longtext: 8vb3-pdb

content
HEADER    HYDROLASE                               11-DEC-23   8VB3
TITLE     DIENELACTONE HYDROLASE FROM SOLIMONAS FLUMINIS
COMPND    MOL_ID: 1;
COMPND   2 MOLECULE: DIENELACTONE HYDROLASE;
COMPND   3 CHAIN: A, B;
COMPND   4 ENGINEERED: YES
SOURCE    MOL_ID: 1;
SOURCE   2 ORGANISM_SCIENTIFIC: SOLIMONAS FLUMINIS;
SOURCE   3 ORGANISM_TAXID: 2086571;
SOURCE   4 GENE: C3942_20560;
SOURCE   5 EXPRESSION_SYSTEM: ESCHERICHIA COLI BL21(DE3);
SOURCE   6 EXPRESSION_SYSTEM_TAXID: 469008
KEYWDS    HYDROLASE, DIENELACTONE, METAGENOMIC, SOLIMONAS FLUMINIS, ESTERASE
EXPDTA    X-RAY DIFFRACTION
AUTHOR    J.D.F.SCHNETTLER FERNANDEZ,E.C.CAMPBELL,F.HOLLFELDER
REVDAT   1   18-DEC-24 8VB3    0
JRNL        AUTH   J.D.F.SCHNETTLER FERNANDEZ,E.C.CAMPBELL,R.KHASHIEV,
JRNL        AUTH 2 J.O.KLEIN,F.HOLLFELDER
JRNL        TITL   METAL-INDEPENDENT ORGANOPHOSPHATE HYDROLYSIS IN A PROTEIN
JRNL        TITL 2 FAMILY POSSESSING A CATALYTIC TRIAD
JRNL        REF    TO BE PUBLISHED
JRNL        REFN
REMARK   2
REMARK   2 RESOLUTION.    1.45 ANGSTROMS.
REMARK   3
REMARK   3 REFINEMENT.
REMARK   3   PROGRAM     : PHENIX 1.20.1_4487
REMARK   3   AUTHORS     : PAUL ADAMS,PAVEL AFONINE,VINCENT CHEN,IAN
REMARK   3               : DAVIS,KRESHNA GOPAL,RALF GROSSE-KUNSTLEVE,
REMARK   3               : LI-WEI HUNG,ROBERT IMMORMINO,TOM IOERGER,
REMARK   3               : AIRLIE MCCOY,ERIK MCKEE,NIGEL MORIARTY,
REMARK   3               : REETAL PAI,RANDY READ,JANE RICHARDSON,
REMARK   3               : DAVID RICHARDSON,TOD ROMO,JIM SACCHETTINI,
REMARK   3               : NICHOLAS SAUTER,JACOB SMITH,LAURENT
REMARK   3               : STORONI,TOM TERWILLIGER,PETER ZWART
REMARK   3
REMARK   3    REFINEMENT TARGET : GEOSTD + MONOMER LIBRARY + CDL V1.2
REMARK   3
REMARK   3  DATA USED IN REFINEMENT.
REMARK   3   RESOLUTION RANGE HIGH (ANGSTROMS) : 1.45
REMARK   3   RESOLUTION RANGE LOW  (ANGSTROMS) : 39.63
REMARK   3   MIN(FOBS/SIGMA_FOBS)              : 1.400
REMARK   3   COMPLETENESS FOR RANGE        (%) : 99.7
REMARK   3   NUMBER OF REFLECTIONS             : 86212
REMARK   3
REMARK   3  FIT TO DATA USED IN REFINEMENT.
REMARK   3   R VALUE     (WORKING + TEST SET) : 0.159
REMARK   3   R VALUE            (WORKING SET) : 0.158
REMARK   3   FREE R VALUE                     : 0.186
REMARK   3   FREE R VALUE TEST SET SIZE   (%) : 5.080
REMARK   3   FREE R VALUE TEST SET COUNT      : 4382
REMARK   3
REMARK   3  FIT TO DATA USED IN REFINEMENT (IN BINS).
REMARK   3   BIN  RESOLUTION RANGE  COMPL.    NWORK NFREE   RWORK  RFREE
REMARK   3     1 39.6300 -  4.5000    1.00     2784   166  0.1621 0.1899
REMARK   3     2  4.5000 -  3.5800    1.00     2774   146  0.1403 0.1759
REMARK   3     3  3.5700 -  3.1200    1.00     2737   153  0.1595 0.1844
REMARK   3     4  3.1200 -  2.8400    1.00     2735   144  0.1684 0.1947
REMARK   3     5  2.8400 -  2.6300    1.00     2740   146  0.1719 0.1861
REMARK   3     6  2.6300 -  2.4800    1.00     2749   151  0.1698 0.1932
REMARK   3     7  2.4800 -  2.3600    1.00     2730   142  0.1662 0.1821
REMARK   3     8  2.3600 -  2.2500    1.00     2738   155  0.1509 0.1867
REMARK   3     9  2.2500 -  2.1700    1.00     2741   142  0.1562 0.1778
REMARK   3    10  2.1700 -  2.0900    1.00     2726   150  0.1563 0.1870
REMARK   3    11  2.0900 -  2.0300    1.00     2750   153  0.1454 0.1829
REMARK   3    12  2.0300 -  1.9700    1.00     2721   147  0.1470 0.1549
REMARK   3    13  1.9700 -  1.9200    1.00     2699   146  0.1545 0.1890
REMARK   3    14  1.9200 -  1.8700    1.00     2756   136  0.1643 0.2076
REMARK   3    15  1.8700 -  1.8300    1.00     2683   149  0.1623 0.1879
REMARK   3    16  1.8300 -  1.7900    1.00     2763   160  0.1536 0.1631
REMARK   3    17  1.7900 -  1.7500    1.00     2682   141  0.1512 0.1727
REMARK   3    18  1.7500 -  1.7200    1.00     2771   150  0.1483 0.1873
REMARK   3    19  1.7200 -  1.6900    1.00     2717   130  0.1575 0.2382
REMARK   3    20  1.6900 -  1.6600    1.00     2719   134  0.1458 0.1735
REMARK   3    21  1.6600 -  1.6300    1.00     2776   108  0.1415 0.1643
REMARK   3    22  1.6300 -  1.6100    1.00     2723   114  0.1500 0.1933
REMARK   3    23  1.6100 -  1.5800    1.00     2728   156  0.1526 0.1832
REMARK   3    24  1.5800 -  1.5600    0.99     2733   158  0.1628 0.2005
REMARK   3    25  1.5600 -  1.5400    1.00     2667   149  0.1711 0.2215
REMARK   3    26  1.5400 -  1.5200    0.99     2710   165  0.1665 0.2143
REMARK   3    27  1.5200 -  1.5000    0.99     2716   145  0.1714 0.1909
REMARK   3    28  1.5000 -  1.4800    0.99     2653   152  0.1759 0.2005
REMARK   3    29  1.4800 -  1.4700    0.99     2712   149  0.1807 0.1947
REMARK   3    30  1.4700 -  1.4500    0.99     2697   145  0.1829 0.2309
REMARK   3
REMARK   3  BULK SOLVENT MODELLING.
