longtext: 8zvo-pdb

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HEADER    SIGNALING PROTEIN                       11-JUN-24   8ZVO
TITLE     ATKAI2 APO STRUCTURE
COMPND    MOL_ID: 1;
COMPND   2 MOLECULE: PROBABLE ESTERASE KAI2;
COMPND   3 CHAIN: A;
COMPND   4 SYNONYM: PROTEIN DWARF-14-LIKE,PROTEIN D14-LIKE,PROTEIN HYPOSENSITIVE
COMPND   5 TO LIGHT,PROTEIN KARRIKIN INSENSITIVE 2;
COMPND   6 ENGINEERED: YES
SOURCE    MOL_ID: 1;
SOURCE   2 ORGANISM_SCIENTIFIC: ARABIDOPSIS THALIANA;
SOURCE   3 ORGANISM_COMMON: THALE CRESS;
SOURCE   4 ORGANISM_TAXID: 3702;
SOURCE   5 GENE: KAI2, D14L, HTL, AT4G37470, F6G17.120;
SOURCE   6 EXPRESSION_SYSTEM: ESCHERICHIA COLI B;
SOURCE   7 EXPRESSION_SYSTEM_TAXID: 37762
KEYWDS    KARRIKIN INSENSITIVE 2, SIGNALING PROTEIN
EXPDTA    X-RAY DIFFRACTION
AUTHOR    K.TAKEGAMIE,J.TAKEUCHI,A.NAKAMURA
REVDAT   1   19-FEB-25 8ZVO    0
JRNL        AUTH   R.KUSHIHARA,A.NAKAMURA,K.TAKEGAMIE,Y.SETO,H.DORA,T.OHNISHI,
JRNL        AUTH 2 Y.TODOROKI,J.TAKEUCHI
JRNL        TITL   STRUCTURAL REQUIREMENT OF KAI2 LIGANDS FOR ACTIVATION OF ITS
JRNL        TITL 2 SIGNAL TRANSDUCTION
JRNL        REF    PROC.NATL.ACAD.SCI.USA                     2025
JRNL        REFN                   ESSN 1091-6490
JRNL        DOI    10.1073/PNAS.2414779122
REMARK   2
REMARK   2 RESOLUTION.    1.49 ANGSTROMS.
REMARK   3
REMARK   3 REFINEMENT.
REMARK   3   PROGRAM     : PHENIX 1.20.1_4487
REMARK   3   AUTHORS     : PAUL ADAMS,PAVEL AFONINE,VINCENT CHEN,IAN
REMARK   3               : DAVIS,KRESHNA GOPAL,RALF GROSSE-KUNSTLEVE,
REMARK   3               : LI-WEI HUNG,ROBERT IMMORMINO,TOM IOERGER,
REMARK   3               : AIRLIE MCCOY,ERIK MCKEE,NIGEL MORIARTY,
REMARK   3               : REETAL PAI,RANDY READ,JANE RICHARDSON,
REMARK   3               : DAVID RICHARDSON,TOD ROMO,JIM SACCHETTINI,
REMARK   3               : NICHOLAS SAUTER,JACOB SMITH,LAURENT
REMARK   3               : STORONI,TOM TERWILLIGER,PETER ZWART
REMARK   3
REMARK   3    REFINEMENT TARGET : GEOSTD + MONOMER LIBRARY + CDL V1.2
REMARK   3
REMARK   3  DATA USED IN REFINEMENT.
REMARK   3   RESOLUTION RANGE HIGH (ANGSTROMS) : 1.49
REMARK   3   RESOLUTION RANGE LOW  (ANGSTROMS) : 47.54
REMARK   3   MIN(FOBS/SIGMA_FOBS)              : 1.380
REMARK   3   COMPLETENESS FOR RANGE        (%) : 97.7
REMARK   3   NUMBER OF REFLECTIONS             : 42770
REMARK   3
REMARK   3  FIT TO DATA USED IN REFINEMENT.
