longtext: 9ju4-pdb

content
HEADER    PROTEIN BINDING                         07-OCT-24   9JU4
TITLE     CRYSTAL STRUCTURE OF THE THERMOTOGA MARITIMA COLD SHOCK PROTEIN MUTANT
TITLE    2 EST#13 IN COMPLEX WITH AACEST
COMPND    MOL_ID: 1;
COMPND   2 MOLECULE: ALPHA/BETA HYDROLASE FOLD-3 DOMAIN PROTEIN;
COMPND   3 CHAIN: A;
COMPND   4 ENGINEERED: YES;
COMPND   5 MOL_ID: 2;
COMPND   6 MOLECULE: THE THERMOTOGA MARITIMA COLD SHOCK PROTEIN MUTANT BINDING
COMPND   7 TO AACEST;
COMPND   8 CHAIN: B;
COMPND   9 ENGINEERED: YES
SOURCE    MOL_ID: 1;
SOURCE   2 ORGANISM_SCIENTIFIC: ALICYCLOBACILLUS ACIDOCALDARIUS;
SOURCE   3 ORGANISM_TAXID: 405212;
SOURCE   4 GENE: AACI_2875;
SOURCE   5 EXPRESSION_SYSTEM: ESCHERICHIA COLI BL21(DE3);
SOURCE   6 EXPRESSION_SYSTEM_TAXID: 469008;
SOURCE   7 MOL_ID: 2;
SOURCE   8 ORGANISM_SCIENTIFIC: THERMOTOGA MARITIMA;
SOURCE   9 ORGANISM_TAXID: 2336;
SOURCE  10 EXPRESSION_SYSTEM: ESCHERICHIA COLI BL21(DE3);
SOURCE  11 EXPRESSION_SYSTEM_TAXID: 469008
KEYWDS    ANTIBODY-MIMICS, COLD SHOCK PROTEIN, REFOLDING, HEAT STERILIZATION,
KEYWDS   2 FREEZE-DRYING, PROTEIN BINDING
EXPDTA    X-RAY DIFFRACTION
AUTHOR    S.-I.TANAKA,H.AMESAKA
REVDAT   1   15-JAN-25 9JU4    0
JRNL        AUTH   H.AMESAKA,M.TACHIBANA,M.HARA,S.TOYA,H.NAKAGAWA,H.MATSUMURA,
JRNL        AUTH 2 A.HIRATA,M.FUJIHASHI,K.TAKANO,S.I.TANAKA
JRNL        TITL   HEAT-STERILIZABLE ANTIBODY MIMICS DESIGNED ON THE COLD SHOCK
JRNL        TITL 2 PROTEIN SCAFFOLD FROM HYPERTHERMOPHILE THERMOTOGA MARITIMA.
JRNL        REF    PROTEIN SCI.                  V.  34 70018 2025
JRNL        REFN                   ESSN 1469-896X
JRNL        PMID   39724358
JRNL        DOI    10.1002/PRO.70018
REMARK   2
REMARK   2 RESOLUTION.    2.00 ANGSTROMS.
REMARK   3
REMARK   3 REFINEMENT.
REMARK   3   PROGRAM     : PHENIX (1.17.1_3660: ???)
REMARK   3   AUTHORS     : PAUL ADAMS,PAVEL AFONINE,VINCENT CHEN,IAN
REMARK   3               : DAVIS,KRESHNA GOPAL,RALF GROSSE-KUNSTLEVE,
REMARK   3               : LI-WEI HUNG,ROBERT IMMORMINO,TOM IOERGER,
REMARK   3               : AIRLIE MCCOY,ERIK MCKEE,NIGEL MORIARTY,
REMARK   3               : REETAL PAI,RANDY READ,JANE RICHARDSON,
REMARK   3               : DAVID RICHARDSON,TOD ROMO,JIM SACCHETTINI,
REMARK   3               : NICHOLAS SAUTER,JACOB SMITH,LAURENT
REMARK   3               : STORONI,TOM TERWILLIGER,PETER ZWART
REMARK   3
REMARK   3    REFINEMENT TARGET : ML
REMARK   3
REMARK   3  DATA USED IN REFINEMENT.
REMARK   3   RESOLUTION RANGE HIGH (ANGSTROMS) : 2.00
REMARK   3   RESOLUTION RANGE LOW  (ANGSTROMS) : 46.65
REMARK   3   MIN(FOBS/SIGMA_FOBS)              : 1.350
REMARK   3   COMPLETENESS FOR RANGE        (%) : 98.7
REMARK   3   NUMBER OF REFLECTIONS             : 28793
REMARK   3
REMARK   3  FIT TO DATA USED IN REFINEMENT.
