longtext: 7wan-pdb

content
HEADER    HYDROLASE                               14-DEC-21   7WAN
TITLE     CRYSTAL STRUCTURE OF HALOTAG COMPLEXED WITH UL2
COMPND    MOL_ID: 1;
COMPND   2 MOLECULE: HALOALKANE DEHALOGENASE;
COMPND   3 CHAIN: A;
COMPND   4 EC: 3.8.1.5;
COMPND   5 ENGINEERED: YES;
COMPND   6 MUTATION: YES
SOURCE    MOL_ID: 1;
SOURCE   2 ORGANISM_SCIENTIFIC: RHODOCOCCUS SP.;
SOURCE   3 ORGANISM_TAXID: 1831;
SOURCE   4 GENE: DHAA;
SOURCE   5 EXPRESSION_SYSTEM: ESCHERICHIA COLI BL21(DE3);
SOURCE   6 EXPRESSION_SYSTEM_TAXID: 469008
KEYWDS    HALOTAG, HALOALKANE DEHALOGENASE, HYDROLASE
EXPDTA    X-RAY DIFFRACTION
AUTHOR    M.PRATYUSH,M.KANG,H.LEE,C.LEE,H.RHEE
REVDAT   1   02-FEB-22 7WAN    0
JRNL        AUTH   P.K.MISHRA,M.G.KANG,H.LEE,S.KIM,S.CHOI,N.SHARMA,C.M.PARK,
JRNL        AUTH 2 J.KO,C.LEE,J.K.SEO,H.W.RHEE
JRNL        TITL   A CHEMICAL TOOL FOR BLUE LIGHT-INDUCIBLE PROXIMITY
JRNL        TITL 2 PHOTO-CROSSLINKING IN LIVE CELLS
JRNL        REF    CHEM SCI                                   2022
JRNL        REFN                   ESSN 2041-6539
JRNL        DOI    10.1039/D1SC04871F
REMARK   2
REMARK   2 RESOLUTION.    2.28 ANGSTROMS.
REMARK   3
REMARK   3 REFINEMENT.
REMARK   3   PROGRAM     : PHENIX 1.14_3260
REMARK   3   AUTHORS     : PAUL ADAMS,PAVEL AFONINE,VINCENT CHEN,IAN
REMARK   3               : DAVIS,KRESHNA GOPAL,RALF GROSSE-KUNSTLEVE,
REMARK   3               : LI-WEI HUNG,ROBERT IMMORMINO,TOM IOERGER,
REMARK   3               : AIRLIE MCCOY,ERIK MCKEE,NIGEL MORIARTY,
REMARK   3               : REETAL PAI,RANDY READ,JANE RICHARDSON,
REMARK   3               : DAVID RICHARDSON,TOD ROMO,JIM SACCHETTINI,
REMARK   3               : NICHOLAS SAUTER,JACOB SMITH,LAURENT
REMARK   3               : STORONI,TOM TERWILLIGER,PETER ZWART
REMARK   3
REMARK   3    REFINEMENT TARGET : ML
REMARK   3
REMARK   3  DATA USED IN REFINEMENT.
REMARK   3   RESOLUTION RANGE HIGH (ANGSTROMS) : 2.28
REMARK   3   RESOLUTION RANGE LOW  (ANGSTROMS) : 32.28
REMARK   3   MIN(FOBS/SIGMA_FOBS)              : 1.400
REMARK   3   COMPLETENESS FOR RANGE        (%) : 97.2
REMARK   3   NUMBER OF REFLECTIONS             : 11713
REMARK   3
REMARK   3  FIT TO DATA USED IN REFINEMENT.
REMARK   3   R VALUE     (WORKING + TEST SET) : 0.180
REMARK   3   R VALUE            (WORKING SET) : 0.178
REMARK   3   FREE R VALUE                     : 0.228
REMARK   3   FREE R VALUE TEST SET SIZE   (%) : 5.010
REMARK   3   FREE R VALUE TEST SET COUNT      : 587
REMARK   3
REMARK   3  FIT TO DATA USED IN REFINEMENT (IN BINS).
