longtext: 9HH0-pdb

content
HEADER    HYDROLASE                               20-NOV-24   9HH0
TITLE     CRYSTAL STRUCTURE OF RECOMBINANT SOMAN-AGED SWINE
TITLE    2 BUTYRYLCHOLINESTERASE
COMPND    MOL_ID: 1;
COMPND   2 MOLECULE: CARBOXYLIC ESTER HYDROLASE;
COMPND   3 CHAIN: A, B, C, D;
COMPND   4 EC: 3.1.1.-;
COMPND   5 ENGINEERED: YES;
COMPND   6 OTHER_DETAILS: MATURE PROTEIN FORM (DEVOID OF SIGNAL PEPTIDE) AND
COMPND   7 DEVOID OF C-TERMINAL PART (STOP CODON AT RESIDUE POSITION 530)
SOURCE    MOL_ID: 1;
SOURCE   2 ORGANISM_SCIENTIFIC: SUS SCROFA;
SOURCE   3 ORGANISM_COMMON: PIG;
SOURCE   4 ORGANISM_TAXID: 9823;
SOURCE   5 GENE: BCHE;
SOURCE   6 EXPRESSION_SYSTEM: DROSOPHILA MELANOGASTER;
SOURCE   7 EXPRESSION_SYSTEM_TAXID: 7227
KEYWDS    BUTYRYLCHOLINESTERASE, SWINE, RECOMBINANT, ORGANOPHOSPHORUS COMPOUND,
KEYWDS   2 AGING., HYDROLASE
EXPDTA    X-RAY DIFFRACTION
AUTHOR    X.BRAZZOLOTTO,F.NACHON
REVDAT   1   03-DEC-25 9HH0    0
JRNL        AUTH   X.BRAZZOLOTTO,F.NACHON
JRNL        TITL   CRYSTAL STRUCTURE OF RECOMBINANT SOMAN-AGED SWINE
JRNL        TITL 2 BUTYRYLCHOLINESTERASE
JRNL        REF    TO BE PUBLISHED
JRNL        REFN
REMARK   2
REMARK   2 RESOLUTION.    2.66 ANGSTROMS.
REMARK   3
REMARK   3 REFINEMENT.
REMARK   3   PROGRAM     : PHENIX 1.21.2_5419
REMARK   3   AUTHORS     : PAUL ADAMS,PAVEL AFONINE,VINCENT CHEN,IAN
REMARK   3               : DAVIS,KRESHNA GOPAL,RALF GROSSE-KUNSTLEVE,
REMARK   3               : LI-WEI HUNG,ROBERT IMMORMINO,TOM IOERGER,
REMARK   3               : AIRLIE MCCOY,ERIK MCKEE,NIGEL MORIARTY,
REMARK   3               : REETAL PAI,RANDY READ,JANE RICHARDSON,
REMARK   3               : DAVID RICHARDSON,TOD ROMO,JIM SACCHETTINI,
REMARK   3               : NICHOLAS SAUTER,JACOB SMITH,LAURENT
REMARK   3               : STORONI,TOM TERWILLIGER,PETER ZWART
REMARK   3
REMARK   3    REFINEMENT TARGET : GEOSTD + MONOMER LIBRARY + CDL V1.2
REMARK   3
REMARK   3  DATA USED IN REFINEMENT.
REMARK   3   RESOLUTION RANGE HIGH (ANGSTROMS) : 2.66
REMARK   3   RESOLUTION RANGE LOW  (ANGSTROMS) : 124.69
REMARK   3   MIN(FOBS/SIGMA_FOBS)              : 1.340
REMARK   3   COMPLETENESS FOR RANGE        (%) : 99.8
REMARK   3   NUMBER OF REFLECTIONS             : 76123
REMARK   3
REMARK   3  FIT TO DATA USED IN REFINEMENT.
REMARK   3   R VALUE     (WORKING + TEST SET) : 0.197
REMARK   3   R VALUE            (WORKING SET) : 0.195
REMARK   3   FREE R VALUE                     : 0.236
REMARK   3   FREE R VALUE TEST SET SIZE   (%) : 5.190
REMARK   3   FREE R VALUE TEST SET COUNT      : 3952
REMARK   3
REMARK   3  FIT TO DATA USED IN REFINEMENT (IN BINS).
REMARK   3   BIN  RESOLUTION RANGE  COMPL.    NWORK NFREE   RWORK  RFREE
REMARK   3     1124.6900 -  8.0900    0.99     2646   121  0.1700 0.1756
REMARK   3     2  8.0900 -  6.4200    1.00     2603   140  0.1786 0.1824
REMARK   3     3  6.4200 -  5.6100    1.00     2577   157  0.1794 0.2005
REMARK   3     4  5.6100 -  5.1000    1.00     2597   144  0.1647 0.2222
REMARK   3     5  5.1000 -  4.7300    1.00     2562   173  0.1497 0.1848
REMARK   3     6  4.7300 -  4.4500    1.00     2554   152  0.1372 0.1996
REMARK   3     7  4.4500 -  4.2300    1.00     2562   158  0.1436 0.1784
REMARK   3     8  4.2300 -  4.0500    1.00     2624   127  0.1543 0.1774
REMARK   3     9  4.0500 -  3.8900    1.00     2598   112  0.1619 0.2120
REMARK   3    10  3.8900 -  3.7600    1.00     2550   176  0.1744 0.2288
REMARK   3    11  3.7600 -  3.6400    1.00     2641    93  0.1866 0.2187
REMARK   3    12  3.6400 -  3.5300    1.00     2583   131  0.1881 0.2286
REMARK   3    13  3.5300 -  3.4400    1.00     2573   141  0.1985 0.2897
REMARK   3    14  3.4400 -  3.3600    1.00     2570   132  0.2205 0.2605
REMARK   3    15  3.3600 -  3.2800    1.00     2591   136  0.2172 0.2677
REMARK   3    16  3.2800 -  3.2100    1.00     2589   136  0.2322 0.2744
REMARK   3    17  3.2100 -  3.1500    1.00     2581   135  0.2436 0.2918
REMARK   3    18  3.1500 -  3.0900    1.00     2577   170  0.2547 0.2743
REMARK   3    19  3.0900 -  3.0300    1.00     2526   147  0.2505 0.3169
REMARK   3    20  3.0300 -  2.9800    1.00     2592   133  0.2491 0.3110
REMARK   3    21  2.9800 -  2.9300    1.00     2594   120  0.2596 0.2963
REMARK   3    22  2.9300 -  2.8900    1.00     2569   155  0.2612 0.3285
REMARK   3    23  2.8900 -  2.8400    1.00     2541   156  0.2621 0.2965
REMARK   3    24  2.8400 -  2.8000    1.00     2580   155  0.2609 0.2951
REMARK   3    25  2.8000 -  2.7700    1.00     2513   145  0.2676 0.3340
REMARK   3    26  2.7700 -  2.7300    1.00     2614   129  0.2836 0.3176
REMARK   3    27  2.7300 -  2.7000    0.99     2556   128  0.2886 0.3156
REMARK   3    28  2.7000 -  2.6600    0.98     2508   150  0.2853 0.3402
REMARK   3
REMARK   3  BULK SOLVENT MODELLING.
REMARK   3   METHOD USED        : FLAT BULK SOLVENT MODEL
REMARK   3   SOLVENT RADIUS     : 1.10
REMARK   3   SHRINKAGE RADIUS   : 0.90
REMARK   3   K_SOL              : NULL
REMARK   3   B_SOL              : NULL
REMARK   3
REMARK   3  ERROR ESTIMATES.
REMARK   3   COORDINATE ERROR (MAXIMUM-LIKELIHOOD BASED)     : 0.362
REMARK   3   PHASE ERROR (DEGREES, MAXIMUM-LIKELIHOOD BASED) : 24.190
REMARK   3
REMARK   3  B VALUES.
REMARK   3   FROM WILSON PLOT           (A**2) : 41.58
REMARK   3   MEAN B VALUE      (OVERALL, A**2) : 52.34
REMARK   3   OVERALL ANISOTROPIC B VALUE.
REMARK   3    B11 (A**2) : NULL
REMARK   3    B22 (A**2) : NULL
REMARK   3    B33 (A**2) : NULL
REMARK   3    B12 (A**2) : NULL
REMARK   3    B13 (A**2) : NULL
REMARK   3    B23 (A**2) : NULL
REMARK   3
REMARK   3  TWINNING INFORMATION.
REMARK   3   FRACTION: NULL
REMARK   3   OPERATOR: NULL
REMARK   3
REMARK   3  DEVIATIONS FROM IDEAL VALUES.