REMARK   3   R VALUE     (WORKING + TEST SET) : 0.148
REMARK   3   R VALUE            (WORKING SET) : 0.147
REMARK   3   FREE R VALUE                     : 0.172
REMARK   3   FREE R VALUE TEST SET SIZE   (%) : 4.690
REMARK   3   FREE R VALUE TEST SET COUNT      : 2005
REMARK   3
REMARK   3  FIT TO DATA USED IN REFINEMENT (IN BINS).
REMARK   3   BIN  RESOLUTION RANGE  COMPL.    NWORK NFREE   RWORK  RFREE
REMARK   3     1 47.5400 -  3.5800    1.00     3063   148  0.1364 0.1428
REMARK   3     2  3.5800 -  2.8400    1.00     3004   144  0.1345 0.1586
REMARK   3     3  2.8400 -  2.4800    1.00     2979   147  0.1455 0.1822
REMARK   3     4  2.4800 -  2.2600    0.99     2974   148  0.1426 0.1856
REMARK   3     5  2.2600 -  2.0900    0.99     2936   144  0.1420 0.1556
REMARK   3     6  2.0900 -  1.9700    0.99     2954   149  0.1435 0.1694
REMARK   3     7  1.9700 -  1.8700    0.99     2928   145  0.1389 0.1709
REMARK   3     8  1.8700 -  1.7900    0.98     2928   144  0.1449 0.1698
REMARK   3     9  1.7900 -  1.7200    0.98     2919   141  0.1572 0.2054
REMARK   3    10  1.7200 -  1.6600    0.98     2910   142  0.1807 0.2197
REMARK   3    11  1.6600 -  1.6100    0.98     2899   154  0.1676 0.2039
REMARK   3    12  1.6100 -  1.5600    0.97     2876   127  0.1649 0.1857
REMARK   3    13  1.5600 -  1.5200    0.97     2911   150  0.1762 0.2143
REMARK   3    14  1.5200 -  1.4900    0.85     2484   122  0.2310 0.2610
REMARK   3
REMARK   3  BULK SOLVENT MODELLING.
REMARK   3   METHOD USED        : FLAT BULK SOLVENT MODEL
REMARK   3   SOLVENT RADIUS     : 1.10
REMARK   3   SHRINKAGE RADIUS   : 0.90
REMARK   3   K_SOL              : NULL
REMARK   3   B_SOL              : NULL
REMARK   3
REMARK   3  ERROR ESTIMATES.
REMARK   3   COORDINATE ERROR (MAXIMUM-LIKELIHOOD BASED)     : 0.125
REMARK   3   PHASE ERROR (DEGREES, MAXIMUM-LIKELIHOOD BASED) : 16.472
REMARK   3
REMARK   3  B VALUES.
REMARK   3   FROM WILSON PLOT           (A**2) : 12.76
REMARK   3   MEAN B VALUE      (OVERALL, A**2) : 17.93
REMARK   3   OVERALL ANISOTROPIC B VALUE.
REMARK   3    B11 (A**2) : NULL
REMARK   3    B22 (A**2) : NULL
REMARK   3    B33 (A**2) : NULL
REMARK   3    B12 (A**2) : NULL
REMARK   3    B13 (A**2) : NULL
REMARK   3    B23 (A**2) : NULL
REMARK   3
REMARK   3  TWINNING INFORMATION.
REMARK   3   FRACTION: NULL
REMARK   3   OPERATOR: NULL
REMARK   3
REMARK   3  DEVIATIONS FROM IDEAL VALUES.
REMARK   3                 RMSD          COUNT
REMARK   3   BOND      :  0.007           2316
REMARK   3   ANGLE     :  0.913           3158
REMARK   3   CHIRALITY :  0.088            353
REMARK   3   PLANARITY :  0.006            414
REMARK   3   DIHEDRAL  : 14.158            847
REMARK   3
REMARK   3  TLS DETAILS
REMARK   3   NUMBER OF TLS GROUPS  : NULL
REMARK   3
REMARK   3  NCS DETAILS
REMARK   3   NUMBER OF NCS GROUPS : NULL
REMARK   3
REMARK   3  OTHER REFINEMENT REMARKS: NULL
REMARK   4
REMARK   4 8ZVO COMPLIES WITH FORMAT V. 3.30, 13-JUL-11
REMARK 100
REMARK 100 THIS ENTRY HAS BEEN PROCESSED BY PDBJ ON 12-JUN-24.
