longtext: 9dk4-pdb

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HEADER    LYASE                                   07-SEP-24   9DK4
TITLE     ANCESTRAL HYDROXYNITRILE LYASE WITH FIFTEEN SUBSTITUTIONS
COMPND    MOL_ID: 1;
COMPND   2 MOLECULE: FIFTEEN-SUBSTITUTION VARIANT OF AN ANCESTRAL HYDROXYNITRILE
COMPND   3 LYASE;
COMPND   4 CHAIN: A, B, C, D;
COMPND   5 ENGINEERED: YES;
COMPND   6 MUTATION: YES
SOURCE    MOL_ID: 1;
SOURCE   2 ORGANISM_SCIENTIFIC: SYNTHETIC CONSTRUCT;
SOURCE   3 ORGANISM_TAXID: 32630;
SOURCE   4 EXPRESSION_SYSTEM: ESCHERICHIA COLI;
SOURCE   5 EXPRESSION_SYSTEM_TAXID: 562
KEYWDS    ENGINEERED PROTEIN, ESTERASE, HYDROXYNITRILE LYASE, HYDROLASE FOLD,
KEYWDS   2 LYASE
EXPDTA    X-RAY DIFFRACTION
AUTHOR    S.C.SARAK,P.TAN,R.L.EVANS III,K.SHI,R.J.KAZLAUSKAS,H.AIHARA,
AUTHOR   2 C.T.PIERCE,M.E.WALSH,L.R.GREENBERG
REVDAT   1   02-OCT-24 9DK4    0
JRNL        AUTH   P.TAN,S.SARAK
JRNL        TITL   TO BE PUBLISHED
JRNL        REF    TO BE PUBLISHED
JRNL        REFN
REMARK   2
REMARK   2 RESOLUTION.    1.88 ANGSTROMS.
REMARK   3
REMARK   3 REFINEMENT.
REMARK   3   PROGRAM     : PHENIX 1.19.2_4158
REMARK   3   AUTHORS     : PAUL ADAMS,PAVEL AFONINE,VINCENT CHEN,IAN
REMARK   3               : DAVIS,KRESHNA GOPAL,RALF GROSSE-KUNSTLEVE,
REMARK   3               : LI-WEI HUNG,ROBERT IMMORMINO,TOM IOERGER,
REMARK   3               : AIRLIE MCCOY,ERIK MCKEE,NIGEL MORIARTY,
REMARK   3               : REETAL PAI,RANDY READ,JANE RICHARDSON,
REMARK   3               : DAVID RICHARDSON,TOD ROMO,JIM SACCHETTINI,
REMARK   3               : NICHOLAS SAUTER,JACOB SMITH,LAURENT
REMARK   3               : STORONI,TOM TERWILLIGER,PETER ZWART
REMARK   3
REMARK   3    REFINEMENT TARGET : GEOSTD + MONOMER LIBRARY + CDL V1.2
REMARK   3
REMARK   3  DATA USED IN REFINEMENT.
REMARK   3   RESOLUTION RANGE HIGH (ANGSTROMS) : 1.88
REMARK   3   RESOLUTION RANGE LOW  (ANGSTROMS) : 46.41
REMARK   3   MIN(FOBS/SIGMA_FOBS)              : 1.350
REMARK   3   COMPLETENESS FOR RANGE        (%) : 91.1
REMARK   3   NUMBER OF REFLECTIONS             : 73431
REMARK   3
REMARK   3  FIT TO DATA USED IN REFINEMENT.
REMARK   3   R VALUE     (WORKING + TEST SET) : 0.188
REMARK   3   R VALUE            (WORKING SET) : 0.186
REMARK   3   FREE R VALUE                     : 0.227
REMARK   3   FREE R VALUE TEST SET SIZE   (%) : 2.710
REMARK   3   FREE R VALUE TEST SET COUNT      : 1993
REMARK   3
REMARK   3  FIT TO DATA USED IN REFINEMENT (IN BINS).
REMARK   3   BIN  RESOLUTION RANGE  COMPL.    NWORK NFREE   RWORK  RFREE
REMARK   3     1 46.4100 -  4.5300    0.99     5654   155  0.1784 0.1831
REMARK   3     2  4.5300 -  3.5900    0.82     4628   128  0.1564 0.2267
REMARK   3     3  3.5900 -  3.1400    0.86     4869   137  0.1858 0.2110
REMARK   3     4  3.1400 -  2.8500    0.99     5504   154  0.1934 0.2215
REMARK   3     5  2.8500 -  2.6500    0.98     5518   156  0.1858 0.2225
REMARK   3     6  2.6500 -  2.4900    0.98     5489   148  0.1824 0.1961
REMARK   3     7  2.4900 -  2.3700    0.97     5465   158  0.1847 0.2442
REMARK   3     8  2.3700 -  2.2600    0.98     5445   151  0.1889 0.2530
REMARK   3     9  2.2600 -  2.1800    0.98     5448   149  0.1930 0.2682
REMARK   3    10  2.1800 -  2.1000    0.97     5421   154  0.2030 0.2372
REMARK   3    11  2.1000 -  2.0400    0.96     5347   149  0.1992 0.2642
REMARK   3    12  2.0400 -  1.9800    0.94     5217   145  0.2086 0.2762
REMARK   3    13  1.9800 -  1.9300    0.80     4495   123  0.2206 0.2553
REMARK   3    14  1.9300 -  1.8800    0.53     2938    86  0.2771 0.3554
REMARK   3
REMARK   3  BULK SOLVENT MODELLING.
REMARK   3   METHOD USED        : FLAT BULK SOLVENT MODEL
REMARK   3   SOLVENT RADIUS     : 1.11
REMARK   3   SHRINKAGE RADIUS   : 0.90
REMARK   3   K_SOL              : NULL
REMARK   3   B_SOL              : NULL
REMARK   3
REMARK   3  ERROR ESTIMATES.
REMARK   3   COORDINATE ERROR (MAXIMUM-LIKELIHOOD BASED)     : 0.191
REMARK   3   PHASE ERROR (DEGREES, MAXIMUM-LIKELIHOOD BASED) : 21.407
REMARK   3
REMARK   3  B VALUES.
REMARK   3   FROM WILSON PLOT           (A**2) : 18.60
REMARK   3   MEAN B VALUE      (OVERALL, A**2) : 18.79
REMARK   3   OVERALL ANISOTROPIC B VALUE.
REMARK   3    B11 (A**2) : NULL
REMARK   3    B22 (A**2) : NULL
REMARK   3    B33 (A**2) : NULL
REMARK   3    B12 (A**2) : NULL
REMARK   3    B13 (A**2) : NULL
REMARK   3    B23 (A**2) : NULL
REMARK   3
REMARK   3  TWINNING INFORMATION.