REMARK   3   BIN  RESOLUTION RANGE  COMPL.    NWORK NFREE   RWORK  RFREE
REMARK   3     1 32.2840 -  3.6242    1.00     2891   153  0.1492 0.2018
REMARK   3     2  3.6242 -  2.8772    0.99     2826   150  0.1785 0.2304
REMARK   3     3  2.8772 -  2.5137    0.98     2806   143  0.2101 0.2431
REMARK   3     4  2.5137 -  2.2840    0.92     2603   141  0.2169 0.2801
REMARK   3
REMARK   3  BULK SOLVENT MODELLING.
REMARK   3   METHOD USED        : FLAT BULK SOLVENT MODEL
REMARK   3   SOLVENT RADIUS     : 1.11
REMARK   3   SHRINKAGE RADIUS   : 0.90
REMARK   3   K_SOL              : NULL
REMARK   3   B_SOL              : NULL
REMARK   3
REMARK   3  ERROR ESTIMATES.
REMARK   3   COORDINATE ERROR (MAXIMUM-LIKELIHOOD BASED)     : 0.230
REMARK   3   PHASE ERROR (DEGREES, MAXIMUM-LIKELIHOOD BASED) : 22.250
REMARK   3
REMARK   3  B VALUES.
REMARK   3   FROM WILSON PLOT           (A**2) : NULL
REMARK   3   MEAN B VALUE      (OVERALL, A**2) : 21.47
REMARK   3   OVERALL ANISOTROPIC B VALUE.
REMARK   3    B11 (A**2) : NULL
REMARK   3    B22 (A**2) : NULL
REMARK   3    B33 (A**2) : NULL
REMARK   3    B12 (A**2) : NULL
REMARK   3    B13 (A**2) : NULL
REMARK   3    B23 (A**2) : NULL
REMARK   3
REMARK   3  TWINNING INFORMATION.
REMARK   3   FRACTION: NULL
REMARK   3   OPERATOR: NULL
REMARK   3
REMARK   3  DEVIATIONS FROM IDEAL VALUES.
REMARK   3                 RMSD          COUNT
REMARK   3   BOND      :   NULL           NULL
REMARK   3   ANGLE     :   NULL           NULL
REMARK   3   CHIRALITY :   NULL           NULL
REMARK   3   PLANARITY :   NULL           NULL
REMARK   3   DIHEDRAL  :   NULL           NULL
REMARK   3
REMARK   3  TLS DETAILS
REMARK   3   NUMBER OF TLS GROUPS  : NULL
REMARK   3
REMARK   3  NCS DETAILS
REMARK   3   NUMBER OF NCS GROUPS : NULL
REMARK   3
REMARK   3  OTHER REFINEMENT REMARKS: NULL
REMARK   4
REMARK   4 7WAN COMPLIES WITH FORMAT V. 3.30, 13-JUL-11
REMARK 100
REMARK 100 THIS ENTRY HAS BEEN PROCESSED BY PDBJ.
REMARK 100 THE DEPOSITION ID IS D_1300025917.