REMARK   3   METHOD USED        : FLAT BULK SOLVENT MODEL
REMARK   3   SOLVENT RADIUS     : 1.10
REMARK   3   SHRINKAGE RADIUS   : 0.90
REMARK   3   K_SOL              : NULL
REMARK   3   B_SOL              : NULL
REMARK   3
REMARK   3  ERROR ESTIMATES.
REMARK   3   COORDINATE ERROR (MAXIMUM-LIKELIHOOD BASED)     : 0.115
REMARK   3   PHASE ERROR (DEGREES, MAXIMUM-LIKELIHOOD BASED) : 20.450
REMARK   3
REMARK   3  B VALUES.
REMARK   3   FROM WILSON PLOT           (A**2) : 15.15
REMARK   3   MEAN B VALUE      (OVERALL, A**2) : 24.11
REMARK   3   OVERALL ANISOTROPIC B VALUE.
REMARK   3    B11 (A**2) : NULL
REMARK   3    B22 (A**2) : NULL
REMARK   3    B33 (A**2) : NULL
REMARK   3    B12 (A**2) : NULL
REMARK   3    B13 (A**2) : NULL
REMARK   3    B23 (A**2) : NULL
REMARK   3
REMARK   3  TWINNING INFORMATION.
REMARK   3   FRACTION: NULL
REMARK   3   OPERATOR: NULL
REMARK   3
REMARK   3  DEVIATIONS FROM IDEAL VALUES.
REMARK   3                 RMSD          COUNT
REMARK   3   BOND      :  0.015           3893
REMARK   3   ANGLE     :  1.520           5308
REMARK   3   CHIRALITY :  0.112            566
REMARK   3   PLANARITY :  0.014            715
REMARK   3   DIHEDRAL  : 13.183            558
REMARK   3
REMARK   3  TLS DETAILS
REMARK   3   NUMBER OF TLS GROUPS  : 13
REMARK   3   TLS GROUP : 1
REMARK   3    SELECTION: CHAIN 'A' AND (RESID -2 THROUGH 30 )
REMARK   3    ORIGIN FOR THE GROUP (A):  -7.8072 -12.7695   8.8741
REMARK   3    T TENSOR
REMARK   3      T11:   0.2289 T22:   0.2244
REMARK   3      T33:   0.1966 T12:   0.0034
REMARK   3      T13:  -0.0179 T23:  -0.0283
REMARK   3    L TENSOR
REMARK   3      L11:   0.3926 L22:   0.0774
REMARK   3      L33:   0.1849 L12:   0.0473
REMARK   3      L13:  -0.0817 L23:   0.1000
REMARK   3    S TENSOR
REMARK   3      S11:   0.0663 S12:   0.1887 S13:  -0.2382
REMARK   3      S21:  -0.1007 S22:  -0.1081 S23:   0.1597
REMARK   3      S31:   0.1736 S32:   0.0766 S33:  -0.0126
REMARK   3   TLS GROUP : 2
REMARK   3    SELECTION: CHAIN 'A' AND (RESID 31 THROUGH 73 )
REMARK   3    ORIGIN FOR THE GROUP (A):  -1.1181  -4.9611  12.3977
REMARK   3    T TENSOR
REMARK   3      T11:   0.1626 T22:   0.2426
REMARK   3      T33:   0.1259 T12:   0.0086
REMARK   3      T13:  -0.0033 T23:  -0.0052
REMARK   3    L TENSOR
REMARK   3      L11:   0.4796 L22:   0.3458
REMARK   3      L33:   0.3763 L12:  -0.1499
REMARK   3      L13:   0.0573 L23:   0.2447
REMARK   3    S TENSOR
REMARK   3      S11:   0.1033 S12:   0.2078 S13:  -0.0536
REMARK   3      S21:  -0.0550 S22:  -0.0014 S23:  -0.0646
REMARK   3      S31:   0.0813 S32:   0.1712 S33:   0.0645
REMARK   3   TLS GROUP : 3
REMARK   3    SELECTION: CHAIN 'A' AND (RESID 74 THROUGH 87 )
REMARK   3    ORIGIN FOR THE GROUP (A):  -2.9753  12.5568   7.0056
REMARK   3    T TENSOR
REMARK   3      T11:   0.3024 T22:   0.5610
REMARK   3      T33:   0.3463 T12:   0.0283
REMARK   3      T13:   0.1135 T23:   0.2025
REMARK   3    L TENSOR
REMARK   3      L11:   0.0645 L22:   0.1898
REMARK   3      L33:   0.0806 L12:  -0.0464
REMARK   3      L13:   0.0089 L23:   0.1020
REMARK   3    S TENSOR
REMARK   3      S11:   0.0204 S12:   0.1528 S13:   0.2345
REMARK   3      S21:  -0.2423 S22:   0.1350 S23:   0.0484
REMARK   3      S31:  -0.0636 S32:  -0.0549 S33:   0.0976
REMARK   3   TLS GROUP : 4
REMARK   3    SELECTION: CHAIN 'A' AND (RESID 88 THROUGH 204 )
REMARK   3    ORIGIN FOR THE GROUP (A):  -8.5249   4.8986  21.9875
REMARK   3    T TENSOR
REMARK   3      T11:   0.1188 T22:   0.1505
REMARK   3      T33:   0.1328 T12:   0.0116
REMARK   3      T13:   0.0113 T23:   0.0279
REMARK   3    L TENSOR
REMARK   3      L11:   0.9236 L22:   0.2143
REMARK   3      L33:   0.6900 L12:  -0.2186
REMARK   3      L13:  -0.0904 L23:   0.1579
REMARK   3    S TENSOR
REMARK   3      S11:   0.0780 S12:   0.1901 S13:   0.1293
REMARK   3      S21:  -0.0187 S22:  -0.0260 S23:  -0.0118
REMARK   3      S31:  -0.0510 S32:  -0.0164 S33:   0.0610
REMARK   3   TLS GROUP : 5
REMARK   3    SELECTION: CHAIN 'A' AND (RESID 205 THROUGH 238 )
REMARK   3    ORIGIN FOR THE GROUP (A):   3.2898  -2.1335  24.5739
REMARK   3    T TENSOR
REMARK   3      T11:   0.1398 T22:   0.2102
REMARK   3      T33:   0.1413 T12:   0.0132
REMARK   3      T13:  -0.0093 T23:  -0.0001
REMARK   3    L TENSOR
REMARK   3      L11:   0.3375 L22:   0.3035
REMARK   3      L33:   0.4628 L12:   0.0012
REMARK   3      L13:   0.2021 L23:   0.3843