REMARK   3   FRACTION: NULL
REMARK   3   OPERATOR: NULL
REMARK   3
REMARK   3  DEVIATIONS FROM IDEAL VALUES.
REMARK   3                 RMSD          COUNT
REMARK   3   BOND      :  0.008           8000
REMARK   3   ANGLE     :  0.876          10872
REMARK   3   CHIRALITY :  0.054           1165
REMARK   3   PLANARITY :  0.007           1397
REMARK   3   DIHEDRAL  :  6.125           1057
REMARK   3
REMARK   3  TLS DETAILS
REMARK   3   NUMBER OF TLS GROUPS  : NULL
REMARK   3
REMARK   3  NCS DETAILS
REMARK   3   NUMBER OF NCS GROUPS : NULL
REMARK   3
REMARK   3  OTHER REFINEMENT REMARKS: NULL
REMARK   4
REMARK   4 9DK4 COMPLIES WITH FORMAT V. 3.30, 13-JUL-11
REMARK 100
REMARK 100 THIS ENTRY HAS BEEN PROCESSED BY RCSB ON 09-SEP-24.
REMARK 100 THE DEPOSITION ID IS D_1000284998.
REMARK 200
REMARK 200 EXPERIMENTAL DETAILS
REMARK 200  EXPERIMENT TYPE                : X-RAY DIFFRACTION
REMARK 200  DATE OF DATA COLLECTION        : 03-MAR-24
REMARK 200  TEMPERATURE           (KELVIN) : 100
REMARK 200  PH                             : NULL
REMARK 200  NUMBER OF CRYSTALS USED        : 1
REMARK 200
REMARK 200  SYNCHROTRON              (Y/N) : Y
REMARK 200  RADIATION SOURCE               : NSLS
REMARK 200  BEAMLINE                       : X17B1
REMARK 200  X-RAY GENERATOR MODEL          : NULL
REMARK 200  MONOCHROMATIC OR LAUE    (M/L) : M
REMARK 200  WAVELENGTH OR RANGE        (A) : 0.979
REMARK 200  MONOCHROMATOR                  : NULL
REMARK 200  OPTICS                         : NULL
REMARK 200
REMARK 200  DETECTOR TYPE                  : PIXEL
REMARK 200  DETECTOR MANUFACTURER          : DECTRIS EIGER X 16M
REMARK 200  INTENSITY-INTEGRATION SOFTWARE : HKL-2000
REMARK 200  DATA SCALING SOFTWARE          : HKL-2000
REMARK 200
REMARK 200  NUMBER OF UNIQUE REFLECTIONS   : 73445
REMARK 200  RESOLUTION RANGE HIGH      (A) : 1.880
REMARK 200  RESOLUTION RANGE LOW       (A) : 46.410
REMARK 200  REJECTION CRITERIA  (SIGMA(I)) : NULL
REMARK 200
REMARK 200 OVERALL.
REMARK 200  COMPLETENESS FOR RANGE     (%) : 91.4
REMARK 200  DATA REDUNDANCY                : 3.200
REMARK 200  R MERGE                    (I) : 0.13700
REMARK 200  R SYM                      (I) : 0.13700
REMARK 200   FOR THE DATA SET  : 4.6000
REMARK 200
REMARK 200 IN THE HIGHEST RESOLUTION SHELL.
REMARK 200  HIGHEST RESOLUTION SHELL, RANGE HIGH (A) : 1.88
REMARK 200  HIGHEST RESOLUTION SHELL, RANGE LOW  (A) : 1.93
REMARK 200  COMPLETENESS FOR SHELL     (%) : NULL
REMARK 200  DATA REDUNDANCY IN SHELL       : NULL
REMARK 200  R MERGE FOR SHELL          (I) : 0.40800
REMARK 200  R SYM FOR SHELL            (I) : 0.40800
REMARK 200   FOR SHELL         : NULL
REMARK 200
REMARK 200 DIFFRACTION PROTOCOL: SINGLE WAVELENGTH
REMARK 200 METHOD USED TO DETERMINE THE STRUCTURE: MOLECULAR REPLACEMENT
REMARK 200 SOFTWARE USED: PHASER
REMARK 200 STARTING MODEL: NULL
REMARK 200
REMARK 200 REMARK: NULL
REMARK 280
REMARK 280 CRYSTAL
REMARK 280 SOLVENT CONTENT, VS   (%): 39.10
REMARK 280 MATTHEWS COEFFICIENT, VM (ANGSTROMS**3/DA): 2.02
REMARK 280
REMARK 280 CRYSTALLIZATION CONDITIONS: J000843, C8 5%(W/V) PEG 20K, 25%(W/V)
REMARK 280  1,1,1-TRIS(HYDROXYMETHYL)PROPANE, 1%(W/V) NDSB 195
REMARK 280  (DIMETHYLETHYLAMMONIUM PROPANE SULFONATE), 1 MM OF EACH ALKALI
REMARK 280  (BARIUM ACETATE, CESIUM ACETATE, RUBIDIUM CHLORIDE, STRONTIUM
REMARK 280  ACETATE) AND 0.1 M N,N-BIS(2-HYDROXYETHYL)-2-AMINOETHANESULFONIC
REMARK 280  ACID/TRIETHYLAMINE PH 7.5, VAPOR DIFFUSION, SITTING DROP,
REMARK 280  TEMPERATURE 295K
REMARK 290
REMARK 290 CRYSTALLOGRAPHIC SYMMETRY
REMARK 290 SYMMETRY OPERATORS FOR SPACE GROUP: P 1 21 1
REMARK 290
REMARK 290      SYMOP   SYMMETRY
REMARK 290     NNNMMM   OPERATOR
REMARK 290       1555   X,Y,Z
REMARK 290       2555   -X,Y+1/2,-Z
REMARK 290
REMARK 290     WHERE NNN -> OPERATOR NUMBER
REMARK 290           MMM -> TRANSLATION VECTOR
REMARK 290
REMARK 290 CRYSTALLOGRAPHIC SYMMETRY TRANSFORMATIONS
REMARK 290 THE FOLLOWING TRANSFORMATIONS OPERATE ON THE ATOM/HETATM
REMARK 290 RECORDS IN THIS ENTRY TO PRODUCE CRYSTALLOGRAPHICALLY
REMARK 290 RELATED MOLECULES.