REMARK 200
REMARK 200 EXPERIMENTAL DETAILS
REMARK 200  EXPERIMENT TYPE                : X-RAY DIFFRACTION
REMARK 200  DATE OF DATA COLLECTION        : 02-APR-16
REMARK 200  TEMPERATURE           (KELVIN) : 100
REMARK 200  PH                             : NULL
REMARK 200  NUMBER OF CRYSTALS USED        : 1
REMARK 200
REMARK 200  SYNCHROTRON              (Y/N) : Y
REMARK 200  RADIATION SOURCE               : PAL/PLS
REMARK 200  BEAMLINE                       : 7A (6B, 6C1)
REMARK 200  X-RAY GENERATOR MODEL          : NULL
REMARK 200  MONOCHROMATIC OR LAUE    (M/L) : M
REMARK 200  WAVELENGTH OR RANGE        (A) : 0.97933
REMARK 200  MONOCHROMATOR                  : NULL
REMARK 200  OPTICS                         : NULL
REMARK 200
REMARK 200  DETECTOR TYPE                  : CCD
REMARK 200  DETECTOR MANUFACTURER          : ADSC QUANTUM 270
REMARK 200  INTENSITY-INTEGRATION SOFTWARE : HKL-2000
REMARK 200  DATA SCALING SOFTWARE          : HKL-2000
REMARK 200
REMARK 200  NUMBER OF UNIQUE REFLECTIONS   : 11723
REMARK 200  RESOLUTION RANGE HIGH      (A) : 2.280
REMARK 200  RESOLUTION RANGE LOW       (A) : 50.000
REMARK 200  REJECTION CRITERIA  (SIGMA(I)) : NULL
REMARK 200
REMARK 200 OVERALL.
REMARK 200  COMPLETENESS FOR RANGE     (%) : 97.9
REMARK 200  DATA REDUNDANCY                : 3.000
REMARK 200  R MERGE                    (I) : 0.12400
REMARK 200  R SYM                      (I) : NULL
REMARK 200   FOR THE DATA SET  : 12.8000
REMARK 200
REMARK 200 IN THE HIGHEST RESOLUTION SHELL.
REMARK 200  HIGHEST RESOLUTION SHELL, RANGE HIGH (A) : 2.30
REMARK 200  HIGHEST RESOLUTION SHELL, RANGE LOW  (A) : 2.34
REMARK 200  COMPLETENESS FOR SHELL     (%) : NULL
REMARK 200  DATA REDUNDANCY IN SHELL       : NULL
REMARK 200  R MERGE FOR SHELL          (I) : 0.28900
REMARK 200  R SYM FOR SHELL            (I) : NULL
REMARK 200   FOR SHELL         : NULL
REMARK 200
REMARK 200 DIFFRACTION PROTOCOL: SINGLE WAVELENGTH
REMARK 200 METHOD USED TO DETERMINE THE STRUCTURE: MOLECULAR REPLACEMENT
REMARK 200 SOFTWARE USED: PHENIX
REMARK 200 STARTING MODEL: 5Y2X
REMARK 200
REMARK 200 REMARK: NULL
REMARK 280
REMARK 280 CRYSTAL
REMARK 280 SOLVENT CONTENT, VS   (%): 38.09
REMARK 280 MATTHEWS COEFFICIENT, VM (ANGSTROMS**3/DA): 1.99
REMARK 280
REMARK 280 CRYSTALLIZATION CONDITIONS: 25% PEG 8K, 0.1 M MES PH 6.5, 0.2 M NA
REMARK 280  -ACETATE, VAPOR DIFFUSION, HANGING DROP, TEMPERATURE 293K
REMARK 290
REMARK 290 CRYSTALLOGRAPHIC SYMMETRY
REMARK 290 SYMMETRY OPERATORS FOR SPACE GROUP: P 1 21 1
REMARK 290
REMARK 290      SYMOP   SYMMETRY
REMARK 290     NNNMMM   OPERATOR
REMARK 290       1555   X,Y,Z
REMARK 290       2555   -X,Y+1/2,-Z
REMARK 290
REMARK 290     WHERE NNN -> OPERATOR NUMBER
REMARK 290           MMM -> TRANSLATION VECTOR
REMARK 290
REMARK 290 CRYSTALLOGRAPHIC SYMMETRY TRANSFORMATIONS
REMARK 290 THE FOLLOWING TRANSFORMATIONS OPERATE ON THE ATOM/HETATM
REMARK 290 RECORDS IN THIS ENTRY TO PRODUCE CRYSTALLOGRAPHICALLY
REMARK 290 RELATED MOLECULES.