REMARK 100 THE DEPOSITION ID IS D_1300048601.
REMARK 200
REMARK 200 EXPERIMENTAL DETAILS
REMARK 200  EXPERIMENT TYPE                : X-RAY DIFFRACTION
REMARK 200  DATE OF DATA COLLECTION        : 05-OCT-22
REMARK 200  TEMPERATURE           (KELVIN) : 100
REMARK 200  PH                             : 7.0-9.0
REMARK 200  NUMBER OF CRYSTALS USED        : 1
REMARK 200
REMARK 200  SYNCHROTRON              (Y/N) : Y
REMARK 200  RADIATION SOURCE               : AICHISR
REMARK 200  BEAMLINE                       : BL2S1
REMARK 200  X-RAY GENERATOR MODEL          : NULL
REMARK 200  MONOCHROMATIC OR LAUE    (M/L) : M
REMARK 200  WAVELENGTH OR RANGE        (A) : 1.12
REMARK 200  MONOCHROMATOR                  : NULL
REMARK 200  OPTICS                         : NULL
REMARK 200
REMARK 200  DETECTOR TYPE                  : CCD
REMARK 200  DETECTOR MANUFACTURER          : ADSC QUANTUM 315R
REMARK 200  INTENSITY-INTEGRATION SOFTWARE : XDS
REMARK 200  DATA SCALING SOFTWARE          : XSCALE
REMARK 200
REMARK 200  NUMBER OF UNIQUE REFLECTIONS   : 42773
REMARK 200  RESOLUTION RANGE HIGH      (A) : 1.490
REMARK 200  RESOLUTION RANGE LOW       (A) : 47.540
REMARK 200  REJECTION CRITERIA  (SIGMA(I)) : NULL
REMARK 200
REMARK 200 OVERALL.
REMARK 200  COMPLETENESS FOR RANGE     (%) : 96.7
REMARK 200  DATA REDUNDANCY                : 3.800
REMARK 200  R MERGE                    (I) : 0.04500
REMARK 200  R SYM                      (I) : NULL
REMARK 200   FOR THE DATA SET  : 18.9500
REMARK 200
REMARK 200 IN THE HIGHEST RESOLUTION SHELL.
REMARK 200  HIGHEST RESOLUTION SHELL, RANGE HIGH (A) : 1.49
REMARK 200  HIGHEST RESOLUTION SHELL, RANGE LOW  (A) : 1.58
REMARK 200  COMPLETENESS FOR SHELL     (%) : NULL
REMARK 200  DATA REDUNDANCY IN SHELL       : NULL
REMARK 200  R MERGE FOR SHELL          (I) : 0.31300
REMARK 200  R SYM FOR SHELL            (I) : NULL
REMARK 200   FOR SHELL         : 4.450
REMARK 200
REMARK 200 DIFFRACTION PROTOCOL: SINGLE WAVELENGTH
REMARK 200 METHOD USED TO DETERMINE THE STRUCTURE: MOLECULAR REPLACEMENT
REMARK 200 SOFTWARE USED: PHASER
REMARK 200 STARTING MODEL: 4JYM
REMARK 200
REMARK 200 REMARK: NULL
REMARK 280
REMARK 280 CRYSTAL
REMARK 280 SOLVENT CONTENT, VS   (%): 41.34
REMARK 280 MATTHEWS COEFFICIENT, VM (ANGSTROMS**3/DA): 2.10
REMARK 280
REMARK 280 CRYSTALLIZATION CONDITIONS: 0.1 M TRIS-HCL (PH 7.0 TO 9.0) WITH
REMARK 280  1.25 TO 2.0 M AMMONIUM SULFATE AND 12% (V/V) GLYCEROL, PH 7.5,
REMARK 280  VAPOR DIFFUSION, SITTING DROP, TEMPERATURE 293K
REMARK 290
REMARK 290 CRYSTALLOGRAPHIC SYMMETRY
REMARK 290 SYMMETRY OPERATORS FOR SPACE GROUP: P 1 21 1
REMARK 290
REMARK 290      SYMOP   SYMMETRY
REMARK 290     NNNMMM   OPERATOR
REMARK 290       1555   X,Y,Z
REMARK 290       2555   -X,Y+1/2,-Z
REMARK 290
REMARK 290     WHERE NNN -> OPERATOR NUMBER
REMARK 290           MMM -> TRANSLATION VECTOR
REMARK 290
REMARK 290 CRYSTALLOGRAPHIC SYMMETRY TRANSFORMATIONS
REMARK 290 THE FOLLOWING TRANSFORMATIONS OPERATE ON THE ATOM/HETATM
REMARK 290 RECORDS IN THIS ENTRY TO PRODUCE CRYSTALLOGRAPHICALLY
REMARK 290 RELATED MOLECULES.