REMARK 290   SMTRY1   1  1.000000  0.000000  0.000000        0.00000
REMARK 290   SMTRY2   1  0.000000  1.000000  0.000000        0.00000
REMARK 290   SMTRY3   1  0.000000  0.000000  1.000000        0.00000
REMARK 290   SMTRY1   2 -1.000000  0.000000  0.000000        0.00000
REMARK 290   SMTRY2   2  0.000000  1.000000  0.000000       40.19250
REMARK 290   SMTRY3   2  0.000000  0.000000 -1.000000        0.00000
REMARK 290
REMARK 290 REMARK: NULL
REMARK 300
REMARK 300 BIOMOLECULE: 1, 2, 3, 4
REMARK 300 SEE REMARK 350 FOR THE AUTHOR PROVIDED AND/OR PROGRAM
REMARK 300 GENERATED ASSEMBLY INFORMATION FOR THE STRUCTURE IN
REMARK 300 THIS ENTRY. THE REMARK MAY ALSO PROVIDE INFORMATION ON
REMARK 300 BURIED SURFACE AREA.
REMARK 350
REMARK 350 COORDINATES FOR A COMPLETE MULTIMER REPRESENTING THE KNOWN
REMARK 350 BIOLOGICALLY SIGNIFICANT OLIGOMERIZATION STATE OF THE
REMARK 350 MOLECULE CAN BE GENERATED BY APPLYING BIOMT TRANSFORMATIONS
REMARK 350 GIVEN BELOW.  BOTH NON-CRYSTALLOGRAPHIC AND
REMARK 350 CRYSTALLOGRAPHIC OPERATIONS ARE GIVEN.
REMARK 350
REMARK 350 BIOMOLECULE: 1
REMARK 350 AUTHOR DETERMINED BIOLOGICAL UNIT: MONOMERIC
REMARK 350 APPLY THE FOLLOWING TO CHAINS: A
REMARK 350   BIOMT1   1  1.000000  0.000000  0.000000        0.00000
REMARK 350   BIOMT2   1  0.000000  1.000000  0.000000        0.00000
REMARK 350   BIOMT3   1  0.000000  0.000000  1.000000        0.00000
REMARK 350
REMARK 350 BIOMOLECULE: 2
REMARK 350 AUTHOR DETERMINED BIOLOGICAL UNIT: MONOMERIC
REMARK 350 APPLY THE FOLLOWING TO CHAINS: B
REMARK 350   BIOMT1   1  1.000000  0.000000  0.000000        0.00000
REMARK 350   BIOMT2   1  0.000000  1.000000  0.000000        0.00000
REMARK 350   BIOMT3   1  0.000000  0.000000  1.000000        0.00000
REMARK 350
REMARK 350 BIOMOLECULE: 3
REMARK 350 AUTHOR DETERMINED BIOLOGICAL UNIT: MONOMERIC
REMARK 350 APPLY THE FOLLOWING TO CHAINS: C
REMARK 350   BIOMT1   1  1.000000  0.000000  0.000000        0.00000
REMARK 350   BIOMT2   1  0.000000  1.000000  0.000000        0.00000
REMARK 350   BIOMT3   1  0.000000  0.000000  1.000000        0.00000
REMARK 350
REMARK 350 BIOMOLECULE: 4
REMARK 350 AUTHOR DETERMINED BIOLOGICAL UNIT: MONOMERIC
REMARK 350 APPLY THE FOLLOWING TO CHAINS: D
REMARK 350   BIOMT1   1  1.000000  0.000000  0.000000        0.00000
REMARK 350   BIOMT2   1  0.000000  1.000000  0.000000        0.00000
REMARK 350   BIOMT3   1  0.000000  0.000000  1.000000        0.00000
REMARK 465
REMARK 465 MISSING RESIDUES
REMARK 465 THE FOLLOWING RESIDUES WERE NOT LOCATED IN THE
REMARK 465 EXPERIMENT. (M=MODEL NUMBER; RES=RESIDUE NAME; C=CHAIN
REMARK 465 IDENTIFIER; SSSEQ=SEQUENCE NUMBER; I=INSERTION CODE.)
REMARK 465
REMARK 465   M RES C SSSEQI
REMARK 465     MET A     1
REMARK 465     GLN A    70
REMARK 465     GLY A    71
REMARK 465     GLU A    72
REMARK 465     SER A   138
REMARK 465     ASN A   139
REMARK 465     ASN A   140
REMARK 465     GLU A   141
REMARK 465     THR A   142
REMARK 465     ASP A   258
REMARK 465     LEU A   259
REMARK 465     LEU A   260
REMARK 465     ALA A   261
REMARK 465     VAL A   262
REMARK 465     ALA A   263
REMARK 465     GLY A   264
REMARK 465     LEU A   265
REMARK 465     GLU A   266
REMARK 465     HIS A   267
REMARK 465     HIS A   268
REMARK 465     HIS A   269
REMARK 465     HIS A   270
REMARK 465     HIS A   271
REMARK 465     HIS A   272
REMARK 465     MET B     1
REMARK 465     GLN B    70
REMARK 465     GLY B    71
REMARK 465     ASN B   139
REMARK 465     ASN B   140
REMARK 465     GLU B   141
REMARK 465     ASP B   258
REMARK 465     LEU B   259
REMARK 465     LEU B   260
REMARK 465     ALA B   261
REMARK 465     VAL B   262
REMARK 465     ALA B   263
REMARK 465     GLY B   264
REMARK 465     LEU B   265
REMARK 465     GLU B   266
REMARK 465     HIS B   267
REMARK 465     HIS B   268
REMARK 465     HIS B   269
REMARK 465     HIS B   270
REMARK 465     HIS B   271
REMARK 465     HIS B   272
REMARK 465     MET C     1
REMARK 465     GLN C    70
REMARK 465     GLY C    71
REMARK 465     GLU C    72
REMARK 465     THR C   137
REMARK 465     SER C   138
REMARK 465     ASN C   139
REMARK 465     ASN C   140
REMARK 465     GLU C   141
REMARK 465     THR C   142
REMARK 465     ASP C   258
REMARK 465     LEU C   259
REMARK 465     LEU C   260
REMARK 465     ALA C   261
REMARK 465     VAL C   262
REMARK 465     ALA C   263
REMARK 465     GLY C   264
REMARK 465     LEU C   265
REMARK 465     GLU C   266
REMARK 465     HIS C   267
REMARK 465     HIS C   268
REMARK 465     HIS C   269
REMARK 465     HIS C   270
REMARK 465     HIS C   271
REMARK 465     HIS C   272
REMARK 465     MET D     1
REMARK 465     GLN D    70
REMARK 465     GLY D    71
REMARK 465     GLU D    72
REMARK 465     THR D   137