REMARK 290   SMTRY1   1  1.000000  0.000000  0.000000        0.00000
REMARK 290   SMTRY2   1  0.000000  1.000000  0.000000        0.00000
REMARK 290   SMTRY3   1  0.000000  0.000000  1.000000        0.00000
REMARK 290   SMTRY1   2 -1.000000  0.000000  0.000000        0.00000
REMARK 290   SMTRY2   2  0.000000  1.000000  0.000000       36.38200
REMARK 290   SMTRY3   2  0.000000  0.000000 -1.000000        0.00000
REMARK 290
REMARK 290 REMARK: NULL
REMARK 300
REMARK 300 BIOMOLECULE: 1
REMARK 300 SEE REMARK 350 FOR THE AUTHOR PROVIDED AND/OR PROGRAM
REMARK 300 GENERATED ASSEMBLY INFORMATION FOR THE STRUCTURE IN
REMARK 300 THIS ENTRY. THE REMARK MAY ALSO PROVIDE INFORMATION ON
REMARK 300 BURIED SURFACE AREA.
REMARK 350
REMARK 350 COORDINATES FOR A COMPLETE MULTIMER REPRESENTING THE KNOWN
REMARK 350 BIOLOGICALLY SIGNIFICANT OLIGOMERIZATION STATE OF THE
REMARK 350 MOLECULE CAN BE GENERATED BY APPLYING BIOMT TRANSFORMATIONS
REMARK 350 GIVEN BELOW.  BOTH NON-CRYSTALLOGRAPHIC AND
REMARK 350 CRYSTALLOGRAPHIC OPERATIONS ARE GIVEN.
REMARK 350
REMARK 350 BIOMOLECULE: 1
REMARK 350 AUTHOR DETERMINED BIOLOGICAL UNIT: MONOMERIC
REMARK 350 SOFTWARE DETERMINED QUATERNARY STRUCTURE: MONOMERIC
REMARK 350 SOFTWARE USED: PISA
REMARK 350 TOTAL BURIED SURFACE AREA: 130 ANGSTROM**2
REMARK 350 SURFACE AREA OF THE COMPLEX: 11050 ANGSTROM**2
REMARK 350 CHANGE IN SOLVENT FREE ENERGY: -12.0 KCAL/MOL
REMARK 350 APPLY THE FOLLOWING TO CHAINS: A
REMARK 350   BIOMT1   1  1.000000  0.000000  0.000000        0.00000
REMARK 350   BIOMT2   1  0.000000  1.000000  0.000000        0.00000
REMARK 350   BIOMT3   1  0.000000  0.000000  1.000000        0.00000
REMARK 465
REMARK 465 MISSING RESIDUES
REMARK 465 THE FOLLOWING RESIDUES WERE NOT LOCATED IN THE
REMARK 465 EXPERIMENT. (M=MODEL NUMBER; RES=RESIDUE NAME; C=CHAIN
REMARK 465 IDENTIFIER; SSSEQ=SEQUENCE NUMBER; I=INSERTION CODE.)
REMARK 465
REMARK 465   M RES C SSSEQI
REMARK 465     SER A    -2
REMARK 465     GLY A    -1
REMARK 465     SER A     0
REMARK 465     ALA A     1
REMARK 465     GLU A     2
REMARK 465     GLU A   293
REMARK 465     ILE A   294
REMARK 465     SER A   295
REMARK 465     GLY A   296
REMARK 500
REMARK 500 GEOMETRY AND STEREOCHEMISTRY
REMARK 500 SUBTOPIC: CLOSE CONTACTS IN SAME ASYMMETRIC UNIT
REMARK 500
REMARK 500 THE FOLLOWING ATOMS ARE IN CLOSE CONTACT.