REMARK   3                 RMSD          COUNT
REMARK   3   BOND      :  0.003          17497
REMARK   3   ANGLE     :  0.580          23724
REMARK   3   CHIRALITY :  0.044           2585
REMARK   3   PLANARITY :  0.005           3017
REMARK   3   DIHEDRAL  : 16.124           6766
REMARK   3
REMARK   3  TLS DETAILS
REMARK   3   NUMBER OF TLS GROUPS  : 4
REMARK   3   TLS GROUP : 1
REMARK   3    SELECTION: CHAIN 'A'
REMARK   3    ORIGIN FOR THE GROUP (A): -11.7180  25.0013   8.1960
REMARK   3    T TENSOR
REMARK   3      T11:   0.1638 T22:   0.2295
REMARK   3      T33:   0.1477 T12:   0.0209
REMARK   3      T13:  -0.0096 T23:   0.0210
REMARK   3    L TENSOR
REMARK   3      L11:   0.2183 L22:   0.3211
REMARK   3      L33:   0.2380 L12:  -0.0989
REMARK   3      L13:  -0.1144 L23:   0.2591
REMARK   3    S TENSOR
REMARK   3      S11:  -0.0080 S12:   0.0791 S13:   0.0330
REMARK   3      S21:  -0.0884 S22:   0.0300 S23:   0.0324
REMARK   3      S31:  -0.0318 S32:  -0.0052 S33:   0.0002
REMARK   3   TLS GROUP : 2
REMARK   3    SELECTION: CHAIN 'B'
REMARK   3    ORIGIN FOR THE GROUP (A): -40.1232  45.5587  32.4429
REMARK   3    T TENSOR
REMARK   3      T11:   0.1305 T22:   0.2343
REMARK   3      T33:   0.2408 T12:   0.0260
REMARK   3      T13:  -0.0104 T23:  -0.0047
REMARK   3    L TENSOR
REMARK   3      L11:   0.2822 L22:   0.1572
REMARK   3      L33:   0.1722 L12:  -0.0848
REMARK   3      L13:  -0.2021 L23:  -0.0237
REMARK   3    S TENSOR
REMARK   3      S11:   0.0139 S12:  -0.0443 S13:  -0.0015
REMARK   3      S21:  -0.0216 S22:  -0.0611 S23:  -0.0192
REMARK   3      S31:  -0.0216 S32:   0.0719 S33:  -0.0004
REMARK   3   TLS GROUP : 3
REMARK   3    SELECTION: CHAIN 'C'
REMARK   3    ORIGIN FOR THE GROUP (A): -85.7143  47.9021  44.3119
REMARK   3    T TENSOR
REMARK   3      T11:   0.0126 T22:   0.5682
REMARK   3      T33:   0.2112 T12:  -0.0667
REMARK   3      T13:  -0.0141 T23:   0.0292
REMARK   3    L TENSOR
REMARK   3      L11:   0.4315 L22:   0.5564
REMARK   3      L33:   0.2698 L12:   0.2222
REMARK   3      L13:  -0.2182 L23:  -0.0801
REMARK   3    S TENSOR
REMARK   3      S11:   0.0167 S12:   0.4853 S13:  -0.1042
REMARK   3      S21:   0.1097 S22:   0.1669 S23:  -0.0147
REMARK   3      S31:  -0.0927 S32:  -0.3390 S33:   0.1910
REMARK   3   TLS GROUP : 4
REMARK   3    SELECTION: CHAIN 'D'
REMARK   3    ORIGIN FOR THE GROUP (A): -19.4465 -19.5859  -4.7950
REMARK   3    T TENSOR
REMARK   3      T11:   0.4825 T22:   0.2295
REMARK   3      T33:   0.3533 T12:  -0.2802
REMARK   3      T13:   0.0330 T23:  -0.0230
REMARK   3    L TENSOR
REMARK   3      L11:   0.1803 L22:   0.1537
REMARK   3      L33:   0.1554 L12:   0.0007
REMARK   3      L13:   0.0411 L23:   0.1126
REMARK   3    S TENSOR
REMARK   3      S11:  -0.0381 S12:   0.0860 S13:  -0.0920
REMARK   3      S21:   0.0771 S22:   0.0136 S23:   0.1750
REMARK   3      S31:   0.4238 S32:  -0.1065 S33:  -0.0108
REMARK   3
REMARK   3  NCS DETAILS
REMARK   3   NUMBER OF NCS GROUPS : NULL
REMARK   3
REMARK   3  OTHER REFINEMENT REMARKS: NULL
REMARK   4
REMARK   4 9HH0 COMPLIES WITH FORMAT V. 3.30, 13-JUL-11
REMARK 100
REMARK 100 THIS ENTRY HAS BEEN PROCESSED BY PDBE ON 20-NOV-24.
REMARK 100 THE DEPOSITION ID IS D_1292143315.
REMARK 200
REMARK 200 EXPERIMENTAL DETAILS
REMARK 200  EXPERIMENT TYPE                : X-RAY DIFFRACTION
REMARK 200  DATE OF DATA COLLECTION        : 05-DEC-12
REMARK 200  TEMPERATURE           (KELVIN) : 100
REMARK 200  PH                             : NULL
REMARK 200  NUMBER OF CRYSTALS USED        : 1
REMARK 200
REMARK 200  SYNCHROTRON              (Y/N) : Y
REMARK 200  RADIATION SOURCE               : ESRF
REMARK 200  BEAMLINE                       : ID23-2
REMARK 200  X-RAY GENERATOR MODEL          : NULL
REMARK 200  MONOCHROMATIC OR LAUE    (M/L) : M
REMARK 200  WAVELENGTH OR RANGE        (A) : 0.872600
REMARK 200  MONOCHROMATOR                  : NULL
REMARK 200  OPTICS                         : NULL
REMARK 200
REMARK 200  DETECTOR TYPE                  : CCD
REMARK 200  DETECTOR MANUFACTURER          : MAR CCD 300 MM
REMARK 200  INTENSITY-INTEGRATION SOFTWARE : XDS
REMARK 200  DATA SCALING SOFTWARE          : XSCALE
REMARK 200
REMARK 200  NUMBER OF UNIQUE REFLECTIONS   : 76253
REMARK 200  RESOLUTION RANGE HIGH      (A) : 2.660
REMARK 200  RESOLUTION RANGE LOW       (A) : 124.700
REMARK 200  REJECTION CRITERIA  (SIGMA(I)) : NULL
REMARK 200
REMARK 200 OVERALL.
REMARK 200  COMPLETENESS FOR RANGE     (%) : 99.8
REMARK 200  DATA REDUNDANCY                : 3.900
REMARK 200  R MERGE                    (I) : 0.15260
REMARK 200  R SYM                      (I) : NULL
REMARK 200   FOR THE DATA SET  : 8.2200
REMARK 200
REMARK 200 IN THE HIGHEST RESOLUTION SHELL.
REMARK 200  HIGHEST RESOLUTION SHELL, RANGE HIGH (A) : 2.66
REMARK 200  HIGHEST RESOLUTION SHELL, RANGE LOW  (A) : 2.70
REMARK 200  COMPLETENESS FOR SHELL     (%) : 97.8
REMARK 200  DATA REDUNDANCY IN SHELL       : 3.50
REMARK 200  R MERGE FOR SHELL          (I) : 1.31100
REMARK 200  R SYM FOR SHELL            (I) : NULL
REMARK 200   FOR SHELL         : 1.250
REMARK 200
REMARK 200 DIFFRACTION PROTOCOL: SINGLE WAVELENGTH
REMARK 200 METHOD USED TO DETERMINE THE STRUCTURE: MOLECULAR REPLACEMENT
REMARK 200 SOFTWARE USED: PHASER
REMARK 200 STARTING MODEL: NULL
REMARK 200
REMARK 200 REMARK: NULL
REMARK 280
REMARK 280 CRYSTAL
REMARK 280 SOLVENT CONTENT, VS   (%): 56.73
REMARK 280 MATTHEWS COEFFICIENT, VM (ANGSTROMS**3/DA): 2.84
REMARK 280
REMARK 280 CRYSTALLIZATION CONDITIONS: PEG 3350, VAPOR DIFFUSION, HANGING
REMARK 280  DROP, TEMPERATURE 293K
REMARK 290
REMARK 290 CRYSTALLOGRAPHIC SYMMETRY
REMARK 290 SYMMETRY OPERATORS FOR SPACE GROUP: P 41
REMARK 290
REMARK 290      SYMOP   SYMMETRY
REMARK 290     NNNMMM   OPERATOR
REMARK 290       1555   X,Y,Z
REMARK 290       2555   -X,-Y,Z+1/2
REMARK 290       3555   -Y,X,Z+1/4
REMARK 290       4555   Y,-X,Z+3/4
REMARK 290
REMARK 290     WHERE NNN -> OPERATOR NUMBER
REMARK 290           MMM -> TRANSLATION VECTOR
REMARK 290
REMARK 290 CRYSTALLOGRAPHIC SYMMETRY TRANSFORMATIONS
REMARK 290 THE FOLLOWING TRANSFORMATIONS OPERATE ON THE ATOM/HETATM
REMARK 290 RECORDS IN THIS ENTRY TO PRODUCE CRYSTALLOGRAPHICALLY
REMARK 290 RELATED MOLECULES.