REMARK 465     SER D   138
REMARK 465     ASN D   139
REMARK 465     ASN D   140
REMARK 465     GLU D   141
REMARK 465     ASP D   258
REMARK 465     LEU D   259
REMARK 465     LEU D   260
REMARK 465     ALA D   261
REMARK 465     VAL D   262
REMARK 465     ALA D   263
REMARK 465     GLY D   264
REMARK 465     LEU D   265
REMARK 465     GLU D   266
REMARK 465     HIS D   267
REMARK 465     HIS D   268
REMARK 465     HIS D   269
REMARK 465     HIS D   270
REMARK 465     HIS D   271
REMARK 465     HIS D   272
REMARK 470
REMARK 470 MISSING ATOM
REMARK 470 THE FOLLOWING RESIDUES HAVE MISSING ATOMS (M=MODEL NUMBER;
REMARK 470 RES=RESIDUE NAME; C=CHAIN IDENTIFIER; SSEQ=SEQUENCE NUMBER;
REMARK 470 I=INSERTION CODE):
REMARK 470   M RES CSSEQI  ATOMS
REMARK 470     LYS A  32    CE   NZ
REMARK 470     GLN A  50    NE2
REMARK 470     ILE A  51    CG2
REMARK 470     GLU A  66    CG   CD   OE1  OE2
REMARK 470     LYS A  73    CD   CE   NZ
REMARK 470     LYS A  92    CD   CE   NZ
REMARK 470     GLU A 111    CG   CD   OE1  OE2
REMARK 470     GLU A 132    CG   CD   OE1  OE2
REMARK 470     THR A 135    CB   OG1  CG2
REMARK 470     TYR A 136    CB   CG   CD1  CD2  CE1  CE2  CZ
REMARK 470     TYR A 136    OH
REMARK 470     THR A 137    CB   OG1  CG2
REMARK 470     ILE A 143    CG1  CG2  CD1
REMARK 470     THR A 144    CG2
REMARK 470     ILE A 180    CG1  CG2  CD1
REMARK 470     GLN A 185    CG   CD   OE1  NE2
REMARK 470     LYS A 188    NZ
REMARK 470     THR A 190    CG2
REMARK 470     GLU A 191    CB   CG   CD   OE1  OE2
REMARK 470     GLU A 192    CG   CD   OE1  OE2
REMARK 470     LYS A 198    CE   NZ
REMARK 470     LYS A 208    CE   NZ
REMARK 470     GLU A 213    CG   CD   OE1  OE2
REMARK 470     LYS A 223    CG   CD   CE   NZ
REMARK 470     LYS A 226    CE   NZ
REMARK 470     GLU A 244    CD   OE1  OE2
REMARK 470     GLU A 247    CD   OE1  OE2
REMARK 470     LYS B  32    CD   CE   NZ
REMARK 470     LEU B  36    CD1  CD2
REMARK 470     GLN B  50    CG   CD   OE1  NE2
REMARK 470     THR B  53    CG2
REMARK 470     GLU B  56    CG   CD   OE1  OE2
REMARK 470     SER B  67    CB   OG
REMARK 470     GLU B  72    N    CB   CG   CD   OE1  OE2
REMARK 470     LYS B  73    CD   CE   NZ
REMARK 470     LYS B  92    CE   NZ
REMARK 470     GLU B 111    CG   CD   OE1  OE2
REMARK 470     VAL B 124    CB   CG1  CG2
REMARK 470     ASP B 127    OD1  OD2
REMARK 470     GLU B 132    CD   OE1  OE2
REMARK 470     THR B 135    CG2
REMARK 470     THR B 137    CG2
REMARK 470     SER B 138    CB   OG
REMARK 470     THR B 142    CG2
REMARK 470     ILE B 143    CB   CG1  CG2  CD1
REMARK 470     LYS B 156    NZ
REMARK 470     ILE B 180    CG2
REMARK 470     GLN B 185    CG   CD   OE1  NE2
REMARK 470     LYS B 188    CE   NZ
REMARK 470     GLU B 191    CD   OE1  OE2
REMARK 470     LYS B 198    CE   NZ
REMARK 470     LYS B 223    CD   CE   NZ
REMARK 470     LEU C  36    CD1
REMARK 470     THR C  53    CG2
REMARK 470     GLU C  66    CG   CD   OE1  OE2
REMARK 470     LEU C  68    CD1  CD2
REMARK 470     LYS C  73    NZ
REMARK 470     LYS C  92    CE   NZ
REMARK 470     GLU C 111    CG   CD   OE1  OE2
REMARK 470     THR C 135    CG2
REMARK 470     ILE C 143    CG1  CG2  CD1
REMARK 470     THR C 144    CG2
REMARK 470     ILE C 180    CG2
REMARK 470     GLN C 185    CD   OE1  NE2
REMARK 470     GLU C 191    CG   CD   OE1  OE2
REMARK 470     LYS C 208    CE   NZ
REMARK 470     LYS C 223    CD   CE   NZ
REMARK 470     LYS C 226    CG   CD   CE   NZ
REMARK 470     GLU C 244    CD   OE1  OE2
REMARK 470     GLU C 247    CD   OE1  OE2
REMARK 470     LYS D  32    CE   NZ
REMARK 470     LEU D  36    CD1
REMARK 470     GLN D  50    NE2
REMARK 470     THR D  53    CG2
REMARK 470     LYS D  92    CD   CE   NZ
REMARK 470     GLU D 111    CG   CD   OE1  OE2
REMARK 470     VAL D 124    CB   CG1  CG2
REMARK 470     LYS D 129    CE   NZ
REMARK 470     GLU D 132    CG   CD   OE1  OE2
REMARK 470     SER D 134    CB   OG
REMARK 470     THR D 135    OG1  CG2
REMARK 470     THR D 142    OG1  CG2
REMARK 470     ILE D 143    CG2
REMARK 470     LYS D 151    CD   CE   NZ
REMARK 470     LYS D 156    NZ
REMARK 470     ILE D 163    CD1
REMARK 470     ILE D 180    CG1  CG2  CD1
REMARK 470     ASN D 181    OD1  ND2
REMARK 470     GLN D 185    CB   CG   CD   OE1  NE2
REMARK 470     LYS D 188    CE   NZ
REMARK 470     LYS D 198    CE   NZ
REMARK 470     LYS D 208    NZ
REMARK 470     LYS D 223    CD   CE   NZ
REMARK 470     LYS D 226    CE   NZ
REMARK 500
REMARK 500 GEOMETRY AND STEREOCHEMISTRY
REMARK 500 SUBTOPIC: TORSION ANGLES
REMARK 500
REMARK 500 TORSION ANGLES OUTSIDE THE EXPECTED RAMACHANDRAN REGIONS:
REMARK 500 (M=MODEL NUMBER; RES=RESIDUE NAME; C=CHAIN IDENTIFIER;
REMARK 500 SSEQ=SEQUENCE NUMBER; I=INSERTION CODE).