REMARK 500
REMARK 500  ATM1  RES C  SSEQI   ATM2  RES C  SSEQI           DISTANCE
REMARK 500   OD1  ASP A   105     C26  8MS A   301              1.38
REMARK 500   OD1  ASP A   105     C27  8MS A   301              2.01
REMARK 500   O    HOH A   476     O    HOH A   490              2.12
REMARK 500   O    HOH A   475     O    HOH A   489              2.16
REMARK 500
REMARK 500 REMARK: NULL
REMARK 500
REMARK 500 GEOMETRY AND STEREOCHEMISTRY
REMARK 500 SUBTOPIC: TORSION ANGLES
REMARK 500
REMARK 500 TORSION ANGLES OUTSIDE THE EXPECTED RAMACHANDRAN REGIONS:
REMARK 500 (M=MODEL NUMBER; RES=RESIDUE NAME; C=CHAIN IDENTIFIER;
REMARK 500 SSEQ=SEQUENCE NUMBER; I=INSERTION CODE).
REMARK 500
REMARK 500 STANDARD TABLE:
REMARK 500 FORMAT:(10X,I3,1X,A3,1X,A1,I4,A1,4X,F7.2,3X,F7.2)
REMARK 500
REMARK 500 EXPECTED VALUES: GJ KLEYWEGT AND TA JONES (1996). PHI/PSI-
REMARK 500 CHOLOGY: RAMACHANDRAN REVISITED. STRUCTURE 4, 1395 - 1400
REMARK 500
REMARK 500  M RES CSSEQI        PSI       PHI
REMARK 500    PHE A   7       79.01   -119.43
REMARK 500    PRO A  41       40.34   -104.89
REMARK 500    THR A  42     -152.75   -103.10
REMARK 500    GLU A  97      -76.13   -106.03
REMARK 500    ASP A 105     -131.85     60.89
REMARK 500    ARG A 152       45.88    -86.05
REMARK 500    ASP A 155      -70.79   -103.19
REMARK 500    VAL A 244      -70.12   -129.25
REMARK 500    LEU A 270     -102.57   -113.42
REMARK 500    SER A 290       -3.96    -59.97
REMARK 500
REMARK 500 REMARK: NULL
DBREF  7WAN A    1   292  UNP    P0A3G3   DHAA_RHOSO       2    293
SEQADV 7WAN SER A   -2  UNP  P0A3G3              EXPRESSION TAG
SEQADV 7WAN GLY A   -1  UNP  P0A3G3              EXPRESSION TAG
SEQADV 7WAN SER A    0  UNP  P0A3G3              EXPRESSION TAG
SEQADV 7WAN ALA A    1  UNP  P0A3G3    SER     2 ENGINEERED MUTATION
SEQADV 7WAN VAL A   46  UNP  P0A3G3    LEU    47 ENGINEERED MUTATION
SEQADV 7WAN THR A   57  UNP  P0A3G3    SER    58 ENGINEERED MUTATION
SEQADV 7WAN GLY A   77  UNP  P0A3G3    ASP    78 ENGINEERED MUTATION
SEQADV 7WAN PHE A   86  UNP  P0A3G3    TYR    87 ENGINEERED MUTATION
SEQADV 7WAN MET A   87  UNP  P0A3G3    LEU    88 ENGINEERED MUTATION
SEQADV 7WAN PHE A  127  UNP  P0A3G3    CYS   128 ENGINEERED MUTATION
SEQADV 7WAN THR A  154  UNP  P0A3G3    ALA   155 ENGINEERED MUTATION
SEQADV 7WAN LYS A  159  UNP  P0A3G3    GLU   160 ENGINEERED MUTATION
SEQADV 7WAN VAL A  166  UNP  P0A3G3    ALA   167 ENGINEERED MUTATION
SEQADV 7WAN THR A  171  UNP  P0A3G3    ALA   172 ENGINEERED MUTATION
SEQADV 7WAN CYS A  174  UNP  P0A3G3    LYS   175 ENGINEERED MUTATION
SEQADV 7WAN GLY A  175  UNP  P0A3G3    CYS   176 ENGINEERED MUTATION