REMARK   3    S TENSOR
REMARK   3      S11:   0.0629 S12:   0.3349 S13:  -0.0010
REMARK   3      S21:   0.0360 S22:   0.0777 S23:  -0.0199
REMARK   3      S31:   0.1288 S32:   0.0663 S33:   0.0809
REMARK   3   TLS GROUP : 6
REMARK   3    SELECTION: CHAIN 'B' AND (RESID 1 THROUGH 21 )
REMARK   3    ORIGIN FOR THE GROUP (A):   6.7651  -5.7128  65.9077
REMARK   3    T TENSOR
REMARK   3      T11:   0.2566 T22:   0.3806
REMARK   3      T33:   0.1928 T12:   0.0294
REMARK   3      T13:  -0.0431 T23:   0.0376
REMARK   3    L TENSOR
REMARK   3      L11:   0.3068 L22:   0.0711
REMARK   3      L33:   0.1287 L12:  -0.0829
REMARK   3      L13:  -0.0411 L23:  -0.0782
REMARK   3    S TENSOR
REMARK   3      S11:  -0.0938 S12:  -0.6154 S13:  -0.1277
REMARK   3      S21:   0.2459 S22:   0.2942 S23:  -0.0530
REMARK   3      S31:   0.1230 S32:  -0.2893 S33:   0.0030
REMARK   3   TLS GROUP : 7
REMARK   3    SELECTION: CHAIN 'B' AND (RESID 22 THROUGH 35 )
REMARK   3    ORIGIN FOR THE GROUP (A):   8.4066 -13.7492  52.4593
REMARK   3    T TENSOR
REMARK   3      T11:   0.2036 T22:   0.1679
REMARK   3      T33:   0.3751 T12:  -0.0139
REMARK   3      T13:  -0.0539 T23:   0.0274
REMARK   3    L TENSOR
REMARK   3      L11:   0.0565 L22:   0.0379
REMARK   3      L33:   0.0879 L12:   0.0064
REMARK   3      L13:  -0.0322 L23:  -0.0048
REMARK   3    S TENSOR
REMARK   3      S11:   0.1107 S12:  -0.1974 S13:  -0.5358
REMARK   3      S21:   0.2420 S22:  -0.1183 S23:   0.0830
REMARK   3      S31:   0.1378 S32:  -0.1621 S33:  -0.0019
REMARK   3   TLS GROUP : 8
REMARK   3    SELECTION: CHAIN 'B' AND (RESID 36 THROUGH 54 )
REMARK   3    ORIGIN FOR THE GROUP (A):  -2.7588  -5.3294  55.6007
REMARK   3    T TENSOR
REMARK   3      T11:   0.1767 T22:   0.3032
REMARK   3      T33:   0.2012 T12:  -0.0404
REMARK   3      T13:  -0.0224 T23:   0.0631
REMARK   3    L TENSOR
REMARK   3      L11:   0.2212 L22:   0.1326
REMARK   3      L33:   0.2678 L12:   0.0040
REMARK   3      L13:   0.1406 L23:   0.0365
REMARK   3    S TENSOR
REMARK   3      S11:   0.0477 S12:  -0.2125 S13:  -0.1814
REMARK   3      S21:  -0.1441 S22:   0.1567 S23:   0.1790
REMARK   3      S31:   0.0687 S32:  -0.4789 S33:   0.0443
REMARK   3   TLS GROUP : 9
REMARK   3    SELECTION: CHAIN 'B' AND (RESID 55 THROUGH 87 )
REMARK   3    ORIGIN FOR THE GROUP (A):   0.5581   5.3440  61.7646
REMARK   3    T TENSOR
REMARK   3      T11:   0.2038 T22:   0.3627
REMARK   3      T33:   0.1907 T12:   0.0564
REMARK   3      T13:   0.0046 T23:  -0.0209
REMARK   3    L TENSOR
REMARK   3      L11:   0.6305 L22:   0.5813
REMARK   3      L33:   0.6980 L12:  -0.0678
REMARK   3      L13:   0.1422 L23:  -0.1561
REMARK   3    S TENSOR
REMARK   3      S11:  -0.0753 S12:  -0.3909 S13:   0.0678
REMARK   3      S21:   0.0619 S22:   0.3015 S23:   0.0489
REMARK   3      S31:  -0.0847 S32:  -0.2104 S33:   0.2438
REMARK   3   TLS GROUP : 10
REMARK   3    SELECTION: CHAIN 'B' AND (RESID 88 THROUGH 103 )
REMARK   3    ORIGIN FOR THE GROUP (A):  13.8392   4.0920  57.9051
REMARK   3    T TENSOR
REMARK   3      T11:   0.1780 T22:   0.2834
REMARK   3      T33:   0.1703 T12:   0.0000
REMARK   3      T13:  -0.0219 T23:  -0.0503
REMARK   3    L TENSOR
REMARK   3      L11:   0.0480 L22:   0.0308
REMARK   3      L33:  -0.0049 L12:   0.0154
REMARK   3      L13:   0.0073 L23:  -0.0158
REMARK   3    S TENSOR
REMARK   3      S11:   0.0533 S12:  -0.2576 S13:   0.0740
REMARK   3      S21:   0.0769 S22:   0.0000 S23:  -0.1763
REMARK   3      S31:  -0.0210 S32:   0.1647 S33:  -0.0004
REMARK   3   TLS GROUP : 11
REMARK   3    SELECTION: CHAIN 'B' AND (RESID 104 THROUGH 204 )
REMARK   3    ORIGIN FOR THE GROUP (A):   5.6742   6.3911  45.6865
REMARK   3    T TENSOR
REMARK   3      T11:   0.1273 T22:   0.1439
REMARK   3      T33:   0.1551 T12:  -0.0045
REMARK   3      T13:   0.0078 T23:  -0.0257
REMARK   3    L TENSOR
REMARK   3      L11:   0.6206 L22:   0.2673
REMARK   3      L33:   0.6993 L12:   0.0723
REMARK   3      L13:   0.3459 L23:  -0.0195
REMARK   3    S TENSOR
REMARK   3      S11:   0.0342 S12:  -0.0676 S13:   0.0841
REMARK   3      S21:   0.0149 S22:  -0.0030 S23:  -0.0212
REMARK   3      S31:  -0.0323 S32:  -0.0165 S33:   0.1609
REMARK   3   TLS GROUP : 12
REMARK   3    SELECTION: CHAIN 'B' AND (RESID 205 THROUGH 218 )
REMARK   3    ORIGIN FOR THE GROUP (A): -13.8852   5.5983  51.9339
REMARK   3    T TENSOR
REMARK   3      T11:   0.1590 T22:   0.3253