REMARK 290   SMTRY1   1  1.000000  0.000000  0.000000        0.00000
REMARK 290   SMTRY2   1  0.000000  1.000000  0.000000        0.00000
REMARK 290   SMTRY3   1  0.000000  0.000000  1.000000        0.00000
REMARK 290   SMTRY1   2 -1.000000  0.000000  0.000000        0.00000
REMARK 290   SMTRY2   2  0.000000  1.000000  0.000000       27.89500
REMARK 290   SMTRY3   2  0.000000  0.000000 -1.000000        0.00000
REMARK 290
REMARK 290 REMARK: NULL
REMARK 300
REMARK 300 BIOMOLECULE: 1
REMARK 300 SEE REMARK 350 FOR THE AUTHOR PROVIDED AND/OR PROGRAM
REMARK 300 GENERATED ASSEMBLY INFORMATION FOR THE STRUCTURE IN
REMARK 300 THIS ENTRY. THE REMARK MAY ALSO PROVIDE INFORMATION ON
REMARK 300 BURIED SURFACE AREA.
REMARK 350
REMARK 350 COORDINATES FOR A COMPLETE MULTIMER REPRESENTING THE KNOWN
REMARK 350 BIOLOGICALLY SIGNIFICANT OLIGOMERIZATION STATE OF THE
REMARK 350 MOLECULE CAN BE GENERATED BY APPLYING BIOMT TRANSFORMATIONS
REMARK 350 GIVEN BELOW.  BOTH NON-CRYSTALLOGRAPHIC AND
REMARK 350 CRYSTALLOGRAPHIC OPERATIONS ARE GIVEN.
REMARK 350
REMARK 350 BIOMOLECULE: 1
REMARK 350 AUTHOR DETERMINED BIOLOGICAL UNIT: MONOMERIC
REMARK 350 SOFTWARE DETERMINED QUATERNARY STRUCTURE: MONOMERIC
REMARK 350 SOFTWARE USED: PISA
REMARK 350 TOTAL BURIED SURFACE AREA: 1890 ANGSTROM**2
REMARK 350 SURFACE AREA OF THE COMPLEX: 11050 ANGSTROM**2
REMARK 350 CHANGE IN SOLVENT FREE ENERGY: -16.0 KCAL/MOL
REMARK 350 APPLY THE FOLLOWING TO CHAINS: A
REMARK 350   BIOMT1   1  1.000000  0.000000  0.000000        0.00000
REMARK 350   BIOMT2   1  0.000000  1.000000  0.000000        0.00000
REMARK 350   BIOMT3   1  0.000000  0.000000  1.000000        0.00000
REMARK 465
REMARK 465 MISSING RESIDUES
REMARK 465 THE FOLLOWING RESIDUES WERE NOT LOCATED IN THE
REMARK 465 EXPERIMENT. (M=MODEL NUMBER; RES=RESIDUE NAME; C=CHAIN
REMARK 465 IDENTIFIER; SSSEQ=SEQUENCE NUMBER; I=INSERTION CODE.)