REMARK 290   SMTRY1   1  1.000000  0.000000  0.000000        0.00000
REMARK 290   SMTRY2   1  0.000000  1.000000  0.000000        0.00000
REMARK 290   SMTRY3   1  0.000000  0.000000  1.000000        0.00000
REMARK 290   SMTRY1   2 -1.000000  0.000000  0.000000        0.00000
REMARK 290   SMTRY2   2  0.000000 -1.000000  0.000000        0.00000
REMARK 290   SMTRY3   2  0.000000  0.000000  1.000000       87.58650
REMARK 290   SMTRY1   3  0.000000 -1.000000  0.000000        0.00000
REMARK 290   SMTRY2   3  1.000000  0.000000  0.000000        0.00000
REMARK 290   SMTRY3   3  0.000000  0.000000  1.000000       43.79325
REMARK 290   SMTRY1   4  0.000000  1.000000  0.000000        0.00000
REMARK 290   SMTRY2   4 -1.000000  0.000000  0.000000        0.00000
REMARK 290   SMTRY3   4  0.000000  0.000000  1.000000      131.37975
REMARK 290
REMARK 290 REMARK: NULL
REMARK 300
REMARK 300 BIOMOLECULE: 1, 2, 3, 4
REMARK 300 SEE REMARK 350 FOR THE AUTHOR PROVIDED AND/OR PROGRAM
REMARK 300 GENERATED ASSEMBLY INFORMATION FOR THE STRUCTURE IN
REMARK 300 THIS ENTRY. THE REMARK MAY ALSO PROVIDE INFORMATION ON
REMARK 300 BURIED SURFACE AREA.
REMARK 350
REMARK 350 COORDINATES FOR A COMPLETE MULTIMER REPRESENTING THE KNOWN
REMARK 350 BIOLOGICALLY SIGNIFICANT OLIGOMERIZATION STATE OF THE
REMARK 350 MOLECULE CAN BE GENERATED BY APPLYING BIOMT TRANSFORMATIONS
REMARK 350 GIVEN BELOW.  BOTH NON-CRYSTALLOGRAPHIC AND
REMARK 350 CRYSTALLOGRAPHIC OPERATIONS ARE GIVEN.
REMARK 350
REMARK 350 BIOMOLECULE: 1
REMARK 350 AUTHOR DETERMINED BIOLOGICAL UNIT: MONOMERIC
REMARK 350 APPLY THE FOLLOWING TO CHAINS: A, E, F
REMARK 350   BIOMT1   1  1.000000  0.000000  0.000000        0.00000
REMARK 350   BIOMT2   1  0.000000  1.000000  0.000000        0.00000
REMARK 350   BIOMT3   1  0.000000  0.000000  1.000000        0.00000
REMARK 350
REMARK 350 BIOMOLECULE: 2
REMARK 350 AUTHOR DETERMINED BIOLOGICAL UNIT: MONOMERIC
REMARK 350 APPLY THE FOLLOWING TO CHAINS: B, G, H
REMARK 350   BIOMT1   1  1.000000  0.000000  0.000000        0.00000
REMARK 350   BIOMT2   1  0.000000  1.000000  0.000000        0.00000
REMARK 350   BIOMT3   1  0.000000  0.000000  1.000000        0.00000
REMARK 350
REMARK 350 BIOMOLECULE: 3
REMARK 350 AUTHOR DETERMINED BIOLOGICAL UNIT: MONOMERIC
REMARK 350 APPLY THE FOLLOWING TO CHAINS: C, I, J, K
REMARK 350   BIOMT1   1  1.000000  0.000000  0.000000        0.00000
REMARK 350   BIOMT2   1  0.000000  1.000000  0.000000        0.00000
REMARK 350   BIOMT3   1  0.000000  0.000000  1.000000        0.00000
REMARK 350
REMARK 350 BIOMOLECULE: 4
REMARK 350 AUTHOR DETERMINED BIOLOGICAL UNIT: MONOMERIC
REMARK 350 APPLY THE FOLLOWING TO CHAINS: D, L
REMARK 350   BIOMT1   1  1.000000  0.000000  0.000000        0.00000
REMARK 350   BIOMT2   1  0.000000  1.000000  0.000000        0.00000
REMARK 350   BIOMT3   1  0.000000  0.000000  1.000000        0.00000
REMARK 465
REMARK 465 MISSING RESIDUES
REMARK 465 THE FOLLOWING RESIDUES WERE NOT LOCATED IN THE
REMARK 465 EXPERIMENT. (M=MODEL NUMBER; RES=RESIDUE NAME; C=CHAIN
REMARK 465 IDENTIFIER; SSSEQ=SEQUENCE NUMBER; I=INSERTION CODE.)
REMARK 465
REMARK 465   M RES C SSSEQI
REMARK 465     GLU A     1
REMARK 465     GLU A     2
REMARK 465     ASP A     3
REMARK 465     GLY A   482
REMARK 465     THR A   483
REMARK 465     GLN A   484
REMARK 465     GLU B     1
REMARK 465     GLU B     2
REMARK 465     GLY B   482
REMARK 465     THR B   483
REMARK 465     GLN B   484
REMARK 465     ASN B   485
REMARK 465     ASN B   486
REMARK 465     GLU C     1
REMARK 465     GLU C     2
REMARK 465     ASP C     3
REMARK 465     GLY C   482
REMARK 465     THR C   483
REMARK 465     GLN C   484
REMARK 465     ASN C   485
REMARK 465     ASN C   486
REMARK 465     GLU D     1
REMARK 465     GLU D     2
REMARK 465     ASP D     3
REMARK 465     ILE D     4
REMARK 465     ILE D     5
REMARK 465     VAL D     6
REMARK 465     THR D     7
REMARK 465     THR D     8
REMARK 465     LYS D     9
REMARK 465     MET D    49
REMARK 465     TRP D    56
REMARK 465     ASN D    57
REMARK 465     VAL D   280
REMARK 465     PRO D   281
REMARK 465     ASN D   282
REMARK 465     HIS D   283
REMARK 465     MET D   284
REMARK 465     ASN D   481
REMARK 465     GLY D   482
REMARK 465     THR D   483
REMARK 465     GLN D   484
REMARK 500
REMARK 500 GEOMETRY AND STEREOCHEMISTRY
REMARK 500 SUBTOPIC: CLOSE CONTACTS IN SAME ASYMMETRIC UNIT
REMARK 500
REMARK 500 THE FOLLOWING ATOMS ARE IN CLOSE CONTACT.
REMARK 500
REMARK 500  ATM1  RES C  SSEQI   ATM2  RES C  SSEQI           DISTANCE
REMARK 500   NE2  HIS D   438     O2    GB D   601              1.30
REMARK 500
REMARK 500 REMARK: NULL
REMARK 500
REMARK 500 GEOMETRY AND STEREOCHEMISTRY
REMARK 500 SUBTOPIC: TORSION ANGLES
REMARK 500
REMARK 500 TORSION ANGLES OUTSIDE THE EXPECTED RAMACHANDRAN REGIONS:
REMARK 500 (M=MODEL NUMBER; RES=RESIDUE NAME; C=CHAIN IDENTIFIER;
REMARK 500 SSEQ=SEQUENCE NUMBER; I=INSERTION CODE).