REMARK   3      T33:   0.1766 T12:  -0.0151
REMARK   3      T13:   0.0178 T23:  -0.0444
REMARK   3    L TENSOR
REMARK   3      L11:   0.0277 L22:   0.0393
REMARK   3      L33:   0.0935 L12:  -0.0244
REMARK   3      L13:   0.0057 L23:  -0.0645
REMARK   3    S TENSOR
REMARK   3      S11:   0.0752 S12:  -0.4562 S13:   0.1507
REMARK   3      S21:   0.0586 S22:  -0.0520 S23:   0.0141
REMARK   3      S31:  -0.0378 S32:  -0.0595 S33:   0.0012
REMARK   3   TLS GROUP : 13
REMARK   3    SELECTION: CHAIN 'B' AND (RESID 219 THROUGH 238 )
REMARK   3    ORIGIN FOR THE GROUP (A):   1.0155  -5.6769  41.3487
REMARK   3    T TENSOR
REMARK   3      T11:   0.1854 T22:   0.1479
REMARK   3      T33:   0.1773 T12:   0.0071
REMARK   3      T13:  -0.0411 T23:  -0.0297
REMARK   3    L TENSOR
REMARK   3      L11:   0.0618 L22:   0.1937
REMARK   3      L33:   0.2212 L12:  -0.0710
REMARK   3      L13:   0.0011 L23:  -0.1930
REMARK   3    S TENSOR
REMARK   3      S11:   0.1422 S12:   0.0108 S13:  -0.2752
REMARK   3      S21:  -0.0984 S22:  -0.0073 S23:   0.1447
REMARK   3      S31:   0.1793 S32:  -0.0282 S33:   0.0717
REMARK   3
REMARK   3  NCS DETAILS
REMARK   3   NUMBER OF NCS GROUPS : NULL
REMARK   3
REMARK   3  OTHER REFINEMENT REMARKS: NULL
REMARK   4
REMARK   4 8VB3 COMPLIES WITH FORMAT V. 3.30, 13-JUL-11
REMARK 100
REMARK 100 THIS ENTRY HAS BEEN PROCESSED BY RCSB ON 12-DEC-23.
REMARK 100 THE DEPOSITION ID IS D_1000279843.
REMARK 200
REMARK 200 EXPERIMENTAL DETAILS
REMARK 200  EXPERIMENT TYPE                : X-RAY DIFFRACTION
REMARK 200  DATE OF DATA COLLECTION        : 23-FEB-19
REMARK 200  TEMPERATURE           (KELVIN) : 100
REMARK 200  PH                             : 7
REMARK 200  NUMBER OF CRYSTALS USED        : 1
REMARK 200
REMARK 200  SYNCHROTRON              (Y/N) : Y
REMARK 200  RADIATION SOURCE               : DIAMOND
REMARK 200  BEAMLINE                       : I03
REMARK 200  X-RAY GENERATOR MODEL          : NULL
REMARK 200  MONOCHROMATIC OR LAUE    (M/L) : M
REMARK 200  WAVELENGTH OR RANGE        (A) : 0.976
REMARK 200  MONOCHROMATOR                  : NULL
REMARK 200  OPTICS                         : NULL
REMARK 200
REMARK 200  DETECTOR TYPE                  : PIXEL
REMARK 200  DETECTOR MANUFACTURER          : DECTRIS EIGER X 16M
REMARK 200  INTENSITY-INTEGRATION SOFTWARE : XDS
REMARK 200  DATA SCALING SOFTWARE          : XDS
REMARK 200
REMARK 200  NUMBER OF UNIQUE REFLECTIONS   : 86395
REMARK 200  RESOLUTION RANGE HIGH      (A) : 1.450
REMARK 200  RESOLUTION RANGE LOW       (A) : 39.630
REMARK 200  REJECTION CRITERIA  (SIGMA(I)) : NULL
REMARK 200
REMARK 200 OVERALL.
REMARK 200  COMPLETENESS FOR RANGE     (%) : 99.7
REMARK 200  DATA REDUNDANCY                : 6.500
REMARK 200  R MERGE                    (I) : 0.06690
REMARK 200  R SYM                      (I) : NULL
REMARK 200   FOR THE DATA SET  : 12.0100
REMARK 200
REMARK 200 IN THE HIGHEST RESOLUTION SHELL.
REMARK 200  HIGHEST RESOLUTION SHELL, RANGE HIGH (A) : 1.45
REMARK 200  HIGHEST RESOLUTION SHELL, RANGE LOW  (A) : 1.50
REMARK 200  COMPLETENESS FOR SHELL     (%) : 99.1
REMARK 200  DATA REDUNDANCY IN SHELL       : 6.30
REMARK 200  R MERGE FOR SHELL          (I) : 0.28750
REMARK 200  R SYM FOR SHELL            (I) : NULL
REMARK 200   FOR SHELL         : 4.430
REMARK 200
REMARK 200 DIFFRACTION PROTOCOL: SINGLE WAVELENGTH
REMARK 200 METHOD USED TO DETERMINE THE STRUCTURE: MOLECULAR REPLACEMENT
REMARK 200 SOFTWARE USED: MOLREP
REMARK 200 STARTING MODEL: NULL
REMARK 200
REMARK 200 REMARK: NULL
REMARK 280
REMARK 280 CRYSTAL
REMARK 280 SOLVENT CONTENT, VS   (%): 46.19
REMARK 280 MATTHEWS COEFFICIENT, VM (ANGSTROMS**3/DA): 2.29
REMARK 280
REMARK 280 CRYSTALLIZATION CONDITIONS: 20% W/V PEG3000, 0.1 M TRIS, PH 7, 0.2
REMARK 280  M CALCIUM ACETATE, VAPOR DIFFUSION, SITTING DROP, TEMPERATURE
REMARK 280  291.15K
REMARK 290
REMARK 290 CRYSTALLOGRAPHIC SYMMETRY
REMARK 290 SYMMETRY OPERATORS FOR SPACE GROUP: P 1 21 1
REMARK 290
REMARK 290      SYMOP   SYMMETRY
REMARK 290     NNNMMM   OPERATOR
REMARK 290       1555   X,Y,Z
REMARK 290       2555   -X,Y+1/2,-Z
REMARK 290
REMARK 290     WHERE NNN -> OPERATOR NUMBER
REMARK 290           MMM -> TRANSLATION VECTOR
REMARK 290
REMARK 290 CRYSTALLOGRAPHIC SYMMETRY TRANSFORMATIONS
REMARK 290 THE FOLLOWING TRANSFORMATIONS OPERATE ON THE ATOM/HETATM
REMARK 290 RECORDS IN THIS ENTRY TO PRODUCE CRYSTALLOGRAPHICALLY
REMARK 290 RELATED MOLECULES.