REMARK 500
REMARK 500 STANDARD TABLE:
REMARK 500 FORMAT:(10X,I3,1X,A3,1X,A1,I4,A1,4X,F7.2,3X,F7.2)
REMARK 500
REMARK 500 EXPECTED VALUES: GJ KLEYWEGT AND TA JONES (1996). PHI/PSI-
REMARK 500 CHOLOGY: RAMACHANDRAN REVISITED. STRUCTURE 4, 1395 - 1400
REMARK 500
REMARK 500  M RES CSSEQI        PSI       PHI
REMARK 500    CYS A  13       -0.10     75.20
REMARK 500    SER A  80     -127.67     54.97
REMARK 500    THR A 104       55.41     33.28
REMARK 500    ASP A 109     -167.14   -129.34
REMARK 500    SER A 113      150.25    -48.40
REMARK 500    LYS A 129     -119.01     44.24
REMARK 500    TYR A 222       79.04   -153.38
REMARK 500    ASP A 234     -156.68    -85.99
REMARK 500    MET A 236       58.60   -119.07
REMARK 500    HIS B  14     -167.71   -114.98
REMARK 500    SER B  80     -130.60     56.93
REMARK 500    THR B 104       55.55     31.90
REMARK 500    ASP B 109     -169.42   -126.65
REMARK 500    PHE B 125       75.40     35.97
REMARK 500    LYS B 129     -125.95     46.93
REMARK 500    ASP B 234     -155.74    -85.74
REMARK 500    SER C  80     -127.81     60.99
REMARK 500    THR C 104       56.15     31.51
REMARK 500    LYS C 129     -123.33     52.61
REMARK 500    ASP C 234     -153.53    -86.72
REMARK 500    MET C 236       66.51   -119.50
REMARK 500    LYS C 241       47.90   -142.54
REMARK 500    SER D  80     -126.47     56.46
REMARK 500    THR D 104       56.49     36.47
REMARK 500    ASP D 109     -165.88   -129.94
REMARK 500    PHE D 125       71.04     43.54
REMARK 500    LYS D 129     -121.85     46.67
REMARK 500    ASP D 234     -153.14    -90.75
REMARK 500    MET D 236       62.60   -112.19
REMARK 500    LYS D 241       44.28   -142.27
REMARK 500
REMARK 500 REMARK: NULL
REMARK 620
REMARK 620 METAL COORDINATION
REMARK 620 (M=MODEL NUMBER; RES=RESIDUE NAME; C=CHAIN IDENTIFIER;
REMARK 620 SSEQ=SEQUENCE NUMBER; I=INSERTION CODE):
REMARK 620
REMARK 620 COORDINATION ANGLES FOR:  M RES CSSEQI METAL
REMARK 620                              NA A 301  NA
REMARK 620 N RES CSSEQI ATOM
REMARK 620 1 ASP A  37   OD2
REMARK 620 2 HOH A 445   O    72.7
REMARK 620 3 HOH A 457   O   122.8 126.3
REMARK 620 4 MET B 171   O   125.6  90.9 108.9
REMARK 620 N                    1     2     3
REMARK 620
REMARK 620 COORDINATION ANGLES FOR:  M RES CSSEQI METAL
REMARK 620                              NA D 302  NA
REMARK 620 N RES CSSEQI ATOM
REMARK 620 1 SER A 240   O
REMARK 620 2 HOH A 424   O   123.3
REMARK 620 3 GLU D 206   OE2  83.0 123.0
REMARK 620 4 HOH D 440   O   137.9  88.8 102.7
REMARK 620 N                    1     2     3
REMARK 620
REMARK 620 COORDINATION ANGLES FOR:  M RES CSSEQI METAL
REMARK 620                              NA B 301  NA
REMARK 620 N RES CSSEQI ATOM
REMARK 620 1 HOH A 461   O
REMARK 620 2 GLU B 167   OE1 117.3
REMARK 620 N                    1
REMARK 620
REMARK 620 COORDINATION ANGLES FOR:  M RES CSSEQI METAL
REMARK 620                              NA B 302  NA
REMARK 620 N RES CSSEQI ATOM
REMARK 620 1 GLU B 206   OE2
REMARK 620 2 SER C 240   O    58.7
REMARK 620 N                    1
REMARK 620
REMARK 620 COORDINATION ANGLES FOR:  M RES CSSEQI METAL
REMARK 620                              NA C 301  NA
REMARK 620 N RES CSSEQI ATOM
REMARK 620 1 THR C 110   OG1
REMARK 620 2 TYR C 222   OH   97.2
REMARK 620 N                    1
REMARK 620
REMARK 620 COORDINATION ANGLES FOR:  M RES CSSEQI METAL
REMARK 620                              NA C 302  NA
REMARK 620 N RES CSSEQI ATOM
REMARK 620 1 TYR C 116   OH
REMARK 620 2 ASN C 221   OD1 102.9
REMARK 620 N                    1
REMARK 620
REMARK 620 COORDINATION ANGLES FOR:  M RES CSSEQI METAL
REMARK 620                              NA D 301  NA
REMARK 620 N RES CSSEQI ATOM
REMARK 620 1 ASP D 109   OD1
REMARK 620 2 SER D 113   O   119.7
REMARK 620 3 HOH D 435   O   143.2  86.0
REMARK 620 N                    1     2
DBREF  9DK4 A    1   272  PDB    9DK4     9DK4             1    272
DBREF  9DK4 B    1   272  PDB    9DK4     9DK4             1    272
DBREF  9DK4 C    1   272  PDB    9DK4     9DK4             1    272
DBREF  9DK4 D    1   272  PDB    9DK4     9DK4             1    272
SEQRES   1 A  272  MET ALA THR ALA HIS PHE VAL LEU VAL HIS GLY ALA CYS
SEQRES   2 A  272  HIS GLY ALA TRP ILE TRP TYR LYS LEU LYS PRO LEU LEU
SEQRES   3 A  272  GLU ALA ALA GLY HIS LYS VAL THR ALA LEU ASP LEU ALA
SEQRES   4 A  272  ALA SER GLY ILE ASP PRO ARG GLN ILE GLU GLN ILE ASN
SEQRES   5 A  272  THR PHE ASP GLU TYR SER GLU PRO LEU LEU THR PHE MET
SEQRES   6 A  272  GLU SER LEU PRO GLN GLY GLU LYS VAL ILE LEU VAL GLY
SEQRES   7 A  272  HIS SER PHE GLY GLY LEU ASN ILE ALA LEU ALA ALA ASP
SEQRES   8 A  272  LYS TYR PRO GLU LYS ILE SER ALA ALA VAL PHE LEU THR