REMARK 500
REMARK 500 STANDARD TABLE:
REMARK 500 FORMAT:(10X,I3,1X,A3,1X,A1,I4,A1,4X,F7.2,3X,F7.2)
REMARK 500
REMARK 500 EXPECTED VALUES: GJ KLEYWEGT AND TA JONES (1996). PHI/PSI-
REMARK 500 CHOLOGY: RAMACHANDRAN REVISITED. STRUCTURE 4, 1395 - 1400
REMARK 500
REMARK 500  M RES CSSEQI        PSI       PHI
REMARK 500    PHE A  43       -4.37     72.93
REMARK 500    ASP A  54     -158.05   -103.23
REMARK 500    ALA A  62     -168.11    -76.67
REMARK 500    ASN A 106       50.35   -146.59
REMARK 500    PHE A 153       19.48   -140.65
REMARK 500    ALA A 162       79.11   -157.13
REMARK 500    SER A 198     -112.60     59.84
REMARK 500    VAL A 288       90.23    -63.37
REMARK 500    ASP A 297      -76.34   -102.76
REMARK 500    ASP A 324       77.50   -117.05
REMARK 500    MET A 374      -66.60   -125.11
REMARK 500    ILE A 398      -59.16   -127.62
REMARK 500    GLU A 506      -76.67    -99.74
REMARK 500    LYS A 513       72.50     53.64
REMARK 500    PHE B  43       -2.24     72.28
REMARK 500    ASP B  54     -127.56   -113.94
REMARK 500    ASN B 106       50.46   -149.56
REMARK 500    SER B 198     -114.66     58.66
REMARK 500    HIS B 283       86.79     55.00
REMARK 500    VAL B 288       75.05     47.80
REMARK 500    ASP B 297      -73.74   -123.38
REMARK 500    ASP B 324       75.57   -118.65
REMARK 500    MET B 374      -63.97   -132.28
REMARK 500    ILE B 398      -61.42   -128.80
REMARK 500    GLU B 422       31.98   -140.45
REMARK 500    GLU B 506      -85.72    -94.05
REMARK 500    ASP C  54     -119.12    -79.72
REMARK 500    ASN C 106       62.76     60.22
REMARK 500    PHE C 118       12.22     59.52
REMARK 500    ALA C 162       72.45   -167.46
REMARK 500    LYS C 180      -70.48    -80.34
REMARK 500    ASN C 181       47.98    -99.35
REMARK 500    SER C 198     -112.51     59.04
REMARK 500    ASP C 297      -84.21    -84.00
REMARK 500    ASP C 324       69.25   -116.56
REMARK 500    THR C 377     -159.67   -112.99
REMARK 500    GLU C 383       32.59    -91.20
REMARK 500    ILE C 398      -59.52   -130.08
REMARK 500    PRO C 449        2.25    -62.32
REMARK 500    GLU C 506      -66.44    -96.07
REMARK 500    LYS D  12       80.59   -166.38
REMARK 500    LEU D  21     -108.12     55.26
REMARK 500    PHE D  43       -2.28     77.81
REMARK 500    PRO D  53      -84.38    -85.72
REMARK 500    THR D  59        5.81   -155.64
REMARK 500    ALA D  62     -133.64     34.64
REMARK 500    ASN D  63     -152.61   -147.55
REMARK 500    ASP D  91       97.42    -67.87
REMARK 500    PHE D 153       13.63   -146.82
REMARK 500    ALA D 162       63.64   -161.90
REMARK 500
REMARK 500 THIS ENTRY HAS      62 RAMACHANDRAN OUTLIERS.
REMARK 500
REMARK 500 REMARK: NULL
DBREF1 9HH0 A    1   529  UNP                  A0A4X1VEU5_PIG
DBREF2 9HH0 A     A0A4X1VEU5                         29         557
DBREF1 9HH0 B    1   529  UNP                  A0A4X1VEU5_PIG
DBREF2 9HH0 B     A0A4X1VEU5                         29         557
DBREF1 9HH0 C    1   529  UNP                  A0A4X1VEU5_PIG
DBREF2 9HH0 C     A0A4X1VEU5                         29         557
DBREF1 9HH0 D    1   529  UNP                  A0A4X1VEU5_PIG
DBREF2 9HH0 D     A0A4X1VEU5                         29         557
SEQRES   1 A  529  GLU GLU ASP ILE ILE VAL THR THR LYS ASN GLY LYS VAL
SEQRES   2 A  529  ARG GLY MET ASN LEU PRO VAL LEU GLY GLY THR VAL THR
SEQRES   3 A  529  ALA PHE LEU GLY ILE PRO TYR ALA GLN PRO PRO LEU GLY
SEQRES   4 A  529  ARG LEU ARG PHE LYS LYS PRO GLN SER MET THR LYS TRP
SEQRES   5 A  529  PRO ASP ILE TRP ASN ALA THR LYS TYR ALA ASN SER CYS
SEQRES   6 A  529  TYR GLN ASN THR ASP GLN SER PHE PRO GLY PHE VAL GLY
SEQRES   7 A  529  SER GLU MET TRP ASN PRO ASN THR GLU LEU SER GLU ASP
SEQRES   8 A  529  CYS LEU TYR LEU ASN VAL TRP ILE PRO ALA PRO LYS PRO
SEQRES   9 A  529  LYS ASN ALA THR VAL MET ILE TRP ILE TYR GLY GLY GLY
SEQRES  10 A  529  PHE GLN THR GLY THR SER SER LEU HIS VAL TYR ASP GLY
SEQRES  11 A  529  LYS PHE LEU SER ARG VAL GLU ARG VAL ILE VAL VAL SER
SEQRES  12 A  529  MET ASN TYR ARG VAL GLY ALA LEU GLY PHE LEU ALA LEU
SEQRES  13 A  529  PRO GLY ASN PRO GLU ALA PRO GLY ASN MET GLY LEU PHE
SEQRES  14 A  529  ASP GLN GLN LEU ALA LEU GLN TRP VAL GLN LYS ASN ILE
SEQRES  15 A  529  ALA ALA PHE GLY GLY ASN PRO LYS SER VAL THR LEU PHE
SEQRES  16 A  529  GLY GLU SER ALA GLY ALA VAL SER VAL SER LEU HIS LEU
SEQRES  17 A  529  LEU SER PRO ARG SER HIS PRO LEU PHE ALA ARG ALA ILE
SEQRES  18 A  529  LEU GLN SER GLY SER SER ASN ALA PRO TRP ALA VAL THR
SEQRES  19 A  529  SER LEU TYR GLU ALA ARG ASN ARG THR LEU THR LEU ALA
SEQRES  20 A  529  LYS PHE ILE GLY CYS SER ARG GLU ASN GLU THR GLU ILE
SEQRES  21 A  529  ILE LYS CYS LEU ARG ASN LYS ASP PRO GLN GLU ILE LEU
SEQRES  22 A  529  GLN ASN GLU VAL PHE VAL VAL PRO ASN HIS MET LEU LEU
SEQRES  23 A  529  SER VAL ASN PHE GLY PRO THR VAL ASP GLY ASP PHE LEU
SEQRES  24 A  529  THR ASP LEU PRO ASP THR LEU LEU GLN LEU GLY GLN PHE
SEQRES  25 A  529  LYS LYS THR GLN ILE LEU VAL GLY VAL ASN LYS ASP GLU
SEQRES  26 A  529  GLY THR ALA PHE LEU VAL TYR GLY ALA PRO GLY PHE SER
SEQRES  27 A  529  LYS ASP ASN ASN SER ILE ILE THR ARG LYS GLU PHE GLU
SEQRES  28 A  529  GLU GLY LEU LYS ILE PHE PHE PRO GLY VAL SER GLU PHE
SEQRES  29 A  529  GLY LYS GLU SER ILE LEU PHE HIS TYR MET ASP TRP THR
SEQRES  30 A  529  ASP ASP GLN ARG ALA GLU ASN TYR ARG ASP ALA LEU ASP
SEQRES  31 A  529  ASP VAL VAL GLY ASP TYR ASP ILE ILE CYS PRO ALA LEU
SEQRES  32 A  529  GLU PHE THR LYS LYS PHE SER GLU MET GLY ASN ASN ALA
SEQRES  33 A  529  PHE PHE TYR TYR PHE GLU HIS ARG SER SER LYS LEU PRO
SEQRES  34 A  529  TRP PRO GLU TRP MET GLY VAL MET HIS GLY TYR GLU ILE
SEQRES  35 A  529  GLU PHE VAL PHE GLY LEU PRO LEU GLU ARG ARG ALA ASN
SEQRES  36 A  529  TYR THR LYS ALA GLU GLU ILE LEU SER ARG SER ILE MET
SEQRES  37 A  529  LYS ARG TRP ALA ASN PHE ALA LYS TYR GLY ASN PRO ASN
SEQRES  38 A  529  GLY THR GLN ASN ASN SER THR ARG TRP PRO VAL PHE LYS
SEQRES  39 A  529  SER ASN GLU GLN LYS TYR LEU THR LEU ASN ALA GLU SER
SEQRES  40 A  529  PRO ARG VAL TYR THR LYS LEU ARG ALA GLN GLN CYS ARG
SEQRES  41 A  529  PHE TRP THR LEU PHE PHE PRO LYS VAL
SEQRES   1 B  529  GLU GLU ASP ILE ILE VAL THR THR LYS ASN GLY LYS VAL
SEQRES   2 B  529  ARG GLY MET ASN LEU PRO VAL LEU GLY GLY THR VAL THR
SEQRES   3 B  529  ALA PHE LEU GLY ILE PRO TYR ALA GLN PRO PRO LEU GLY
SEQRES   4 B  529  ARG LEU ARG PHE LYS LYS PRO GLN SER MET THR LYS TRP
SEQRES   5 B  529  PRO ASP ILE TRP ASN ALA THR LYS TYR ALA ASN SER CYS