SEQADV 7WAN ASN A  194  UNP  P0A3G3    LYS   195 ENGINEERED MUTATION
SEQADV 7WAN GLU A  223  UNP  P0A3G3    ALA   224 ENGINEERED MUTATION
SEQADV 7WAN ASP A  226  UNP  P0A3G3    ASN   227 ENGINEERED MUTATION
SEQADV 7WAN LYS A  256  UNP  P0A3G3    GLU   257 ENGINEERED MUTATION
SEQADV 7WAN ALA A  263  UNP  P0A3G3    THR   264 ENGINEERED MUTATION
SEQADV 7WAN ASN A  271  UNP  P0A3G3    HIS   272 ENGINEERED MUTATION
SEQADV 7WAN LEU A  272  UNP  P0A3G3    TYR   273 ENGINEERED MUTATION
SEQADV 7WAN SER A  290  UNP  P0A3G3    PRO   291 ENGINEERED MUTATION
SEQADV 7WAN THR A  291  UNP  P0A3G3    ALA   292 ENGINEERED MUTATION
SEQADV 7WAN GLU A  293  UNP  P0A3G3              EXPRESSION TAG
SEQADV 7WAN ILE A  294  UNP  P0A3G3              EXPRESSION TAG
SEQADV 7WAN SER A  295  UNP  P0A3G3              EXPRESSION TAG
SEQADV 7WAN GLY A  296  UNP  P0A3G3              EXPRESSION TAG
SEQRES   1 A  299  SER GLY SER ALA GLU ILE GLY THR GLY PHE PRO PHE ASP
SEQRES   2 A  299  PRO HIS TYR VAL GLU VAL LEU GLY GLU ARG MET HIS TYR
SEQRES   3 A  299  VAL ASP VAL GLY PRO ARG ASP GLY THR PRO VAL LEU PHE
SEQRES   4 A  299  LEU HIS GLY ASN PRO THR SER SER TYR VAL TRP ARG ASN
SEQRES   5 A  299  ILE ILE PRO HIS VAL ALA PRO THR HIS ARG CYS ILE ALA
SEQRES   6 A  299  PRO ASP LEU ILE GLY MET GLY LYS SER ASP LYS PRO ASP
SEQRES   7 A  299  LEU GLY TYR PHE PHE ASP ASP HIS VAL ARG PHE MET ASP
SEQRES   8 A  299  ALA PHE ILE GLU ALA LEU GLY LEU GLU GLU VAL VAL LEU
SEQRES   9 A  299  VAL ILE HIS ASP TRP GLY SER ALA LEU GLY PHE HIS TRP
SEQRES  10 A  299  ALA LYS ARG ASN PRO GLU ARG VAL LYS GLY ILE ALA PHE
SEQRES  11 A  299  MET GLU PHE ILE ARG PRO ILE PRO THR TRP ASP GLU TRP
SEQRES  12 A  299  PRO GLU PHE ALA ARG GLU THR PHE GLN ALA PHE ARG THR
SEQRES  13 A  299  THR ASP VAL GLY ARG LYS LEU ILE ILE ASP GLN ASN VAL
SEQRES  14 A  299  PHE ILE GLU GLY THR LEU PRO CYS GLY VAL VAL ARG PRO
SEQRES  15 A  299  LEU THR GLU VAL GLU MET ASP HIS TYR ARG GLU PRO PHE
SEQRES  16 A  299  LEU ASN PRO VAL ASP ARG GLU PRO LEU TRP ARG PHE PRO
SEQRES  17 A  299  ASN GLU LEU PRO ILE ALA GLY GLU PRO ALA ASN ILE VAL
SEQRES  18 A  299  ALA LEU VAL GLU GLU TYR MET ASP TRP LEU HIS GLN SER
SEQRES  19 A  299  PRO VAL PRO LYS LEU LEU PHE TRP GLY THR PRO GLY VAL
SEQRES  20 A  299  LEU ILE PRO PRO ALA GLU ALA ALA ARG LEU ALA LYS SER
SEQRES  21 A  299  LEU PRO ASN CYS LYS ALA VAL ASP ILE GLY PRO GLY LEU
SEQRES  22 A  299  ASN LEU LEU GLN GLU ASP ASN PRO ASP LEU ILE GLY SER
SEQRES  23 A  299  GLU ILE ALA ARG TRP LEU SER THR LEU GLU ILE SER GLY
HET    8MS  A 301      27
HET     CL  A 302       1
HETNAM     8MS (R)-[4-(2-AZANYLHYDRAZINYL)PHENYL]-[2-[2-(2-
HETNAM   2 8MS  HEXOXYETHOXY)ETHOXY]ETHYLAMINO]METHANOL