SEQRES   9 A  272  ALA LEU MET PRO ASP THR GLU HIS SER PRO SER TYR VAL
SEQRES  10 A  272  VAL ASP LYS PHE MET GLU VAL PHE PRO ASP TRP LYS ASP
SEQRES  11 A  272  THR GLU PHE SER THR TYR THR SER ASN ASN GLU THR ILE
SEQRES  12 A  272  THR GLY MET LEU LEU GLY PHE LYS PHE MET ARG GLU LYS
SEQRES  13 A  272  LEU TYR GLN ASN CYS PRO ILE GLU ASP TYR GLU LEU ALA
SEQRES  14 A  272  LYS MET LEU THR ARG PRO GLY SER PHE PHE ILE ASN ASP
SEQRES  15 A  272  LEU ALA GLN ARG PRO LYS PHE THR GLU GLU GLY TYR GLY
SEQRES  16 A  272  SER ILE LYS ARG VAL TYR VAL TRP THR ASP GLU ASP LYS
SEQRES  17 A  272  ILE PHE PRO PRO GLU PHE GLN LEU TRP GLN ILE GLU ASN
SEQRES  18 A  272  TYR LYS PRO ASP LYS VAL TYR ARG VAL GLN GLY GLY ASP
SEQRES  19 A  272  HIS MET PRO GLN LEU SER LYS THR ASN GLU LEU ALA GLU
SEQRES  20 A  272  ILE LEU GLN GLU VAL ALA ASP THR TYR ALA ASP LEU LEU
SEQRES  21 A  272  ALA VAL ALA GLY LEU GLU HIS HIS HIS HIS HIS HIS
SEQRES   1 B  272  MET ALA THR ALA HIS PHE VAL LEU VAL HIS GLY ALA CYS
SEQRES   2 B  272  HIS GLY ALA TRP ILE TRP TYR LYS LEU LYS PRO LEU LEU
SEQRES   3 B  272  GLU ALA ALA GLY HIS LYS VAL THR ALA LEU ASP LEU ALA
SEQRES   4 B  272  ALA SER GLY ILE ASP PRO ARG GLN ILE GLU GLN ILE ASN
SEQRES   5 B  272  THR PHE ASP GLU TYR SER GLU PRO LEU LEU THR PHE MET
SEQRES   6 B  272  GLU SER LEU PRO GLN GLY GLU LYS VAL ILE LEU VAL GLY
SEQRES   7 B  272  HIS SER PHE GLY GLY LEU ASN ILE ALA LEU ALA ALA ASP
SEQRES   8 B  272  LYS TYR PRO GLU LYS ILE SER ALA ALA VAL PHE LEU THR
SEQRES   9 B  272  ALA LEU MET PRO ASP THR GLU HIS SER PRO SER TYR VAL
SEQRES  10 B  272  VAL ASP LYS PHE MET GLU VAL PHE PRO ASP TRP LYS ASP
SEQRES  11 B  272  THR GLU PHE SER THR TYR THR SER ASN ASN GLU THR ILE
SEQRES  12 B  272  THR GLY MET LEU LEU GLY PHE LYS PHE MET ARG GLU LYS
SEQRES  13 B  272  LEU TYR GLN ASN CYS PRO ILE GLU ASP TYR GLU LEU ALA
SEQRES  14 B  272  LYS MET LEU THR ARG PRO GLY SER PHE PHE ILE ASN ASP
SEQRES  15 B  272  LEU ALA GLN ARG PRO LYS PHE THR GLU GLU GLY TYR GLY
SEQRES  16 B  272  SER ILE LYS ARG VAL TYR VAL TRP THR ASP GLU ASP LYS
SEQRES  17 B  272  ILE PHE PRO PRO GLU PHE GLN LEU TRP GLN ILE GLU ASN
SEQRES  18 B  272  TYR LYS PRO ASP LYS VAL TYR ARG VAL GLN GLY GLY ASP
SEQRES  19 B  272  HIS MET PRO GLN LEU SER LYS THR ASN GLU LEU ALA GLU
SEQRES  20 B  272  ILE LEU GLN GLU VAL ALA ASP THR TYR ALA ASP LEU LEU
SEQRES  21 B  272  ALA VAL ALA GLY LEU GLU HIS HIS HIS HIS HIS HIS
SEQRES   1 C  272  MET ALA THR ALA HIS PHE VAL LEU VAL HIS GLY ALA CYS
SEQRES   2 C  272  HIS GLY ALA TRP ILE TRP TYR LYS LEU LYS PRO LEU LEU
SEQRES   3 C  272  GLU ALA ALA GLY HIS LYS VAL THR ALA LEU ASP LEU ALA
SEQRES   4 C  272  ALA SER GLY ILE ASP PRO ARG GLN ILE GLU GLN ILE ASN
SEQRES   5 C  272  THR PHE ASP GLU TYR SER GLU PRO LEU LEU THR PHE MET
SEQRES   6 C  272  GLU SER LEU PRO GLN GLY GLU LYS VAL ILE LEU VAL GLY
SEQRES   7 C  272  HIS SER PHE GLY GLY LEU ASN ILE ALA LEU ALA ALA ASP
SEQRES   8 C  272  LYS TYR PRO GLU LYS ILE SER ALA ALA VAL PHE LEU THR
SEQRES   9 C  272  ALA LEU MET PRO ASP THR GLU HIS SER PRO SER TYR VAL
SEQRES  10 C  272  VAL ASP LYS PHE MET GLU VAL PHE PRO ASP TRP LYS ASP
SEQRES  11 C  272  THR GLU PHE SER THR TYR THR SER ASN ASN GLU THR ILE
SEQRES  12 C  272  THR GLY MET LEU LEU GLY PHE LYS PHE MET ARG GLU LYS
SEQRES  13 C  272  LEU TYR GLN ASN CYS PRO ILE GLU ASP TYR GLU LEU ALA
SEQRES  14 C  272  LYS MET LEU THR ARG PRO GLY SER PHE PHE ILE ASN ASP
SEQRES  15 C  272  LEU ALA GLN ARG PRO LYS PHE THR GLU GLU GLY TYR GLY
SEQRES  16 C  272  SER ILE LYS ARG VAL TYR VAL TRP THR ASP GLU ASP LYS
SEQRES  17 C  272  ILE PHE PRO PRO GLU PHE GLN LEU TRP GLN ILE GLU ASN
SEQRES  18 C  272  TYR LYS PRO ASP LYS VAL TYR ARG VAL GLN GLY GLY ASP
SEQRES  19 C  272  HIS MET PRO GLN LEU SER LYS THR ASN GLU LEU ALA GLU
SEQRES  20 C  272  ILE LEU GLN GLU VAL ALA ASP THR TYR ALA ASP LEU LEU
SEQRES  21 C  272  ALA VAL ALA GLY LEU GLU HIS HIS HIS HIS HIS HIS
SEQRES   1 D  272  MET ALA THR ALA HIS PHE VAL LEU VAL HIS GLY ALA CYS
SEQRES   2 D  272  HIS GLY ALA TRP ILE TRP TYR LYS LEU LYS PRO LEU LEU
SEQRES   3 D  272  GLU ALA ALA GLY HIS LYS VAL THR ALA LEU ASP LEU ALA
SEQRES   4 D  272  ALA SER GLY ILE ASP PRO ARG GLN ILE GLU GLN ILE ASN
SEQRES   5 D  272  THR PHE ASP GLU TYR SER GLU PRO LEU LEU THR PHE MET
SEQRES   6 D  272  GLU SER LEU PRO GLN GLY GLU LYS VAL ILE LEU VAL GLY
SEQRES   7 D  272  HIS SER PHE GLY GLY LEU ASN ILE ALA LEU ALA ALA ASP
SEQRES   8 D  272  LYS TYR PRO GLU LYS ILE SER ALA ALA VAL PHE LEU THR
SEQRES   9 D  272  ALA LEU MET PRO ASP THR GLU HIS SER PRO SER TYR VAL
SEQRES  10 D  272  VAL ASP LYS PHE MET GLU VAL PHE PRO ASP TRP LYS ASP
SEQRES  11 D  272  THR GLU PHE SER THR TYR THR SER ASN ASN GLU THR ILE