SEQRES   6 B  529  TYR GLN ASN THR ASP GLN SER PHE PRO GLY PHE VAL GLY
SEQRES   7 B  529  SER GLU MET TRP ASN PRO ASN THR GLU LEU SER GLU ASP
SEQRES   8 B  529  CYS LEU TYR LEU ASN VAL TRP ILE PRO ALA PRO LYS PRO
SEQRES   9 B  529  LYS ASN ALA THR VAL MET ILE TRP ILE TYR GLY GLY GLY
SEQRES  10 B  529  PHE GLN THR GLY THR SER SER LEU HIS VAL TYR ASP GLY
SEQRES  11 B  529  LYS PHE LEU SER ARG VAL GLU ARG VAL ILE VAL VAL SER
SEQRES  12 B  529  MET ASN TYR ARG VAL GLY ALA LEU GLY PHE LEU ALA LEU
SEQRES  13 B  529  PRO GLY ASN PRO GLU ALA PRO GLY ASN MET GLY LEU PHE
SEQRES  14 B  529  ASP GLN GLN LEU ALA LEU GLN TRP VAL GLN LYS ASN ILE
SEQRES  15 B  529  ALA ALA PHE GLY GLY ASN PRO LYS SER VAL THR LEU PHE
SEQRES  16 B  529  GLY GLU SER ALA GLY ALA VAL SER VAL SER LEU HIS LEU
SEQRES  17 B  529  LEU SER PRO ARG SER HIS PRO LEU PHE ALA ARG ALA ILE
SEQRES  18 B  529  LEU GLN SER GLY SER SER ASN ALA PRO TRP ALA VAL THR
SEQRES  19 B  529  SER LEU TYR GLU ALA ARG ASN ARG THR LEU THR LEU ALA
SEQRES  20 B  529  LYS PHE ILE GLY CYS SER ARG GLU ASN GLU THR GLU ILE
SEQRES  21 B  529  ILE LYS CYS LEU ARG ASN LYS ASP PRO GLN GLU ILE LEU
SEQRES  22 B  529  GLN ASN GLU VAL PHE VAL VAL PRO ASN HIS MET LEU LEU
SEQRES  23 B  529  SER VAL ASN PHE GLY PRO THR VAL ASP GLY ASP PHE LEU
SEQRES  24 B  529  THR ASP LEU PRO ASP THR LEU LEU GLN LEU GLY GLN PHE
SEQRES  25 B  529  LYS LYS THR GLN ILE LEU VAL GLY VAL ASN LYS ASP GLU
SEQRES  26 B  529  GLY THR ALA PHE LEU VAL TYR GLY ALA PRO GLY PHE SER
SEQRES  27 B  529  LYS ASP ASN ASN SER ILE ILE THR ARG LYS GLU PHE GLU
SEQRES  28 B  529  GLU GLY LEU LYS ILE PHE PHE PRO GLY VAL SER GLU PHE
SEQRES  29 B  529  GLY LYS GLU SER ILE LEU PHE HIS TYR MET ASP TRP THR
SEQRES  30 B  529  ASP ASP GLN ARG ALA GLU ASN TYR ARG ASP ALA LEU ASP
SEQRES  31 B  529  ASP VAL VAL GLY ASP TYR ASP ILE ILE CYS PRO ALA LEU
SEQRES  32 B  529  GLU PHE THR LYS LYS PHE SER GLU MET GLY ASN ASN ALA
SEQRES  33 B  529  PHE PHE TYR TYR PHE GLU HIS ARG SER SER LYS LEU PRO
SEQRES  34 B  529  TRP PRO GLU TRP MET GLY VAL MET HIS GLY TYR GLU ILE
SEQRES  35 B  529  GLU PHE VAL PHE GLY LEU PRO LEU GLU ARG ARG ALA ASN
SEQRES  36 B  529  TYR THR LYS ALA GLU GLU ILE LEU SER ARG SER ILE MET
SEQRES  37 B  529  LYS ARG TRP ALA ASN PHE ALA LYS TYR GLY ASN PRO ASN
SEQRES  38 B  529  GLY THR GLN ASN ASN SER THR ARG TRP PRO VAL PHE LYS
SEQRES  39 B  529  SER ASN GLU GLN LYS TYR LEU THR LEU ASN ALA GLU SER
SEQRES  40 B  529  PRO ARG VAL TYR THR LYS LEU ARG ALA GLN GLN CYS ARG
SEQRES  41 B  529  PHE TRP THR LEU PHE PHE PRO LYS VAL
SEQRES   1 C  529  GLU GLU ASP ILE ILE VAL THR THR LYS ASN GLY LYS VAL
SEQRES   2 C  529  ARG GLY MET ASN LEU PRO VAL LEU GLY GLY THR VAL THR
SEQRES   3 C  529  ALA PHE LEU GLY ILE PRO TYR ALA GLN PRO PRO LEU GLY
SEQRES   4 C  529  ARG LEU ARG PHE LYS LYS PRO GLN SER MET THR LYS TRP
SEQRES   5 C  529  PRO ASP ILE TRP ASN ALA THR LYS TYR ALA ASN SER CYS
SEQRES   6 C  529  TYR GLN ASN THR ASP GLN SER PHE PRO GLY PHE VAL GLY
SEQRES   7 C  529  SER GLU MET TRP ASN PRO ASN THR GLU LEU SER GLU ASP
SEQRES   8 C  529  CYS LEU TYR LEU ASN VAL TRP ILE PRO ALA PRO LYS PRO
SEQRES   9 C  529  LYS ASN ALA THR VAL MET ILE TRP ILE TYR GLY GLY GLY
SEQRES  10 C  529  PHE GLN THR GLY THR SER SER LEU HIS VAL TYR ASP GLY
SEQRES  11 C  529  LYS PHE LEU SER ARG VAL GLU ARG VAL ILE VAL VAL SER
SEQRES  12 C  529  MET ASN TYR ARG VAL GLY ALA LEU GLY PHE LEU ALA LEU
SEQRES  13 C  529  PRO GLY ASN PRO GLU ALA PRO GLY ASN MET GLY LEU PHE
SEQRES  14 C  529  ASP GLN GLN LEU ALA LEU GLN TRP VAL GLN LYS ASN ILE
SEQRES  15 C  529  ALA ALA PHE GLY GLY ASN PRO LYS SER VAL THR LEU PHE
SEQRES  16 C  529  GLY GLU SER ALA GLY ALA VAL SER VAL SER LEU HIS LEU
SEQRES  17 C  529  LEU SER PRO ARG SER HIS PRO LEU PHE ALA ARG ALA ILE
SEQRES  18 C  529  LEU GLN SER GLY SER SER ASN ALA PRO TRP ALA VAL THR
SEQRES  19 C  529  SER LEU TYR GLU ALA ARG ASN ARG THR LEU THR LEU ALA
SEQRES  20 C  529  LYS PHE ILE GLY CYS SER ARG GLU ASN GLU THR GLU ILE
SEQRES  21 C  529  ILE LYS CYS LEU ARG ASN LYS ASP PRO GLN GLU ILE LEU
SEQRES  22 C  529  GLN ASN GLU VAL PHE VAL VAL PRO ASN HIS MET LEU LEU
SEQRES  23 C  529  SER VAL ASN PHE GLY PRO THR VAL ASP GLY ASP PHE LEU
SEQRES  24 C  529  THR ASP LEU PRO ASP THR LEU LEU GLN LEU GLY GLN PHE
SEQRES  25 C  529  LYS LYS THR GLN ILE LEU VAL GLY VAL ASN LYS ASP GLU
SEQRES  26 C  529  GLY THR ALA PHE LEU VAL TYR GLY ALA PRO GLY PHE SER
SEQRES  27 C  529  LYS ASP ASN ASN SER ILE ILE THR ARG LYS GLU PHE GLU
SEQRES  28 C  529  GLU GLY LEU LYS ILE PHE PHE PRO GLY VAL SER GLU PHE
SEQRES  29 C  529  GLY LYS GLU SER ILE LEU PHE HIS TYR MET ASP TRP THR
SEQRES  30 C  529  ASP ASP GLN ARG ALA GLU ASN TYR ARG ASP ALA LEU ASP
SEQRES  31 C  529  ASP VAL VAL GLY ASP TYR ASP ILE ILE CYS PRO ALA LEU
SEQRES  32 C  529  GLU PHE THR LYS LYS PHE SER GLU MET GLY ASN ASN ALA
SEQRES  33 C  529  PHE PHE TYR TYR PHE GLU HIS ARG SER SER LYS LEU PRO
SEQRES  34 C  529  TRP PRO GLU TRP MET GLY VAL MET HIS GLY TYR GLU ILE
SEQRES  35 C  529  GLU PHE VAL PHE GLY LEU PRO LEU GLU ARG ARG ALA ASN
SEQRES  36 C  529  TYR THR LYS ALA GLU GLU ILE LEU SER ARG SER ILE MET
SEQRES  37 C  529  LYS ARG TRP ALA ASN PHE ALA LYS TYR GLY ASN PRO ASN
SEQRES  38 C  529  GLY THR GLN ASN ASN SER THR ARG TRP PRO VAL PHE LYS
SEQRES  39 C  529  SER ASN GLU GLN LYS TYR LEU THR LEU ASN ALA GLU SER
SEQRES  40 C  529  PRO ARG VAL TYR THR LYS LEU ARG ALA GLN GLN CYS ARG
SEQRES  41 C  529  PHE TRP THR LEU PHE PHE PRO LYS VAL
SEQRES   1 D  529  GLU GLU ASP ILE ILE VAL THR THR LYS ASN GLY LYS VAL
SEQRES   2 D  529  ARG GLY MET ASN LEU PRO VAL LEU GLY GLY THR VAL THR
SEQRES   3 D  529  ALA PHE LEU GLY ILE PRO TYR ALA GLN PRO PRO LEU GLY
SEQRES   4 D  529  ARG LEU ARG PHE LYS LYS PRO GLN SER MET THR LYS TRP
SEQRES   5 D  529  PRO ASP ILE TRP ASN ALA THR LYS TYR ALA ASN SER CYS
SEQRES   6 D  529  TYR GLN ASN THR ASP GLN SER PHE PRO GLY PHE VAL GLY
SEQRES   7 D  529  SER GLU MET TRP ASN PRO ASN THR GLU LEU SER GLU ASP
SEQRES   8 D  529  CYS LEU TYR LEU ASN VAL TRP ILE PRO ALA PRO LYS PRO
SEQRES   9 D  529  LYS ASN ALA THR VAL MET ILE TRP ILE TYR GLY GLY GLY
SEQRES  10 D  529  PHE GLN THR GLY THR SER SER LEU HIS VAL TYR ASP GLY
SEQRES  11 D  529  LYS PHE LEU SER ARG VAL GLU ARG VAL ILE VAL VAL SER
SEQRES  12 D  529  MET ASN TYR ARG VAL GLY ALA LEU GLY PHE LEU ALA LEU
SEQRES  13 D  529  PRO GLY ASN PRO GLU ALA PRO GLY ASN MET GLY LEU PHE
SEQRES  14 D  529  ASP GLN GLN LEU ALA LEU GLN TRP VAL GLN LYS ASN ILE
SEQRES  15 D  529  ALA ALA PHE GLY GLY ASN PRO LYS SER VAL THR LEU PHE