REMARK   3   R VALUE     (WORKING + TEST SET) : 0.171
REMARK   3   R VALUE            (WORKING SET) : 0.170
REMARK   3   FREE R VALUE                     : 0.207
REMARK   3   FREE R VALUE TEST SET SIZE   (%) : 3.080
REMARK   3   FREE R VALUE TEST SET COUNT      : 886
REMARK   3
REMARK   3  FIT TO DATA USED IN REFINEMENT (IN BINS).
REMARK   3   BIN  RESOLUTION RANGE  COMPL.    NWORK NFREE   RWORK  RFREE
REMARK   3     1 46.6500 -  3.6300    0.97     4674   155  0.1568 0.1999
REMARK   3     2  3.6300 -  2.8800    0.99     4669   148  0.1736 0.1996
REMARK   3     3  2.8800 -  2.5200    0.99     4644   152  0.1823 0.2188
REMARK   3     4  2.5200 -  2.2900    0.99     4649   140  0.1777 0.2392
REMARK   3     5  2.2900 -  2.1300    0.99     4618   145  0.1774 0.2008
REMARK   3     6  2.1300 -  2.0000    1.00     4653   146  0.1709 0.2041
REMARK   3
REMARK   3  BULK SOLVENT MODELLING.
REMARK   3   METHOD USED        : FLAT BULK SOLVENT MODEL
REMARK   3   SOLVENT RADIUS     : 1.11
REMARK   3   SHRINKAGE RADIUS   : 0.90
REMARK   3   K_SOL              : NULL
REMARK   3   B_SOL              : NULL
REMARK   3
REMARK   3  ERROR ESTIMATES.
REMARK   3   COORDINATE ERROR (MAXIMUM-LIKELIHOOD BASED)     : 0.160
REMARK   3   PHASE ERROR (DEGREES, MAXIMUM-LIKELIHOOD BASED) : 20.290
REMARK   3
REMARK   3  B VALUES.
REMARK   3   FROM WILSON PLOT           (A**2) : NULL
REMARK   3   MEAN B VALUE      (OVERALL, A**2) : NULL
REMARK   3   OVERALL ANISOTROPIC B VALUE.
REMARK   3    B11 (A**2) : NULL
REMARK   3    B22 (A**2) : NULL
REMARK   3    B33 (A**2) : NULL
REMARK   3    B12 (A**2) : NULL
REMARK   3    B13 (A**2) : NULL
REMARK   3    B23 (A**2) : NULL
REMARK   3
REMARK   3  TWINNING INFORMATION.
REMARK   3   FRACTION: NULL
REMARK   3   OPERATOR: NULL
REMARK   3
REMARK   3  DEVIATIONS FROM IDEAL VALUES.
REMARK   3                 RMSD          COUNT
REMARK   3   BOND      :  0.008           2939
REMARK   3   ANGLE     :  0.873           3995
REMARK   3   CHIRALITY :  0.055            424
REMARK   3   PLANARITY :  0.005            524
REMARK   3   DIHEDRAL  :  7.288            400
REMARK   3
REMARK   3  TLS DETAILS
REMARK   3   NUMBER OF TLS GROUPS  : NULL
REMARK   3
REMARK   3  NCS DETAILS
REMARK   3   NUMBER OF NCS GROUPS : NULL
REMARK   3
REMARK   3  OTHER REFINEMENT REMARKS: NULL
REMARK   4
REMARK   4 9JU4 COMPLIES WITH FORMAT V. 3.30, 13-JUL-11
REMARK 100
REMARK 100 THIS ENTRY HAS BEEN PROCESSED BY PDBJ ON 08-OCT-24.
REMARK 100 THE DEPOSITION ID IS D_1300052253.
REMARK 200
REMARK 200 EXPERIMENTAL DETAILS
REMARK 200  EXPERIMENT TYPE                : X-RAY DIFFRACTION
REMARK 200  DATE OF DATA COLLECTION        : 20-JUL-24
REMARK 200  TEMPERATURE           (KELVIN) : 100
REMARK 200  PH                             : 5.0
REMARK 200  NUMBER OF CRYSTALS USED        : 1
REMARK 200
REMARK 200  SYNCHROTRON              (Y/N) : Y
REMARK 200  RADIATION SOURCE               : SPRING-8
REMARK 200  BEAMLINE                       : BL41XU
REMARK 200  X-RAY GENERATOR MODEL          : NULL
REMARK 200  MONOCHROMATIC OR LAUE    (M/L) : M
REMARK 200  WAVELENGTH OR RANGE        (A) : 1.0
REMARK 200  MONOCHROMATOR                  : NULL
REMARK 200  OPTICS                         : NULL
REMARK 200
REMARK 200  DETECTOR TYPE                  : PIXEL
REMARK 200  DETECTOR MANUFACTURER          : DECTRIS EIGER X 16M
REMARK 200  INTENSITY-INTEGRATION SOFTWARE : XDS
REMARK 200  DATA SCALING SOFTWARE          : XDS
REMARK 200
REMARK 200  NUMBER OF UNIQUE REFLECTIONS   : 28793
REMARK 200  RESOLUTION RANGE HIGH      (A) : 1.520
REMARK 200  RESOLUTION RANGE LOW       (A) : 46.650
REMARK 200  REJECTION CRITERIA  (SIGMA(I)) : NULL
REMARK 200
REMARK 200 OVERALL.