SEQRES  12 D  272  THR GLY MET LEU LEU GLY PHE LYS PHE MET ARG GLU LYS
SEQRES  13 D  272  LEU TYR GLN ASN CYS PRO ILE GLU ASP TYR GLU LEU ALA
SEQRES  14 D  272  LYS MET LEU THR ARG PRO GLY SER PHE PHE ILE ASN ASP
SEQRES  15 D  272  LEU ALA GLN ARG PRO LYS PHE THR GLU GLU GLY TYR GLY
SEQRES  16 D  272  SER ILE LYS ARG VAL TYR VAL TRP THR ASP GLU ASP LYS
SEQRES  17 D  272  ILE PHE PRO PRO GLU PHE GLN LEU TRP GLN ILE GLU ASN
SEQRES  18 D  272  TYR LYS PRO ASP LYS VAL TYR ARG VAL GLN GLY GLY ASP
SEQRES  19 D  272  HIS MET PRO GLN LEU SER LYS THR ASN GLU LEU ALA GLU
SEQRES  20 D  272  ILE LEU GLN GLU VAL ALA ASP THR TYR ALA ASP LEU LEU
SEQRES  21 D  272  ALA VAL ALA GLY LEU GLU HIS HIS HIS HIS HIS HIS
HET     NA  A 301       1
HET     NA  B 301       1
HET     NA  B 302       1
HET     NA  C 301       1
HET     NA  C 302       1
HET     NA  D 301       1
HET     NA  D 302       1
HETNAM      NA SODIUM ION
FORMUL   5   NA    7(NA 1+)
FORMUL  12  HOH   *261(H2 O)
HELIX    1 AA1 GLY A   15  TYR A   20  5                                   6
HELIX    2 AA2 LYS A   21  ALA A   29  1                                   9
HELIX    3 AA3 GLN A   47  ILE A   51  5                                   5
HELIX    4 AA4 THR A   53  SER A   67  1                                  15
HELIX    5 AA5 PHE A   81  TYR A   93  1                                  13
HELIX    6 AA6 SER A  115  VAL A  124  1                                  10
HELIX    7 AA7 GLY A  149  LEU A  157  1                                   9
HELIX    8 AA8 PRO A  162  THR A  173  1                                  12
HELIX    9 AA9 PHE A  179  ARG A  186  1                                   8
HELIX   10 AB1 GLY A  193  ILE A  197  5                                   5
HELIX   11 AB2 PRO A  211  TYR A  222  1                                  12
HELIX   12 AB3 MET A  236  LYS A  241  1                                   6
HELIX   13 AB4 LYS A  241  ALA A  257  1                                  17
HELIX   14 AB5 GLY B   15  TYR B   20  5                                   6
HELIX   15 AB6 LYS B   21  ALA B   29  1                                   9
HELIX   16 AB7 GLN B   47  ILE B   51  5                                   5
HELIX   17 AB8 THR B   53  SER B   58  1                                   6
HELIX   18 AB9 SER B   58  LEU B   68  1                                  11
HELIX   19 AC1 PHE B   81  TYR B   93  1                                  13
HELIX   20 AC2 SER B  115  VAL B  124  1                                  10
HELIX   21 AC3 GLY B  149  LEU B  157  1                                   9
HELIX   22 AC4 PRO B  162  THR B  173  1                                  12
HELIX   23 AC5 PHE B  179  ARG B  186  1                                   8
HELIX   24 AC6 GLY B  193  ILE B  197  5                                   5
HELIX   25 AC7 PRO B  211  TYR B  222  1                                  12
HELIX   26 AC8 MET B  236  LYS B  241  1                                   6
HELIX   27 AC9 LYS B  241  ALA B  257  1                                  17
HELIX   28 AD1 GLY C   15  TYR C   20  5                                   6
HELIX   29 AD2 LYS C   21  ALA C   29  1                                   9
HELIX   30 AD3 GLN C   47  ILE C   51  5                                   5
HELIX   31 AD4 THR C   53  LEU C   68  1                                  16
HELIX   32 AD5 PHE C   81  TYR C   93  1                                  13
HELIX   33 AD6 SER C  115  VAL C  124  1                                  10
HELIX   34 AD7 GLY C  149  LEU C  157  1                                   9
HELIX   35 AD8 PRO C  162  THR C  173  1                                  12
HELIX   36 AD9 PHE C  179  ARG C  186  1                                   8
HELIX   37 AE1 GLY C  193  ILE C  197  5                                   5
HELIX   38 AE2 PRO C  211  TYR C  222  1                                  12
HELIX   39 AE3 MET C  236  LYS C  241  1                                   6
HELIX   40 AE4 LYS C  241  ALA C  257  1                                  17
HELIX   41 AE5 GLY D   15  TYR D   20  5                                   6
HELIX   42 AE6 LYS D   21  ALA D   28  1                                   8
HELIX   43 AE7 GLN D   47  ILE D   51  5                                   5
HELIX   44 AE8 THR D   53  SER D   58  1                                   6
HELIX   45 AE9 SER D   58  LEU D   68  1                                  11
HELIX   46 AF1 PHE D   81  TYR D   93  1                                  13
HELIX   47 AF2 SER D  115  VAL D  124  1                                  10
HELIX   48 AF3 GLY D  149  LEU D  157  1                                   9