REMARK 290   SMTRY1   1  1.000000  0.000000  0.000000        0.00000
REMARK 290   SMTRY2   1  0.000000  1.000000  0.000000        0.00000
REMARK 290   SMTRY3   1  0.000000  0.000000  1.000000        0.00000
REMARK 290   SMTRY1   2 -1.000000  0.000000  0.000000        0.00000
REMARK 290   SMTRY2   2  0.000000  1.000000  0.000000       43.91750
REMARK 290   SMTRY3   2  0.000000  0.000000 -1.000000        0.00000
REMARK 290
REMARK 290 REMARK: NULL
REMARK 300
REMARK 300 BIOMOLECULE: 1
REMARK 300 SEE REMARK 350 FOR THE AUTHOR PROVIDED AND/OR PROGRAM
REMARK 300 GENERATED ASSEMBLY INFORMATION FOR THE STRUCTURE IN
REMARK 300 THIS ENTRY. THE REMARK MAY ALSO PROVIDE INFORMATION ON
REMARK 300 BURIED SURFACE AREA.
REMARK 350
REMARK 350 COORDINATES FOR A COMPLETE MULTIMER REPRESENTING THE KNOWN
REMARK 350 BIOLOGICALLY SIGNIFICANT OLIGOMERIZATION STATE OF THE
REMARK 350 MOLECULE CAN BE GENERATED BY APPLYING BIOMT TRANSFORMATIONS
REMARK 350 GIVEN BELOW.  BOTH NON-CRYSTALLOGRAPHIC AND
REMARK 350 CRYSTALLOGRAPHIC OPERATIONS ARE GIVEN.
REMARK 350
REMARK 350 BIOMOLECULE: 1
REMARK 350 AUTHOR DETERMINED BIOLOGICAL UNIT: DIMERIC
REMARK 350 SOFTWARE DETERMINED QUATERNARY STRUCTURE: DIMERIC
REMARK 350 SOFTWARE USED: PISA
REMARK 350 TOTAL BURIED SURFACE AREA: 3620 ANGSTROM**2
REMARK 350 SURFACE AREA OF THE COMPLEX: 19880 ANGSTROM**2
REMARK 350 CHANGE IN SOLVENT FREE ENERGY: -123.0 KCAL/MOL
REMARK 350 APPLY THE FOLLOWING TO CHAINS: A
REMARK 350   BIOMT1   1  1.000000  0.000000  0.000000        0.00000
REMARK 350   BIOMT2   1  0.000000  1.000000  0.000000        0.00000
REMARK 350   BIOMT3   1  0.000000  0.000000  1.000000        0.00000
REMARK 350 APPLY THE FOLLOWING TO CHAINS: B
REMARK 350   BIOMT1   2  1.000000  0.000000  0.000000      -28.76200
REMARK 350   BIOMT2   2  0.000000  1.000000  0.000000        0.00000
REMARK 350   BIOMT3   2  0.000000  0.000000  1.000000      -70.50231
REMARK 465
REMARK 465 MISSING RESIDUES
REMARK 465 THE FOLLOWING RESIDUES WERE NOT LOCATED IN THE
REMARK 465 EXPERIMENT. (M=MODEL NUMBER; RES=RESIDUE NAME; C=CHAIN
REMARK 465 IDENTIFIER; SSSEQ=SEQUENCE NUMBER; I=INSERTION CODE.)
REMARK 465
REMARK 465   M RES C SSSEQI
REMARK 465     MET A   -12
REMARK 465     ALA A   -11
REMARK 465     SER A   -10
REMARK 465     TRP A    -9
REMARK 465     SER A    -8
REMARK 465     HIS A    -7
REMARK 465     PRO A    -6
REMARK 465     GLN A    -5
REMARK 465     PHE A    -4
REMARK 465     GLU A    -3
REMARK 465     MET B   -12
REMARK 465     ALA B   -11
REMARK 465     SER B   -10
REMARK 465     TRP B    -9
REMARK 465     SER B    -8
REMARK 465     HIS B    -7
REMARK 465     PRO B    -6
REMARK 465     GLN B    -5
REMARK 465     PHE B    -4
REMARK 465     GLU B    -3
REMARK 465     LYS B    -2
REMARK 465     GLY B    -1
REMARK 465     ALA B     0
REMARK 500
REMARK 500 GEOMETRY AND STEREOCHEMISTRY
REMARK 500 SUBTOPIC: CLOSE CONTACTS IN SAME ASYMMETRIC UNIT
REMARK 500
REMARK 500 THE FOLLOWING ATOMS ARE IN CLOSE CONTACT.
REMARK 500
REMARK 500  ATM1  RES C  SSEQI   ATM2  RES C  SSEQI           DISTANCE
REMARK 500   OE1  GLU B   174     O    HOH B   401              2.17
REMARK 500   OD2  CSD A   119     NE2  HIS A   200              2.19
REMARK 500
REMARK 500 REMARK: NULL
REMARK 500
REMARK 500 GEOMETRY AND STEREOCHEMISTRY
REMARK 500 SUBTOPIC: COVALENT BOND LENGTHS
REMARK 500
REMARK 500 THE STEREOCHEMICAL PARAMETERS OF THE FOLLOWING RESIDUES
REMARK 500 HAVE VALUES WHICH DEVIATE FROM EXPECTED VALUES BY MORE
REMARK 500 THAN 6*RMSD (M=MODEL NUMBER; RES=RESIDUE NAME; C=CHAIN
REMARK 500 IDENTIFIER; SSEQ=SEQUENCE NUMBER; I=INSERTION CODE).
REMARK 500
REMARK 500 STANDARD TABLE:
REMARK 500 FORMAT: (10X,I3,1X,2(A3,1X,A1,I4,A1,1X,A4,3X),1X,F6.3)
REMARK 500
REMARK 500 EXPECTED VALUES PROTEIN: ENGH AND HUBER, 1999
REMARK 500 EXPECTED VALUES NUCLEIC ACID: CLOWNEY ET AL 1996
REMARK 500
REMARK 500  M RES CSSEQI ATM1   RES CSSEQI ATM2   DEVIATION
REMARK 500    CYS A 119   CB    CYS A 119   SG     -0.099
REMARK 500
REMARK 500 REMARK: NULL
REMARK 500
REMARK 500 GEOMETRY AND STEREOCHEMISTRY
REMARK 500 SUBTOPIC: TORSION ANGLES
REMARK 500
REMARK 500 TORSION ANGLES OUTSIDE THE EXPECTED RAMACHANDRAN REGIONS:
REMARK 500 (M=MODEL NUMBER; RES=RESIDUE NAME; C=CHAIN IDENTIFIER;
REMARK 500 SSEQ=SEQUENCE NUMBER; I=INSERTION CODE).