REMARK 465
REMARK 465   M RES C SSSEQI
REMARK 465     ALA A   269
REMARK 465     MET A   270
REMARK 465     GLU A   271
REMARK 465     ASN A   272
REMARK 465     LEU A   273
REMARK 465     TYR A   274
REMARK 465     PHE A   275
REMARK 465     GLN A   276
REMARK 500
REMARK 500 GEOMETRY AND STEREOCHEMISTRY
REMARK 500 SUBTOPIC: CLOSE CONTACTS IN SAME ASYMMETRIC UNIT
REMARK 500
REMARK 500 THE FOLLOWING ATOMS ARE IN CLOSE CONTACT.
REMARK 500
REMARK 500  ATM1  RES C  SSEQI   ATM2  RES C  SSEQI           DISTANCE
REMARK 500   OE1  GLU A     6     O    HOH A   401              2.00
REMARK 500   O    HOH A   444     O    HOH A   619              2.07
REMARK 500   NH2  ARG A   176     O    HOH A   402              2.12
REMARK 500   O    HOH A   528     O    HOH A   686              2.13
REMARK 500   O    HOH A   606     O    HOH A   744              2.14
REMARK 500   O    HOH A   652     O    HOH A   692              2.14
REMARK 500   O    HOH A   697     O    HOH A   723              2.16
REMARK 500   O    HOH A   497     O    HOH A   658              2.17
REMARK 500   OE2  GLU A     6     O    HOH A   403              2.17
REMARK 500   O    HOH A   517     O    HOH A   728              2.19
REMARK 500
REMARK 500 REMARK: NULL
REMARK 500
REMARK 500 GEOMETRY AND STEREOCHEMISTRY
REMARK 500 SUBTOPIC: CLOSE CONTACTS
REMARK 500
REMARK 500 THE FOLLOWING ATOMS THAT ARE RELATED BY CRYSTALLOGRAPHIC
REMARK 500 SYMMETRY ARE IN CLOSE CONTACT.  AN ATOM LOCATED WITHIN 0.15
REMARK 500 ANGSTROMS OF A SYMMETRY RELATED ATOM IS ASSUMED TO BE ON A
REMARK 500 SPECIAL POSITION AND IS, THEREFORE, LISTED IN REMARK 375
REMARK 500 INSTEAD OF REMARK 500.  ATOMS WITH NON-BLANK ALTERNATE
REMARK 500 LOCATION INDICATORS ARE NOT INCLUDED IN THE CALCULATIONS.
REMARK 500
REMARK 500 DISTANCE CUTOFF:
REMARK 500 2.2 ANGSTROMS FOR CONTACTS NOT INVOLVING HYDROGEN ATOMS
REMARK 500 1.6 ANGSTROMS FOR CONTACTS INVOLVING HYDROGEN ATOMS
REMARK 500
REMARK 500  ATM1  RES C  SSEQI   ATM2  RES C  SSEQI  SSYMOP   DISTANCE
REMARK 500   O    HOH A   406     O    HOH A   470     2544     2.03
REMARK 500   O    HOH A   685     O    HOH A   692     2555     2.16
REMARK 500
REMARK 500 REMARK: NULL
REMARK 500
REMARK 500 GEOMETRY AND STEREOCHEMISTRY
REMARK 500 SUBTOPIC: TORSION ANGLES
REMARK 500
REMARK 500 TORSION ANGLES OUTSIDE THE EXPECTED RAMACHANDRAN REGIONS:
REMARK 500 (M=MODEL NUMBER; RES=RESIDUE NAME; C=CHAIN IDENTIFIER;
REMARK 500 SSEQ=SEQUENCE NUMBER; I=INSERTION CODE).