HELIX   49 AF4 PRO D  162  THR D  173  1                                  12
HELIX   50 AF5 PHE D  179  ARG D  186  1                                   8
HELIX   51 AF6 GLY D  193  ILE D  197  5                                   5
HELIX   52 AF7 PRO D  211  TYR D  222  1                                  12
HELIX   53 AF8 MET D  236  LYS D  241  1                                   6
HELIX   54 AF9 LYS D  241  ALA D  257  1                                  17
SHEET    1 AA1 6 LYS A  32  LEU A  36  0
SHEET    2 AA1 6 HIS A   5  VAL A   9  1  N  LEU A   8   O  THR A  34
SHEET    3 AA1 6 VAL A  74  HIS A  79  1  O  VAL A  77   N  VAL A   9
SHEET    4 AA1 6 ILE A  97  LEU A 103  1  O  VAL A 101   N  LEU A  76
SHEET    5 AA1 6 ARG A 199  THR A 204  1  O  VAL A 200   N  PHE A 102
SHEET    6 AA1 6 LYS A 226  VAL A 230  1  O  VAL A 230   N  TRP A 203
SHEET    1 AA2 2 GLU A 132  THR A 135  0
SHEET    2 AA2 2 THR A 144  LEU A 147 -1  O  GLY A 145   N  SER A 134
SHEET    1 AA3 6 LYS B  32  LEU B  36  0
SHEET    2 AA3 6 HIS B   5  VAL B   9  1  N  LEU B   8   O  THR B  34
SHEET    3 AA3 6 VAL B  74  HIS B  79  1  O  VAL B  77   N  VAL B   9
SHEET    4 AA3 6 ILE B  97  LEU B 103  1  O  VAL B 101   N  LEU B  76
SHEET    5 AA3 6 ARG B 199  THR B 204  1  O  VAL B 200   N  PHE B 102
SHEET    6 AA3 6 LYS B 226  VAL B 230  1  O  VAL B 230   N  TRP B 203
SHEET    1 AA4 2 GLU B 132  TYR B 136  0
SHEET    2 AA4 2 ILE B 143  LEU B 147 -1  O  GLY B 145   N  SER B 134
SHEET    1 AA5 6 LYS C  32  LEU C  36  0
SHEET    2 AA5 6 HIS C   5  VAL C   9  1  N  LEU C   8   O  THR C  34
SHEET    3 AA5 6 VAL C  74  HIS C  79  1  O  VAL C  77   N  VAL C   9
SHEET    4 AA5 6 ILE C  97  LEU C 103  1  O  VAL C 101   N  LEU C  76
SHEET    5 AA5 6 ARG C 199  THR C 204  1  O  VAL C 200   N  PHE C 102
SHEET    6 AA5 6 LYS C 226  VAL C 230  1  O  VAL C 230   N  TRP C 203
SHEET    1 AA6 3 GLU C 132  SER C 134  0
SHEET    2 AA6 3 GLY C 145  LEU C 147 -1  O  GLY C 145   N  SER C 134
SHEET    3 AA6 3 GLY C 176  SER C 177 -1  O  GLY C 176   N  MET C 146
SHEET    1 AA7 6 LYS D  32  ALA D  35  0
SHEET    2 AA7 6 HIS D   5  VAL D   9  1  N  LEU D   8   O  THR D  34
SHEET    3 AA7 6 VAL D  74  HIS D  79  1  O  VAL D  77   N  VAL D   9
SHEET    4 AA7 6 ILE D  97  LEU D 103  1  O  VAL D 101   N  LEU D  76
SHEET    5 AA7 6 ARG D 199  THR D 204  1  O  VAL D 200   N  PHE D 102
SHEET    6 AA7 6 LYS D 226  VAL D 230  1  O  VAL D 230   N  TRP D 203
SHEET    1 AA8 2 GLU D 132  THR D 135  0
SHEET    2 AA8 2 THR D 144  LEU D 147 -1  O  GLY D 145   N  SER D 134
LINK         OD2 ASP A  37                NA    NA A 301     1555   1555  2.66
LINK         O   SER A 240                NA    NA D 302     1555   1555  2.87
LINK        NA    NA A 301                 O   HOH A 445     1555   1555  3.11
LINK        NA    NA A 301                 O   HOH A 457     1555   1555  2.93
LINK        NA    NA A 301                 O   MET B 171     1555   1555  2.56
LINK         O   HOH A 424                NA    NA D 302     1555   1555  2.85
LINK         O   HOH A 461                NA    NA B 301     1555   1555  2.76
LINK         OE1 GLU B 167                NA    NA B 301     1555   1555  2.41
LINK         OE2 GLU B 206                NA    NA B 302     1555   1555  2.45
LINK        NA    NA B 302                 O   SER C 240     2746   1555  2.93
LINK         OG1 THR C 110                NA    NA C 301     1555   1555  2.51
LINK         OH  TYR C 116                NA    NA C 302     1555   1555  2.91
LINK         OD1 ASN C 221                NA    NA C 302     1555   1555  2.49
LINK         OH  TYR C 222                NA    NA C 301     1555   1555  3.15
LINK         OD1 ASP D 109                NA    NA D 301     1555   1555  2.75
LINK         O   SER D 113                NA    NA D 301     1555   1555  2.76
LINK         OE2 GLU D 206                NA    NA D 302     1555   1555  2.42
LINK        NA    NA D 301                 O   HOH D 435     1555   1555  2.59
LINK        NA    NA D 302                 O   HOH D 440     1555   1555  3.18
CRYST1   67.244   80.385   92.823  90.00  90.62  90.00 P 1 21 1      8
ORIGX1      1.000000  0.000000  0.000000        0.00000
ORIGX2      0.000000  1.000000  0.000000        0.00000
ORIGX3      0.000000  0.000000  1.000000        0.00000
SCALE1      0.014871  0.000000  0.000161        0.00000
SCALE2      0.000000  0.012440  0.000000        0.00000
SCALE3      0.000000  0.000000  0.010774        0.00000
TER    1922      ALA A 257
TER    3880      ALA B 257
TER    5830      ALA C 257
TER    7777      ALA D 257
MASTER      524    0    7   54   33    0    0    6 8041    4   25   84
END