REMARK 500
REMARK 500 STANDARD TABLE:
REMARK 500 FORMAT:(10X,I3,1X,A3,1X,A1,I4,A1,4X,F7.2,3X,F7.2)
REMARK 500
REMARK 500 EXPECTED VALUES: GJ KLEYWEGT AND TA JONES (1996). PHI/PSI-
REMARK 500 CHOLOGY: RAMACHANDRAN REVISITED. STRUCTURE 4, 1395 - 1400
REMARK 500
REMARK 500  M RES CSSEQI        PSI       PHI
REMARK 500    CSD A 119     -126.77     58.51
REMARK 500    CYS A 119     -122.15     49.46
REMARK 500    HIS A 142       58.32     33.44
REMARK 500    VAL A 199     -153.20   -117.22
REMARK 500    CSD B 119     -126.36     61.22
REMARK 500    CYS B 119     -119.56     51.35
REMARK 500    HIS B 142       58.47     34.83
REMARK 500    VAL B 199     -151.49   -114.67
REMARK 500
REMARK 500 REMARK: NULL
REMARK 525
REMARK 525 SOLVENT
REMARK 525
REMARK 525 THE SOLVENT MOLECULES HAVE CHAIN IDENTIFIERS THAT
REMARK 525 INDICATE THE POLYMER CHAIN WITH WHICH THEY ARE MOST
REMARK 525 CLOSELY ASSOCIATED. THE REMARK LISTS ALL THE SOLVENT
REMARK 525 MOLECULES WHICH ARE MORE THAN 5A AWAY FROM THE
REMARK 525 NEAREST POLYMER CHAIN (M = MODEL NUMBER;
REMARK 525 RES=RESIDUE NAME; C=CHAIN IDENTIFIER; SSEQ=SEQUENCE
REMARK 525 NUMBER; I=INSERTION CODE):
REMARK 525
REMARK 525  M RES CSSEQI
REMARK 525    HOH A 561        DISTANCE =  6.06 ANGSTROMS
REMARK 620
REMARK 620 METAL COORDINATION
REMARK 620 (M=MODEL NUMBER; RES=RESIDUE NAME; C=CHAIN IDENTIFIER;
REMARK 620 SSEQ=SEQUENCE NUMBER; I=INSERTION CODE):
REMARK 620
REMARK 620 COORDINATION ANGLES FOR:  M RES CSSEQI METAL
REMARK 620                              NA A 305  NA
REMARK 620 N RES CSSEQI ATOM
REMARK 620 1 ARG A 103   O
REMARK 620 2 GLN A 105   O   100.1
REMARK 620 3 VAL A 108   O   115.1  89.8
REMARK 620 4 HOH A 516   O   108.8 150.1  71.4
REMARK 620 5 HOH A 524   O   101.2  88.4 143.4  93.3
REMARK 620 N                    1     2     3     4
REMARK 620
REMARK 620 COORDINATION ANGLES FOR:  M RES CSSEQI METAL
REMARK 620                              NA A 306  NA
REMARK 620 N RES CSSEQI ATOM
REMARK 620 1 SER A 131   O
REMARK 620 2 ASP A 208   O    20.7
REMARK 620 3 HOH A 409   O    78.0  60.8
REMARK 620 4 HOH A 424   O   100.7 119.7 170.9
REMARK 620 5 HOH A 432   O   174.5 161.6 101.9  78.4
REMARK 620 6 HOH A 503   O    99.2  88.6  93.7  95.4  86.3
REMARK 620 N                    1     2     3     4     5
REMARK 620
REMARK 620 COORDINATION ANGLES FOR:  M RES CSSEQI METAL
REMARK 620                              NA B 304  NA
REMARK 620 N RES CSSEQI ATOM
REMARK 620 1 ARG B 103   O
REMARK 620 2 GLN B 105   O   102.6
REMARK 620 3 VAL B 108   O   113.0  92.5
REMARK 620 4 HOH B 479   O   105.5 150.3  67.8
REMARK 620 5 HOH B 529   O    99.6  92.9 144.9  91.7
REMARK 620 N                    1     2     3     4
REMARK 620
REMARK 620 COORDINATION ANGLES FOR:  M RES CSSEQI METAL
REMARK 620                              NA B 303  NA
REMARK 620 N RES CSSEQI ATOM
REMARK 620 1 SER B 131   O
REMARK 620 2 ASP B 208   O    16.8
REMARK 620 3 HOH B 437   O   176.3 160.4
REMARK 620 4 HOH B 461   O   103.2 119.5  80.0
REMARK 620 5 HOH B 522   O    85.6  69.0  91.4 170.1
REMARK 620 6 HOH B 526   O    90.9  86.2  90.8  94.1  81.0
REMARK 620 N                    1     2     3     4     5
DBREF1 8VB3 A    1   238  UNP                  A0A2S5TB63_9GAMM
DBREF2 8VB3 A     A0A2S5TB63                          1         238
DBREF1 8VB3 B    1   238  UNP                  A0A2S5TB63_9GAMM
DBREF2 8VB3 B     A0A2S5TB63                          1         238
SEQADV 8VB3 MET A  -12  UNP  A0A2S5TB6           INITIATING METHIONINE
SEQADV 8VB3 ALA A  -11  UNP  A0A2S5TB6           EXPRESSION TAG
SEQADV 8VB3 SER A  -10  UNP  A0A2S5TB6           EXPRESSION TAG
SEQADV 8VB3 TRP A   -9  UNP  A0A2S5TB6           EXPRESSION TAG
SEQADV 8VB3 SER A   -8  UNP  A0A2S5TB6           EXPRESSION TAG
SEQADV 8VB3 HIS A   -7  UNP  A0A2S5TB6           EXPRESSION TAG
SEQADV 8VB3 PRO A   -6  UNP  A0A2S5TB6           EXPRESSION TAG
SEQADV 8VB3 GLN A   -5  UNP  A0A2S5TB6           EXPRESSION TAG
SEQADV 8VB3 PHE A   -4  UNP  A0A2S5TB6           EXPRESSION TAG
SEQADV 8VB3 GLU A   -3  UNP  A0A2S5TB6           EXPRESSION TAG
SEQADV 8VB3 LYS A   -2  UNP  A0A2S5TB6           EXPRESSION TAG
SEQADV 8VB3 GLY A   -1  UNP  A0A2S5TB6           EXPRESSION TAG
SEQADV 8VB3 ALA A    0  UNP  A0A2S5TB6           EXPRESSION TAG
SEQADV 8VB3 MET B  -12  UNP  A0A2S5TB6           INITIATING METHIONINE
SEQADV 8VB3 ALA B  -11  UNP  A0A2S5TB6           EXPRESSION TAG
SEQADV 8VB3 SER B  -10  UNP  A0A2S5TB6           EXPRESSION TAG
SEQADV 8VB3 TRP B   -9  UNP  A0A2S5TB6           EXPRESSION TAG