SEQRES  16 D  529  GLY GLU SER ALA GLY ALA VAL SER VAL SER LEU HIS LEU
SEQRES  17 D  529  LEU SER PRO ARG SER HIS PRO LEU PHE ALA ARG ALA ILE
SEQRES  18 D  529  LEU GLN SER GLY SER SER ASN ALA PRO TRP ALA VAL THR
SEQRES  19 D  529  SER LEU TYR GLU ALA ARG ASN ARG THR LEU THR LEU ALA
SEQRES  20 D  529  LYS PHE ILE GLY CYS SER ARG GLU ASN GLU THR GLU ILE
SEQRES  21 D  529  ILE LYS CYS LEU ARG ASN LYS ASP PRO GLN GLU ILE LEU
SEQRES  22 D  529  GLN ASN GLU VAL PHE VAL VAL PRO ASN HIS MET LEU LEU
SEQRES  23 D  529  SER VAL ASN PHE GLY PRO THR VAL ASP GLY ASP PHE LEU
SEQRES  24 D  529  THR ASP LEU PRO ASP THR LEU LEU GLN LEU GLY GLN PHE
SEQRES  25 D  529  LYS LYS THR GLN ILE LEU VAL GLY VAL ASN LYS ASP GLU
SEQRES  26 D  529  GLY THR ALA PHE LEU VAL TYR GLY ALA PRO GLY PHE SER
SEQRES  27 D  529  LYS ASP ASN ASN SER ILE ILE THR ARG LYS GLU PHE GLU
SEQRES  28 D  529  GLU GLY LEU LYS ILE PHE PHE PRO GLY VAL SER GLU PHE
SEQRES  29 D  529  GLY LYS GLU SER ILE LEU PHE HIS TYR MET ASP TRP THR
SEQRES  30 D  529  ASP ASP GLN ARG ALA GLU ASN TYR ARG ASP ALA LEU ASP
SEQRES  31 D  529  ASP VAL VAL GLY ASP TYR ASP ILE ILE CYS PRO ALA LEU
SEQRES  32 D  529  GLU PHE THR LYS LYS PHE SER GLU MET GLY ASN ASN ALA
SEQRES  33 D  529  PHE PHE TYR TYR PHE GLU HIS ARG SER SER LYS LEU PRO
SEQRES  34 D  529  TRP PRO GLU TRP MET GLY VAL MET HIS GLY TYR GLU ILE
SEQRES  35 D  529  GLU PHE VAL PHE GLY LEU PRO LEU GLU ARG ARG ALA ASN
SEQRES  36 D  529  TYR THR LYS ALA GLU GLU ILE LEU SER ARG SER ILE MET
SEQRES  37 D  529  LYS ARG TRP ALA ASN PHE ALA LYS TYR GLY ASN PRO ASN
SEQRES  38 D  529  GLY THR GLN ASN ASN SER THR ARG TRP PRO VAL PHE LYS
SEQRES  39 D  529  SER ASN GLU GLN LYS TYR LEU THR LEU ASN ALA GLU SER
SEQRES  40 D  529  PRO ARG VAL TYR THR LYS LEU ARG ALA GLN GLN CYS ARG
SEQRES  41 D  529  PHE TRP THR LEU PHE PHE PRO LYS VAL
HET    NAG  E   1      14
HET    FUC  E   2      10
HET    NAG  F   1      14
HET    NAG  F   2      14
HET    BMA  F   3      11
HET    MAN  F   4      11
HET    FUC  F   5      10
HET    NAG  G   1      14
HET    FUC  G   2      10
HET    NAG  H   1      14
HET    NAG  H   2      14
HET    NAG  I   1      14
HET    NAG  I   2      14
HET    NAG  J   1      14
HET    NAG  J   2      14
HET    BMA  J   3      11
HET    FUC  J   4      10
HET    NAG  K   1      14
HET    NAG  K   2      14
HET    FUC  K   3      10
HET    NAG  L   1      14
HET    NAG  L   2      14
HET    NAG  A 601      14
HET    NAG  A 602      14
HET    NAG  A 603      14
HET    GOL  A 604       6
HET    GOL  A 605       6
HET    GOL  A 606       6
HET     GB  A 607       4
HET    GOL  A 608       6
HET    SO4  A 609       5
HET    SO4  A 610       5
HET    SO4  A 611       5
HET    SO4  A 612       5
HET    NAG  B 601      14
HET    NAG  B 602      14
HET    PEG  B 603       7
HET     GB  B 604       4
HET    GOL  B 605       6
HET    SO4  B 606       5
HET    EDO  B 607       4
HET    EDO  B 608       4
HET    EDO  B 609       4
HET     GB  C 601       4
HET    GOL  C 602       6
HET    GOL  C 603       6
HET    SO4  C 604       5
HET    SO4  C 605       5
HET     GB  D 601       4
HET    EDO  D 602       4
HETNAM     NAG 2-ACETAMIDO-2-DEOXY-BETA-D-GLUCOPYRANOSE
HETNAM     FUC ALPHA-L-FUCOPYRANOSE
HETNAM     BMA BETA-D-MANNOPYRANOSE
HETNAM     MAN ALPHA-D-MANNOPYRANOSE
HETNAM     GOL GLYCEROL
HETNAM      GB METHYLPHOSPHONIC ACID ESTER GROUP
HETNAM     SO4 SULFATE ION
HETNAM     PEG DI(HYDROXYETHYL)ETHER
HETNAM     EDO 1,2-ETHANEDIOL
HETSYN     NAG N-ACETYL-BETA-D-GLUCOSAMINE; 2-ACETAMIDO-2-DEOXY-BETA-
HETSYN   2 NAG  D-GLUCOSE; 2-ACETAMIDO-2-DEOXY-D-GLUCOSE; 2-ACETAMIDO-
HETSYN   3 NAG  2-DEOXY-GLUCOSE; N-ACETYL-D-GLUCOSAMINE
HETSYN     FUC ALPHA-L-FUCOSE; 6-DEOXY-ALPHA-L-GALACTOPYRANOSE; L-
HETSYN   2 FUC  FUCOSE; FUCOSE
HETSYN     BMA BETA-D-MANNOSE; D-MANNOSE; MANNOSE
HETSYN     MAN ALPHA-D-MANNOSE; D-MANNOSE; MANNOSE
HETSYN     GOL GLYCERIN; PROPANE-1,2,3-TRIOL
HETSYN     EDO ETHYLENE GLYCOL
FORMUL   5  NAG    19(C8 H15 N O6)
FORMUL   5  FUC    5(C6 H12 O5)
FORMUL   6  BMA    2(C6 H12 O6)
FORMUL   6  MAN    C6 H12 O6
FORMUL  16  GOL    7(C3 H8 O3)
FORMUL  19   GB    4(C H5 O3 P)
FORMUL  21  SO4    7(O4 S 2-)
FORMUL  27  PEG    C4 H10 O3
FORMUL  31  EDO    4(C2 H6 O2)
FORMUL  41  HOH   *324(H2 O)
HELIX    1 AA1 LEU A   38  ARG A   42  5                                   5
HELIX    2 AA2 PHE A   76  MET A   81  1                                   6
HELIX    3 AA3 LEU A  125  ASP A  129  5                                   5
HELIX    4 AA4 GLY A  130  ARG A  138  1                                   9
HELIX    5 AA5 VAL A  148  LEU A  154  1                                   7
HELIX    6 AA6 ASN A  165  GLY A  186  1                                  22
HELIX    7 AA7 SER A  198  LEU A  208  1                                  11
HELIX    8 AA8 LEU A  209  PHE A  217  5                                   9
HELIX    9 AA9 SER A  235  GLY A  251  1                                  17
HELIX   10 AB1 ASN A  256  ASN A  266  1                                  11
HELIX   11 AB2 ASP A  268  VAL A  277  1                                  10
HELIX   12 AB3 PHE A  278  VAL A  280  5                                   3
HELIX   13 AB4 LEU A  302  LEU A  309  1                                   8
HELIX   14 AB5 GLY A  326  VAL A  331  1                                   6
HELIX   15 AB6 THR A  346  PHE A  358  1                                  13
HELIX   16 AB7 SER A  362  MET A  374  1                                  13
HELIX   17 AB8 GLU A  383  ILE A  398  1                                  16
HELIX   18 AB9 ILE A  398  MET A  412  1                                  15
HELIX   19 AC1 PRO A  431  GLY A  435  5                                   5
HELIX   20 AC2 GLU A  441  PHE A  446  1                                   6
HELIX   21 AC3 GLY A  447  ASN A  455  5                                   9
HELIX   22 AC4 THR A  457  GLY A  478  1                                  22
HELIX   23 AC5 ARG A  515  PHE A  525  1                                  11
HELIX   24 AC6 PHE A  526  VAL A  529  5                                   4
HELIX   25 AC7 LEU B   38  ARG B   42  5                                   5
HELIX   26 AC8 PHE B   76  MET B   81  1                                   6
HELIX   27 AC9 LEU B  125  ASP B  129  5                                   5
HELIX   28 AD1 GLY B  130  ARG B  138  1                                   9
HELIX   29 AD2 VAL B  148  LEU B  154  1                                   7