REMARK 500
REMARK 500 STANDARD TABLE:
REMARK 500 FORMAT:(10X,I3,1X,A3,1X,A1,I4,A1,4X,F7.2,3X,F7.2)
REMARK 500
REMARK 500 EXPECTED VALUES: GJ KLEYWEGT AND TA JONES (1996). PHI/PSI-
REMARK 500 CHOLOGY: RAMACHANDRAN REVISITED. STRUCTURE 4, 1395 - 1400
REMARK 500
REMARK 500  M RES CSSEQI        PSI       PHI
REMARK 500    THR A  28     -164.12   -119.92
REMARK 500    SER A  95     -125.82     59.29
REMARK 500    ARG A 123      123.00   -171.15
REMARK 500    LEU A 247       56.40   -119.75
REMARK 500
REMARK 500 REMARK: NULL
REMARK 525
REMARK 525 SOLVENT
REMARK 525
REMARK 525 THE SOLVENT MOLECULES HAVE CHAIN IDENTIFIERS THAT
REMARK 525 INDICATE THE POLYMER CHAIN WITH WHICH THEY ARE MOST
REMARK 525 CLOSELY ASSOCIATED. THE REMARK LISTS ALL THE SOLVENT
REMARK 525 MOLECULES WHICH ARE MORE THAN 5A AWAY FROM THE
REMARK 525 NEAREST POLYMER CHAIN (M = MODEL NUMBER;
REMARK 525 RES=RESIDUE NAME; C=CHAIN IDENTIFIER; SSEQ=SEQUENCE
REMARK 525 NUMBER; I=INSERTION CODE):
REMARK 525
REMARK 525  M RES CSSEQI
REMARK 525    HOH A 762        DISTANCE =  5.86 ANGSTROMS
REMARK 525    HOH A 763        DISTANCE =  7.02 ANGSTROMS
REMARK 900
REMARK 900 RELATED ENTRIES
REMARK 900 RELATED ID: 8ZVN   RELATED DB: PDB
DBREF  8ZVO A    1   270  UNP    Q9SZU7   KAI2_ARATH       1    270
SEQADV 8ZVO GLU A  271  UNP  Q9SZU7              EXPRESSION TAG
SEQADV 8ZVO ASN A  272  UNP  Q9SZU7              EXPRESSION TAG
SEQADV 8ZVO LEU A  273  UNP  Q9SZU7              EXPRESSION TAG
SEQADV 8ZVO TYR A  274  UNP  Q9SZU7              EXPRESSION TAG
SEQADV 8ZVO PHE A  275  UNP  Q9SZU7              EXPRESSION TAG
SEQADV 8ZVO GLN A  276  UNP  Q9SZU7              EXPRESSION TAG
SEQRES   1 A  276  MET GLY VAL VAL GLU GLU ALA HIS ASN VAL LYS VAL ILE
SEQRES   2 A  276  GLY SER GLY GLU ALA THR ILE VAL LEU GLY HIS GLY PHE
SEQRES   3 A  276  GLY THR ASP GLN SER VAL TRP LYS HIS LEU VAL PRO HIS
SEQRES   4 A  276  LEU VAL ASP ASP TYR ARG VAL VAL LEU TYR ASP ASN MET
SEQRES   5 A  276  GLY ALA GLY THR THR ASN PRO ASP TYR PHE ASP PHE ASP
SEQRES   6 A  276  ARG TYR SER ASN LEU GLU GLY TYR SER PHE ASP LEU ILE
SEQRES   7 A  276  ALA ILE LEU GLU ASP LEU LYS ILE GLU SER CYS ILE PHE
SEQRES   8 A  276  VAL GLY HIS SER VAL SER ALA MET ILE GLY VAL LEU ALA
SEQRES   9 A  276  SER LEU ASN ARG PRO ASP LEU PHE SER LYS ILE VAL MET
SEQRES  10 A  276  ILE SER ALA SER PRO ARG TYR VAL ASN ASP VAL ASP TYR
SEQRES  11 A  276  GLN GLY GLY PHE GLU GLN GLU ASP LEU ASN GLN LEU PHE
SEQRES  12 A  276  GLU ALA ILE ARG SER ASN TYR LYS ALA TRP CYS LEU GLY
SEQRES  13 A  276  PHE ALA PRO LEU ALA VAL GLY GLY ASP MET ASP SER ILE
SEQRES  14 A  276  ALA VAL GLN GLU PHE SER ARG THR LEU PHE ASN MET ARG
SEQRES  15 A  276  PRO ASP ILE ALA LEU SER VAL GLY GLN THR ILE PHE GLN
SEQRES  16 A  276  SER ASP MET ARG GLN ILE LEU PRO PHE VAL THR VAL PRO
SEQRES  17 A  276  CYS HIS ILE LEU GLN SER VAL LYS ASP LEU ALA VAL PRO