HETNAM      CL CHLORIDE ION
FORMUL   2  8MS    C19 H36 N4 O4
FORMUL   3   CL    CL 1-
FORMUL   4  HOH   *96(H2 O)
HELIX    1 AA1 SER A   43  ARG A   48  5                                   6
HELIX    2 AA2 ILE A   50  VAL A   54  5                                   5
HELIX    3 AA3 PHE A   79  LEU A   94  1                                  16
HELIX    4 AA4 ASP A  105  ASN A  118  1                                  14
HELIX    5 AA5 THR A  136  TRP A  140  5                                   5
HELIX    6 AA6 PRO A  141  ARG A  152  1                                  12
HELIX    7 AA7 ASP A  155  ILE A  162  1                                   8
HELIX    8 AA8 ASN A  165  GLY A  170  1                                   6
HELIX    9 AA9 LEU A  172  VAL A  176  5                                   5
HELIX   10 AB1 THR A  181  GLU A  190  1                                  10
HELIX   11 AB2 PRO A  191  LEU A  193  5                                   3
HELIX   12 AB3 ASN A  194  ASP A  197  5                                   4
HELIX   13 AB4 ARG A  198  LEU A  208  1                                  11
HELIX   14 AB5 PRO A  214  HIS A  229  1                                  16
HELIX   15 AB6 PRO A  247  LEU A  258  1                                  12
HELIX   16 AB7 LEU A  272  ASN A  277  1                                   6
HELIX   17 AB8 ASN A  277  SER A  290  1                                  14
SHEET    1 AA1 8 HIS A  12  VAL A  16  0
SHEET    2 AA1 8 GLU A  19  VAL A  26 -1  O  MET A  21   N  VAL A  14
SHEET    3 AA1 8 CYS A  60  PRO A  63 -1  O  CYS A  60   N  VAL A  26
SHEET    4 AA1 8 VAL A  34  LEU A  37  1  N  PHE A  36   O  ILE A  61
SHEET    5 AA1 8 VAL A  99  HIS A 104  1  O  VAL A 100   N  LEU A  35
SHEET    6 AA1 8 VAL A 122  MET A 128  1  O  ALA A 126   N  LEU A 101
SHEET    7 AA1 8 LYS A 235  PRO A 242  1  O  LEU A 236   N  PHE A 127
SHEET    8 AA1 8 CYS A 261  GLY A 269  1  O  ILE A 266   N  TRP A 239
CISPEP   1 ASN A   40    PRO A   41          0        -3.34
CISPEP   2 GLU A  213    PRO A  214          0        -3.71
CISPEP   3 THR A  241    PRO A  242          0        -1.75
CRYST1   43.906   72.764   44.432  90.00 109.30  90.00 P 1 21 1      2
ORIGX1      1.000000  0.000000  0.000000        0.00000
ORIGX2      0.000000  1.000000  0.000000        0.00000
ORIGX3      0.000000  0.000000  1.000000        0.00000
SCALE1      0.022776  0.000000  0.007976        0.00000
SCALE2      0.000000  0.013743  0.000000        0.00000
SCALE3      0.000000  0.000000  0.023847        0.00000
TER    2327      LEU A 292
MASTER      243    0    2   17    8    0    0    6 2450    1   27   23
END