SEQADV 8VB3 SER B   -8  UNP  A0A2S5TB6           EXPRESSION TAG
SEQADV 8VB3 HIS B   -7  UNP  A0A2S5TB6           EXPRESSION TAG
SEQADV 8VB3 PRO B   -6  UNP  A0A2S5TB6           EXPRESSION TAG
SEQADV 8VB3 GLN B   -5  UNP  A0A2S5TB6           EXPRESSION TAG
SEQADV 8VB3 PHE B   -4  UNP  A0A2S5TB6           EXPRESSION TAG
SEQADV 8VB3 GLU B   -3  UNP  A0A2S5TB6           EXPRESSION TAG
SEQADV 8VB3 LYS B   -2  UNP  A0A2S5TB6           EXPRESSION TAG
SEQADV 8VB3 GLY B   -1  UNP  A0A2S5TB6           EXPRESSION TAG
SEQADV 8VB3 ALA B    0  UNP  A0A2S5TB6           EXPRESSION TAG
SEQRES   1 A  251  MET ALA SER TRP SER HIS PRO GLN PHE GLU LYS GLY ALA
SEQRES   2 A  251  MET HIS GLN GLN PRO ILE GLU THR THR GLU ASN GLY GLN
SEQRES   3 A  251  ARG HIS ILE HIS GLN PHE PHE LEU ASP GLU THR LEU GLN
SEQRES   4 A  251  GLY PRO ARG PRO GLY VAL LEU VAL PHE PRO GLU ALA PHE
SEQRES   5 A  251  GLY LEU GLY ASP HIS ALA LEU GLN ARG ALA ARG ARG LEU
SEQRES   6 A  251  ALA GLU LEU GLY TYR ALA ALA LEU ALA VAL ASP ILE HIS
SEQRES   7 A  251  GLY GLU GLY ARG GLU PHE GLN ASP LEU ALA GLN VAL ARG
SEQRES   8 A  251  PRO ALA ILE LEU ALA LEU PHE GLY ASP ARG ALA ALA TRP
SEQRES   9 A  251  ARG ALA ARG LEU GLN ALA ALA HIS GLU LEU LEU ARG ALA
SEQRES  10 A  251  GLN PRO GLN VAL ASP ALA ALA ARG THR ALA ALA ILE GLY
SEQRES  11 A  251  PHE CSD PHE GLY GLY ALA CYS SER LEU GLU LEU ALA ARG
SEQRES  12 A  251  SER GLY ALA PRO LEU SER ALA ILE VAL THR PHE HIS ALA
SEQRES  13 A  251  GLY LEU GLN PRO PRO LEU GLU ALA ASP ALA GLY LYS ILE
SEQRES  14 A  251  LYS ALA LYS VAL LEU VAL CYS HIS GLY ALA GLU ASP PRO
SEQRES  15 A  251  LEU MET LYS PRO GLU PRO LEU ALA ALA ILE LEU ALA GLU
SEQRES  16 A  251  LEU THR ARG ASP LYS VAL ASP TRP GLN LEU LEU SER HIS
SEQRES  17 A  251  GLY ASN VAL VAL HIS SER PHE THR ASN PRO ASP ALA ASP
SEQRES  18 A  251  ALA ARG GLY ALA PRO GLY PHE ALA TYR ASN ALA GLY ALA
SEQRES  19 A  251  ASP ARG ARG SER TRP ALA ALA MET GLN GLY LEU PHE ALA
SEQRES  20 A  251  GLU VAL PHE ALA
SEQRES   1 B  251  MET ALA SER TRP SER HIS PRO GLN PHE GLU LYS GLY ALA
SEQRES   2 B  251  MET HIS GLN GLN PRO ILE GLU THR THR GLU ASN GLY GLN
SEQRES   3 B  251  ARG HIS ILE HIS GLN PHE PHE LEU ASP GLU THR LEU GLN
SEQRES   4 B  251  GLY PRO ARG PRO GLY VAL LEU VAL PHE PRO GLU ALA PHE
SEQRES   5 B  251  GLY LEU GLY ASP HIS ALA LEU GLN ARG ALA ARG ARG LEU
SEQRES   6 B  251  ALA GLU LEU GLY TYR ALA ALA LEU ALA VAL ASP ILE HIS
SEQRES   7 B  251  GLY GLU GLY ARG GLU PHE GLN ASP LEU ALA GLN VAL ARG
SEQRES   8 B  251  PRO ALA ILE LEU ALA LEU PHE GLY ASP ARG ALA ALA TRP
SEQRES   9 B  251  ARG ALA ARG LEU GLN ALA ALA HIS GLU LEU LEU ARG ALA
SEQRES  10 B  251  GLN PRO GLN VAL ASP ALA ALA ARG THR ALA ALA ILE GLY
SEQRES  11 B  251  PHE CSD PHE GLY GLY ALA CYS SER LEU GLU LEU ALA ARG
SEQRES  12 B  251  SER GLY ALA PRO LEU SER ALA ILE VAL THR PHE HIS ALA
SEQRES  13 B  251  GLY LEU GLN PRO PRO LEU GLU ALA ASP ALA GLY LYS ILE
SEQRES  14 B  251  LYS ALA LYS VAL LEU VAL CYS HIS GLY ALA GLU ASP PRO
SEQRES  15 B  251  LEU MET LYS PRO GLU PRO LEU ALA ALA ILE LEU ALA GLU
SEQRES  16 B  251  LEU THR ARG ASP LYS VAL ASP TRP GLN LEU LEU SER HIS
SEQRES  17 B  251  GLY ASN VAL VAL HIS SER PHE THR ASN PRO ASP ALA ASP
SEQRES  18 B  251  ALA ARG GLY ALA PRO GLY PHE ALA TYR ASN ALA GLY ALA
SEQRES  19 B  251  ASP ARG ARG SER TRP ALA ALA MET GLN GLY LEU PHE ALA
SEQRES  20 B  251  GLU VAL PHE ALA
MODRES 8VB3 CSD A  119  CYS  MODIFIED RESIDUE
MODRES 8VB3 CSD B  119  CYS  MODIFIED RESIDUE
HET    CSD  A 119       8
HET    CSD  B 119       8
HET    MPD  A 301       8
HET    MPD  A 302       8
HET    MPD  A 303       8
HET     NA  A 304       1
HET     NA  A 305       1
HET     NA  A 306       1
HET    MPD  B 301       8
HET    MPD  B 302       8
HET     NA  B 303       1
HET     NA  B 304       1
HET    MPD  B 305       8
HET    MPD  B 306       8
HETNAM     CSD 3-SULFINOALANINE
HETNAM     MPD (4S)-2-METHYL-2,4-PENTANEDIOL
HETNAM      NA SODIUM ION
HETSYN     CSD S-CYSTEINESULFINIC ACID; S-SULFINOCYSTEINE
FORMUL   1  CSD    2(C3 H7 N O4 S)
FORMUL   3  MPD    7(C6 H14 O2)
FORMUL   6   NA    5(NA 1+)
FORMUL  15  HOH   *314(H2 O)
HELIX    1 AA1 GLY A   42  LEU A   55  1                                  14
HELIX    2 AA2 ASP A   73  GLY A   86  1                                  14
HELIX    3 AA3 ASP A   87  GLN A  105  1                                  19
HELIX    4 AA4 CSD A  119  SER A  131  1                                  13
HELIX    5 AA5 LEU A  149  ALA A  153  5                                   5