SEQRES  18 A  276  VAL VAL VAL SER GLU TYR LEU HIS ALA ASN LEU GLY CYS
SEQRES  19 A  276  GLU SER VAL VAL GLU VAL ILE PRO SER ASP GLY HIS LEU
SEQRES  20 A  276  PRO GLN LEU SER SER PRO ASP SER VAL ILE PRO VAL ILE
SEQRES  21 A  276  LEU ARG HIS ILE ARG ASN ASP ILE ALA MET GLU ASN LEU
SEQRES  22 A  276  TYR PHE GLN
HET    GOL  A 301      12
HET    GOL  A 302       6
HET    GOL  A 303       6
HET    GOL  A 304       6
HET    GOL  A 305       6
HET    GOL  A 306       6
HET    GOL  A 307      12
HET    SO4  A 308       5
HETNAM     GOL GLYCEROL
HETNAM     SO4 SULFATE ION
HETSYN     GOL GLYCERIN; PROPANE-1,2,3-TRIOL
FORMUL   2  GOL    7(C3 H8 O3)
FORMUL   9  SO4    O4 S 2-
FORMUL  10  HOH   *363(H2 O)
HELIX    1 AA1 GLY A    2  HIS A    8  1                                   7
HELIX    2 AA2 ASP A   29  LYS A   34  5                                   6
HELIX    3 AA3 LEU A   36  LEU A   40  5                                   5
HELIX    4 AA4 ASN A   58  PHE A   62  5                                   5
HELIX    5 AA5 ASP A   65  SER A   68  5                                   4
HELIX    6 AA6 ASN A   69  LEU A   84  1                                  16
HELIX    7 AA7 SER A   95  ARG A  108  1                                  14
HELIX    8 AA8 GLU A  135  ASN A  149  1                                  15
HELIX    9 AA9 ASN A  149  GLY A  163  1                                  15
HELIX   10 AB1 SER A  168  MET A  181  1                                  14
HELIX   11 AB2 ARG A  182  GLN A  195  1                                  14
HELIX   12 AB3 MET A  198  VAL A  205  5                                   8
HELIX   13 AB4 PRO A  221  LEU A  232  1                                  12
HELIX   14 AB5 LEU A  247  SER A  252  1                                   6
HELIX   15 AB6 SER A  252  ASN A  266  1                                  15
SHEET    1 AA1 7 LYS A  11  ILE A  13  0
SHEET    2 AA1 7 ARG A  45  LEU A  48 -1  O  VAL A  46   N  ILE A  13
SHEET    3 AA1 7 THR A  19  GLY A  23  1  N  ILE A  20   O  VAL A  47
SHEET    4 AA1 7 CYS A  89  HIS A  94  1  O  HIS A  94   N  GLY A  23
SHEET    5 AA1 7 PHE A 112  ILE A 118  1  O  VAL A 116   N  PHE A  91
SHEET    6 AA1 7 CYS A 209  LYS A 216  1  O  HIS A 210   N  MET A 117
SHEET    7 AA1 7 SER A 236  ASP A 244  1  O  VAL A 237   N  ILE A 211
CRYST1   50.700   55.790   52.870  90.00 115.94  90.00 P 1 21 1      2
ORIGX1      1.000000  0.000000  0.000000        0.00000
ORIGX2      0.000000  1.000000  0.000000        0.00000
ORIGX3      0.000000  0.000000  1.000000        0.00000
SCALE1      0.019724  0.000000  0.009594        0.00000
SCALE2      0.000000  0.017924  0.000000        0.00000
SCALE3      0.000000  0.000000  0.021033        0.00000
TER    2208      ILE A 268
MASTER      290    0    8   15    7    0    0    6 2492    1   59   22
END