1555  2.07
SSBOND   4 CYS A  272    CYS A  289                          1555   1555  2.29
SSBOND   5 CYS A  535    CYS A  552                          1555   1555  2.16
LINK         ND2 ASN A  62                 C1  NAG F   1     1555   1555  1.45
LINK         ND2 ASN A  79                 C1  NAG C   1     1555   1555  1.46
LINK         ND2 ASN A 159                 C1  NAG A 601     1555   1555  1.46
LINK         ND2 ASN A 266                 C1  NAG G   1     1555   1555  1.48
LINK         ND2 ASN A 359                 C1  NAG A 602     1555   1555  1.44
LINK         ND2 ASN A 384                 C1  NAG E   1     1555   1555  1.42
LINK         ND2 ASN A 465                 C1  NAG D   1     1555   1555  1.42
LINK         ND2 ASN A 519                 C1  NAG B   1     1555   1555  1.45
LINK         O4  NAG B   1                 C1  NAG B   2     1555   1555  1.41
LINK         O4  NAG B   2                 C1  BMA B   3     1555   1555  1.49
LINK         O6  BMA B   3                 C1  MAN B   4     1555   1555  1.44
LINK         O3  BMA B   3                 C1  MAN B   8     1555   1555  1.48
LINK         O6  MAN B   4                 C1  MAN B   5     1555   1555  1.46
LINK         O3  MAN B   4                 C1  MAN B   7     1555   1555  1.50
LINK         O2  MAN B   5                 C1  MAN B   6     1555   1555  1.48
LINK         O4  NAG C   1                 C1  NAG C   2     1555   1555  1.46
LINK         O4  NAG C   2                 C1  BMA C   3     1555   1555  1.46
LINK         O3  BMA C   3                 C1  MAN C   4     1555   1555  1.46
LINK         O6  BMA C   3                 C1  MAN C   6     1555   1555  1.48
LINK         O2  MAN C   4                 C1  MAN C   5     1555   1555  1.48
LINK         O4  NAG D   1                 C1  NAG D   2     1555   1555  1.48
LINK         O4  NAG E   1                 C1  NAG E   2     1555   1555  1.48
LINK         O4  NAG F   1                 C1  NAG F   2     1555   1555  1.44
LINK         O4  NAG G   1                 C1  NAG G   2     1555   1555  1.44
LINK         O   THR A  57                NA    NA A 611     1555   1555  2.64
LINK         OG1 THR A  57                NA    NA A 611     1555   1555  2.60
LINK         OE2 GLU A  58                ZN    ZN A 607     1555   1555  2.07
LINK         OE2 GLU A  58                ZN    ZN A 607     1555  12544  2.07
LINK         OD2 ASP A 196                ZN    ZN A 606     1555   1555  2.07
LINK         OD2 ASP A 196                ZN    ZN A 606     1555  10555  2.07
LINK         O   ASP A 273                CA    CA A 604     1555   1555  2.41
LINK         OD1 ASP A 273                CA    CA A 604     1555   1555  2.42
LINK         OD1 ASP A 276                CA    CA A 604     1555   1555  2.32
LINK         OD2 ASP A 276                CA    CA A 604     1555   1555  2.44
LINK         O   LYS A 278                CA    CA A 604     1555   1555  2.34
LINK         OD1 ASP A 280                CA    CA A 604     1555   1555  2.50
LINK         O   VAL A 282                CA    CA A 604     1555   1555  2.38
LINK         NE2 HIS A 425                ZN    ZN A 608     1555   1555  2.08
LINK         OE1 GLU A 469                ZN    ZN A 605     1555   1555  2.69
LINK         OE2 GLU A 469                ZN    ZN A 605     1555   1555  1.86
LINK         OE1 GLU A 469                ZN    ZN A 605     1555  10555  2.69
LINK         OE2 GLU A 469                ZN    ZN A 605     1555  10555  1.86
LINK         OE1 GLU A 473                ZN    ZN A 605     1555   1555  2.01
LINK         OE1 GLU A 473                ZN    ZN A 605     1555  10555  2.01
LINK        CA    CA A 604                 O   HOH A 813     1555   1555  2.59
LINK        ZN    ZN A 606                 O   HOH A 925     1555   1555  2.21
LINK        ZN    ZN A 606                 O   HOH A 925     1555  10555  2.21
LINK        ZN    ZN A 606                 O   HOH A1066     1555   1555  2.13
LINK        ZN    ZN A 606                 O   HOH A1066     1555  10555  2.13
LINK        ZN    ZN A 607                 O   HOH A 948     1555   1555  2.10
LINK        ZN    ZN A 607                 O   HOH A 948     1555  12544  2.10
LINK        ZN    ZN A 607                 O   HOH A1087     1555   1555  2.17
LINK        ZN    ZN A 607                 O   HOH A1087     1555  12544  2.17
LINK        ZN    ZN A 608                 O   HOH A 935     1555   1555  2.25
LINK        ZN    ZN A 608                 O   HOH A1250     1555   1555  2.34
LINK        ZN    ZN A 608                 O   HOH A1275     1555   1555  2.44
LINK        ZN    ZN A 608                 O   HOH A1300     1555   1555  2.53
LINK        NA    NA A 611                 O   HOH A 823     1555  12544  2.16
LINK        NA    NA A 611                 O   HOH A 907     1555   1555  2.70
LINK        NA    NA A 611                 O   HOH A1077     1555   1555  2.82
LINK        NA    NA A 611                 O   HOH A1145     1555   1555  2.67
CISPEP   1 TRP A  537    PRO A  538          0         2.83
CRYST1  170.920  170.920  111.061  90.00  90.00 120.00 P 65 2 2     12
ORIGX1      1.000000  0.000000  0.000000        0.00000
ORIGX2      0.000000  1.000000  0.000000        0.00000
ORIGX3      0.000000  0.000000  1.000000        0.00000
SCALE1      0.005851  0.003378  0.000000        0.00000
SCALE2      0.000000  0.006756  0.000000        0.00000
SCALE3      0.000000  0.000000  0.009004        0.00000
TER    8478      TYR A 574
MASTER      481    0   34   22   19    0    0    6 5392    1  694   43
END