HELIX   30 AD3 ASN B  165  ILE B  182  1                                  18
HELIX   31 AD4 ALA B  183  PHE B  185  5                                   3
HELIX   32 AD5 SER B  198  LEU B  208  1                                  11
HELIX   33 AD6 SER B  210  PHE B  217  5                                   8
HELIX   34 AD7 SER B  235  GLY B  251  1                                  17
HELIX   35 AD8 ASN B  256  ARG B  265  1                                  10
HELIX   36 AD9 ASP B  268  VAL B  277  1                                  10
HELIX   37 AE1 LEU B  302  LEU B  309  1                                   8
HELIX   38 AE2 GLY B  326  VAL B  331  1                                   6
HELIX   39 AE3 THR B  346  PHE B  358  1                                  13
HELIX   40 AE4 SER B  362  MET B  374  1                                  13
HELIX   41 AE5 GLU B  383  ILE B  398  1                                  16
HELIX   42 AE6 ILE B  398  GLU B  411  1                                  14
HELIX   43 AE7 PRO B  431  GLY B  435  5                                   5
HELIX   44 AE8 GLU B  441  PHE B  446  1                                   6
HELIX   45 AE9 GLY B  447  ASN B  455  5                                   9
HELIX   46 AF1 THR B  457  GLY B  478  1                                  22
HELIX   47 AF2 ARG B  515  PHE B  525  1                                  11
HELIX   48 AF3 PHE B  526  VAL B  529  5                                   4
HELIX   49 AF4 LEU C   38  ARG C   42  5                                   5
HELIX   50 AF5 PHE C   76  MET C   81  1                                   6
HELIX   51 AF6 LEU C  125  ASP C  129  5                                   5
HELIX   52 AF7 GLY C  130  ARG C  138  1                                   9
HELIX   53 AF8 GLY C  149  LEU C  154  1                                   6
HELIX   54 AF9 ASN C  165  ILE C  182  1                                  18
HELIX   55 AG1 ALA C  183  PHE C  185  5                                   3
HELIX   56 AG2 SER C  198  LEU C  208  1                                  11
HELIX   57 AG3 SER C  210  PHE C  217  5                                   8
HELIX   58 AG4 SER C  235  ILE C  250  1                                  16
HELIX   59 AG5 GLU C  257  ASN C  266  1                                  10
HELIX   60 AG6 ASP C  268  GLU C  276  1                                   9
HELIX   61 AG7 VAL C  277  VAL C  279  5                                   3
HELIX   62 AG8 LEU C  302  LEU C  309  1                                   8
HELIX   63 AG9 GLY C  326  ALA C  334  1                                   9
HELIX   64 AH1 THR C  346  PHE C  358  1                                  13
HELIX   65 AH2 SER C  362  MET C  374  1                                  13
HELIX   66 AH3 GLU C  383  ILE C  398  1                                  16
HELIX   67 AH4 ILE C  398  MET C  412  1                                  15
HELIX   68 AH5 PRO C  431  GLY C  435  5                                   5
HELIX   69 AH6 GLU C  441  PHE C  446  1                                   6
HELIX   70 AH7 GLY C  447  GLU C  451  5                                   5
HELIX   71 AH8 THR C  457  GLY C  478  1                                  22
HELIX   72 AH9 ARG C  515  PHE C  525  1                                  11
HELIX   73 AI1 PHE C  526  VAL C  529  5                                   4
HELIX   74 AI2 LEU D   38  ARG D   42  5                                   5
HELIX   75 AI3 PHE D   76  MET D   81  1                                   6
HELIX   76 AI4 LEU D  125  ASP D  129  5                                   5
HELIX   77 AI5 GLY D  130  ARG D  138  1                                   9
HELIX   78 AI6 GLY D  149  LEU D  154  1                                   6
HELIX   79 AI7 ASN D  165  ILE D  182  1                                  18
HELIX   80 AI8 ALA D  183  PHE D  185  5                                   3
HELIX   81 AI9 SER D  198  LEU D  208  1                                  11
HELIX   82 AJ1 SER D  210  PHE D  217  5                                   8
HELIX   83 AJ2 SER D  235  PHE D  249  1                                  15
HELIX   84 AJ3 ASN D  256  LYS D  267  1                                  12
HELIX   85 AJ4 ASP D  268  ASN D  275  1                                   8
HELIX   86 AJ5 LEU D  302  LEU D  309  1                                   8
HELIX   87 AJ6 GLY D  326  VAL D  331  1                                   6
HELIX   88 AJ7 THR D  346  PHE D  358  1                                  13
HELIX   89 AJ8 SER D  362  MET D  374  1                                  13
HELIX   90 AJ9 GLU D  383  ILE D  398  1                                  16
HELIX   91 AK1 ILE D  398  GLU D  411  1                                  14
HELIX   92 AK2 PRO D  431  GLY D  435  5                                   5
HELIX   93 AK3 GLU D  441  PHE D  446  1                                   6
HELIX   94 AK4 GLY D  447  ASN D  455  5                                   9
HELIX   95 AK5 THR D  457  GLY D  478  1                                  22
HELIX   96 AK6 ARG D  515  PHE D  525  1                                  11
HELIX   97 AK7 PHE D  526  VAL D  529  5                                   4
SHEET    1 AA1 3 ILE A   5  THR A   7  0
SHEET    2 AA1 3 LYS A  12  ARG A  14 -1  O  VAL A  13   N  VAL A   6
SHEET    3 AA1 3 ILE A  55  ASN A  57  1  O  TRP A  56   N  ARG A  14
SHEET    1 AA211 MET A  16  VAL A  20  0
SHEET    2 AA211 GLY A  23  PRO A  32 -1  O  ALA A  27   N  MET A  16
SHEET    3 AA211 TYR A  94  PRO A 100 -1  O  ILE A  99   N  THR A  26
SHEET    4 AA211 ILE A 140  MET A 144 -1  O  SER A 143   N  ASN A  96
SHEET    5 AA211 ALA A 107  ILE A 113  1  N  TRP A 112   O  VAL A 142
SHEET    6 AA211 GLY A 187  GLU A 197  1  O  ASN A 188   N  ALA A 107
SHEET    7 AA211 ARG A 219  GLN A 223  1  O  ARG A 219   N  LEU A 194
SHEET    8 AA211 ILE A 317  ASN A 322  1  O  LEU A 318   N  LEU A 222
SHEET    9 AA211 ALA A 416  PHE A 421  1  O  PHE A 421   N  VAL A 321
SHEET   10 AA211 LYS A 499  LEU A 503  1  O  LEU A 501   N  PHE A 418
SHEET   11 AA211 VAL A 510  THR A 512 -1  O  TYR A 511   N  TYR A 500
SHEET    1 AA3 3 ILE B   5  THR B   7  0
SHEET    2 AA3 3 LYS B  12  ARG B  14 -1  O  VAL B  13   N  VAL B   6
SHEET    3 AA3 3 ILE B  55  TRP B  56  1  O  TRP B  56   N  LYS B  12
SHEET    1 AA411 ASN B  17  VAL B  20  0
SHEET    2 AA411 GLY B  23  PRO B  32 -1  O  VAL B  25   N  LEU B  18