HELIX    6 AA6 LYS A  172  ASP A  186  1                                  15
HELIX    7 AA7 ASN A  204  ARG A  210  5                                   7
HELIX    8 AA8 ASN A  218  PHE A  237  1                                  20
HELIX    9 AA9 GLY B   42  LEU B   55  1                                  14
HELIX   10 AB1 ASP B   73  GLY B   86  1                                  14
HELIX   11 AB2 ASP B   87  ALA B  104  1                                  18
HELIX   12 AB3 CSD B  119  SER B  131  1                                  13
HELIX   13 AB4 LEU B  149  ALA B  153  5                                   5
HELIX   14 AB5 LYS B  172  ASP B  186  1                                  15
HELIX   15 AB6 ASN B  204  ARG B  210  5                                   7
HELIX   16 AB7 ASN B  218  PHE B  237  1                                  20
SHEET    1 AA116 HIS A   2  GLU A  10  0
SHEET    2 AA116 GLN A  13  LEU A  21 -1  O  LEU A  21   N  HIS A   2
SHEET    3 AA116 ALA A  58  ALA A  61 -1  O  ALA A  59   N  PHE A  20
SHEET    4 AA116 ARG A  29  PHE A  35  1  N  VAL A  34   O  LEU A  60
SHEET    5 AA116 VAL A 108  PHE A 118  1  O  ILE A 116   N  LEU A  33
SHEET    6 AA116 ALA A 137  PHE A 141  1  O  PHE A 141   N  GLY A 117
SHEET    7 AA116 LYS A 159  GLY A 165  1  O  CYS A 163   N  THR A 140
SHEET    8 AA116 TRP A 190  HIS A 195  1  O  LEU A 193   N  VAL A 162
SHEET    9 AA116 TRP B 190  HIS B 195 -1  O  SER B 194   N  LEU A 192
SHEET   10 AA116 LYS B 159  GLY B 165  1  N  HIS B 164   O  LEU B 193
SHEET   11 AA116 ALA B 137  PHE B 141  1  N  THR B 140   O  CYS B 163
SHEET   12 AA116 VAL B 108  PHE B 118  1  N  GLY B 117   O  PHE B 141
SHEET   13 AA116 ARG B  29  PHE B  35  1  N  LEU B  33   O  ILE B 116
SHEET   14 AA116 ALA B  58  ALA B  61  1  O  ALA B  58   N  PRO B  30
SHEET   15 AA116 GLN B  13  LEU B  21 -1  N  GLN B  18   O  ALA B  61
SHEET   16 AA116 HIS B   2  GLU B  10 -1  N  HIS B   2   O  LEU B  21
LINK         C   PHE A 118                 N  ACSD A 119     1555   1555  1.33
LINK         C  ACSD A 119                 N   PHE A 120     1555   1555  1.33
LINK         C   PHE B 118                 N  ACSD B 119     1555   1555  1.32
LINK         C  ACSD B 119                 N   PHE B 120     1555   1555  1.32
LINK         O   ARG A 103                NA    NA A 305     1555   1555  2.28
LINK         O   GLN A 105                NA    NA A 305     1555   1555  2.38
LINK         O   VAL A 108                NA    NA A 305     1555   1555  2.43
LINK         O   SER A 131                NA    NA A 306     1555   1555  2.20
LINK         O   ASP A 208                NA    NA A 306     1555   1655  2.52
LINK        NA    NA A 305                 O   HOH A 516     1555   1555  2.66
LINK        NA    NA A 305                 O   HOH A 524     1555   1555  2.31
LINK        NA    NA A 306                 O   HOH A 409     1555   1555  2.94
LINK        NA    NA A 306                 O   HOH A 424     1555   1555  2.41
LINK        NA    NA A 306                 O   HOH A 432     1555   1455  2.53
LINK        NA    NA A 306                 O   HOH A 503     1555   1555  2.20
LINK         O   ARG B 103                NA    NA B 304     1555   1555  2.34
LINK         O   GLN B 105                NA    NA B 304     1555   1555  2.44
LINK         O   VAL B 108                NA    NA B 304     1555   1555  2.37
LINK         O   SER B 131                NA    NA B 303     1555   1555  2.29
LINK         O   ASP B 208                NA    NA B 303     1555   1455  2.41
LINK        NA    NA B 303                 O   HOH B 437     1555   1655  2.46
LINK        NA    NA B 303                 O   HOH B 461     1555   1655  2.32
LINK        NA    NA B 303                 O   HOH B 522     1555   1555  2.52
LINK        NA    NA B 303                 O   HOH B 526     1555   1555  2.33
LINK        NA    NA B 304                 O   HOH B 479     1555   1555  2.74
LINK        NA    NA B 304                 O   HOH B 529     1555   1555  2.19
CRYST1   40.143   87.835   71.415  90.00  99.17  90.00 P 1 21 1      4
ORIGX1      1.000000  0.000000  0.000000        0.00000
ORIGX2      0.000000  1.000000  0.000000        0.00000
ORIGX3      0.000000  0.000000  1.000000        0.00000
SCALE1      0.024911  0.000000  0.004021        0.00000
SCALE2      0.000000  0.011385  0.000000        0.00000
SCALE3      0.000000  0.000000  0.014184        0.00000
TER    1879      ALA A 238
TER    3744      ALA B 238
MASTER      557    0   14   16   16    0    0    6 4033    2   99   40
END