SHEET    3 AA411 TYR B  94  PRO B 100 -1  O  ILE B  99   N  THR B  26
SHEET    4 AA411 ILE B 140  MET B 144 -1  O  SER B 143   N  ASN B  96
SHEET    5 AA411 ALA B 107  ILE B 113  1  N  TRP B 112   O  VAL B 142
SHEET    6 AA411 GLY B 187  GLU B 197  1  O  ASN B 188   N  ALA B 107
SHEET    7 AA411 ARG B 219  GLN B 223  1  O  ARG B 219   N  LEU B 194
SHEET    8 AA411 ILE B 317  ASN B 322  1  O  LEU B 318   N  LEU B 222
SHEET    9 AA411 ALA B 416  PHE B 421  1  O  PHE B 417   N  VAL B 319
SHEET   10 AA411 LYS B 499  LEU B 503  1  O  LEU B 501   N  PHE B 418
SHEET   11 AA411 VAL B 510  THR B 512 -1  O  TYR B 511   N  TYR B 500
SHEET    1 AA5 3 ILE C   5  THR C   8  0
SHEET    2 AA5 3 GLY C  11  ARG C  14 -1  O  VAL C  13   N  VAL C   6
SHEET    3 AA5 3 TRP C  56  ASN C  57  1  O  TRP C  56   N  ARG C  14
SHEET    1 AA611 MET C  16  PRO C  19  0
SHEET    2 AA611 THR C  24  PRO C  32 -1  O  ALA C  27   N  MET C  16
SHEET    3 AA611 TYR C  94  PRO C 100 -1  O  LEU C  95   N  ILE C  31
SHEET    4 AA611 ILE C 140  MET C 144 -1  O  SER C 143   N  ASN C  96
SHEET    5 AA611 ALA C 107  ILE C 113  1  N  TRP C 112   O  VAL C 142
SHEET    6 AA611 GLY C 187  GLU C 197  1  O  ASN C 188   N  ALA C 107
SHEET    7 AA611 ARG C 219  GLN C 223  1  O  ARG C 219   N  LEU C 194
SHEET    8 AA611 ILE C 317  ASN C 322  1  O  LEU C 318   N  LEU C 222
SHEET    9 AA611 ALA C 416  PHE C 421  1  O  PHE C 421   N  VAL C 321
SHEET   10 AA611 LYS C 499  LEU C 503  1  O  LEU C 501   N  PHE C 418
SHEET   11 AA611 VAL C 510  THR C 512 -1  O  TYR C 511   N  TYR C 500
SHEET    1 AA711 MET D  16  VAL D  20  0
SHEET    2 AA711 GLY D  23  PRO D  32 -1  O  VAL D  25   N  LEU D  18
SHEET    3 AA711 TYR D  94  PRO D 100 -1  O  LEU D  95   N  ILE D  31
SHEET    4 AA711 ILE D 140  MET D 144 -1  O  SER D 143   N  ASN D  96
SHEET    5 AA711 ALA D 107  ILE D 113  1  N  MET D 110   O  ILE D 140
SHEET    6 AA711 GLY D 187  GLU D 197  1  O  PHE D 195   N  ILE D 111
SHEET    7 AA711 ARG D 219  GLN D 223  1  O  ARG D 219   N  LEU D 194
SHEET    8 AA711 ILE D 317  ASN D 322  1  O  LEU D 318   N  LEU D 222
SHEET    9 AA711 ALA D 416  PHE D 421  1  O  PHE D 417   N  VAL D 319
SHEET   10 AA711 LYS D 499  LEU D 503  1  O  LEU D 501   N  PHE D 418
SHEET   11 AA711 VAL D 510  THR D 512 -1  O  TYR D 511   N  TYR D 500
SSBOND   1 CYS A   65    CYS A   92                          1555   1555  2.04
SSBOND   2 CYS A  252    CYS A  263                          1555   1555  2.04
SSBOND   3 CYS A  400    CYS A  519                          1555   1555  2.04
SSBOND   4 CYS B   65    CYS B   92                          1555   1555  2.03
SSBOND   5 CYS B  252    CYS B  263                          1555   1555  2.04
SSBOND   6 CYS B  400    CYS B  519                          1555   1555  2.05
SSBOND   7 CYS C   65    CYS C   92                          1555   1555  2.03
SSBOND   8 CYS C  252    CYS C  263                          1555   1555  2.04
SSBOND   9 CYS C  400    CYS C  519                          1555   1555  2.04
SSBOND  10 CYS D   65    CYS D   92                          1555   1555  2.03
SSBOND  11 CYS D  252    CYS D  263                          1555   1555  2.03
SSBOND  12 CYS D  400    CYS D  519                          1555   1555  2.04
LINK         ND2 ASN A  57                 C1  NAG E   1     1555   1555  1.44
LINK         ND2 ASN A 106                 C1  NAG A 601     1555   1555  1.44
LINK         OG  SER A 198                 P1   GB A 607     1555   1555  1.70
LINK         ND2 ASN A 241                 C1  NAG A 602     1555   1555  1.44
LINK         ND2 ASN A 341                 C1  NAG F   1     1555   1555  1.45
LINK         ND2 ASN A 455                 C1  NAG A 603     1555   1555  1.44
LINK         ND2 ASN B  57                 C1  NAG G   1     1555   1555  1.44
LINK         ND2 ASN B 106                 C1  NAG B 601     1555   1555  1.44
LINK         OG  SER B 198                 P1   GB B 604     1555   1555  1.71
LINK         ND2 ASN B 241                 C1  NAG B 602     1555   1555  1.45
LINK         ND2 ASN B 341                 C1  NAG H   1     1555   1555  1.45
LINK         OG  SER C 198                 P1   GB C 601     1555   1555  1.71
LINK         ND2 ASN C 241                 C1  NAG I   1     1555   1555  1.44
LINK         ND2 ASN C 341                 C1  NAG J   1     1555   1555  1.44
LINK         ND2 ASN C 455                 C1  NAG K   1     1555   1555  1.44
LINK         OG  SER D 198                 P1   GB D 601     1555   1555  1.73
LINK         ND2 ASN D 341                 C1  NAG L   1     1555   1555  1.44
LINK         O6  NAG E   1                 C1  FUC E   2     1555   1555  1.44
LINK         O4  NAG F   1                 C1  NAG F   2     1555   1555  1.45
LINK         O6  NAG F   1                 C1  FUC F   5     1555   1555  1.44
LINK         O4  NAG F   2                 C1  BMA F   3     1555   1555  1.45
LINK         O3  BMA F   3                 C1  MAN F   4     1555   1555  1.45
LINK         O6  NAG G   1                 C1  FUC G   2     1555   1555  1.44
LINK         O4  NAG H   1                 C1  NAG H   2     1555   1555  1.45
LINK         O4  NAG I   1                 C1  NAG I   2     1555   1555  1.44
LINK         O4  NAG J   1                 C1  NAG J   2     1555   1555  1.45
LINK         O6  NAG J   1                 C1  FUC J   4     1555   1555  1.44
LINK         O4  NAG J   2                 C1  BMA J   3     1555   1555  1.45
LINK         O4  NAG K   1                 C1  NAG K   2     1555   1555  1.44
LINK         O6  NAG K   1                 C1  FUC K   3     1555   1555  1.44
LINK         O4  NAG L   1                 C1  NAG L   2     1555   1555  1.45
CISPEP   1 ALA A  101    PRO A  102          0        -0.06
CISPEP   2 ALA B  101    PRO B  102          0        -0.02
CISPEP   3 ALA C  101    PRO C  102          0         1.41
CISPEP   4 ALA D  101    PRO D  102          0         4.04
CRYST1  124.692  124.692  175.173  90.00  90.00  90.00 P 41         16
ORIGX1      1.000000  0.000000  0.000000        0.00000
ORIGX2      0.000000  1.000000  0.000000        0.00000
ORIGX3      0.000000  0.000000  1.000000        0.00000
SCALE1      0.008020  0.000000  0.000000        0.00000
SCALE2      0.000000  0.008020  0.000000        0.00000
SCALE3      0.000000  0.000000  0.005709        0.00000
TER    4189      VAL A 529
TER    8363      VAL B 529
TER   12536      VAL C 529
TER   16594      VAL D 529
MASTER      423    0   50   97   53    0    0    617365    4  506  164
END