REMARK 200  COMPLETENESS FOR RANGE     (%) : 99.2
REMARK 200  DATA REDUNDANCY                : 4.380
REMARK 200  R MERGE                    (I) : NULL
REMARK 200  R SYM                      (I) : NULL
REMARK 200   FOR THE DATA SET  : 11.1300
REMARK 200
REMARK 200 IN THE HIGHEST RESOLUTION SHELL.
REMARK 200  HIGHEST RESOLUTION SHELL, RANGE HIGH (A) : 1.52
REMARK 200  HIGHEST RESOLUTION SHELL, RANGE LOW  (A) : 1.61
REMARK 200  COMPLETENESS FOR SHELL     (%) : NULL
REMARK 200  DATA REDUNDANCY IN SHELL       : NULL
REMARK 200  R MERGE FOR SHELL          (I) : NULL
REMARK 200  R SYM FOR SHELL            (I) : NULL
REMARK 200   FOR SHELL         : NULL
REMARK 200
REMARK 200 DIFFRACTION PROTOCOL: SINGLE WAVELENGTH
REMARK 200 METHOD USED TO DETERMINE THE STRUCTURE: MOLECULAR REPLACEMENT
REMARK 200 SOFTWARE USED: PHENIX
REMARK 200 STARTING MODEL: NULL
REMARK 200
REMARK 200 REMARK: NEEDLE-LIKE CRYSTALS
REMARK 280
REMARK 280 CRYSTAL
REMARK 280 SOLVENT CONTENT, VS   (%): 54.43
REMARK 280 MATTHEWS COEFFICIENT, VM (ANGSTROMS**3/DA): 2.59
REMARK 280
REMARK 280 CRYSTALLIZATION CONDITIONS: 0.1 M SODIUM CITRATE, PH 5.0, AND 20%
REMARK 280  (W/V) PEG8000, VAPOR DIFFUSION, SITTING DROP, TEMPERATURE 292K
REMARK 290
REMARK 290 CRYSTALLOGRAPHIC SYMMETRY
REMARK 290 SYMMETRY OPERATORS FOR SPACE GROUP: P 1 2 1
REMARK 290
REMARK 290      SYMOP   SYMMETRY
REMARK 290     NNNMMM   OPERATOR
REMARK 290       1555   X,Y,Z
REMARK 290       2555   -X,Y,-Z
REMARK 290
REMARK 290     WHERE NNN -> OPERATOR NUMBER
REMARK 290           MMM -> TRANSLATION VECTOR
REMARK 290
REMARK 290 CRYSTALLOGRAPHIC SYMMETRY TRANSFORMATIONS
REMARK 290 THE FOLLOWING TRANSFORMATIONS OPERATE ON THE ATOM/HETATM
REMARK 290 RECORDS IN THIS ENTRY TO PRODUCE CRYSTALLOGRAPHICALLY
REMARK 290 RELATED MOLECULES.
REMARK 290   SMTRY1   1  1.000000  0.000000  0.000000        0.00000
REMARK 290   SMTRY2   1  0.000000  1.000000  0.000000        0.00000
REMARK 290   SMTRY3   1  0.000000  0.000000  1.000000        0.00000
REMARK 290   SMTRY1   2 -1.000000  0.000000  0.000000        0.00000
REMARK 290   SMTRY2   2  0.000000  1.000000  0.000000        0.00000
REMARK 290   SMTRY3   2  0.000000  0.000000 -1.000000        0.00000
REMARK 290
REMARK 290 REMARK: NULL
REMARK 300
REMARK 300 BIOMOLECULE: 1
REMARK 300 SEE REMARK 350 FOR THE AUTHOR PROVIDED AND/OR PROGRAM
REMARK 300 GENERATED ASSEMBLY INFORMATION FOR THE STRUCTURE IN
REMARK 300 THIS ENTRY. THE REMARK MAY ALSO PROVIDE INFORMATION ON
REMARK 300 BURIED SURFACE AREA.
REMARK 350
REMARK 350 COORDINATES FOR A COMPLETE MULTIMER REPRESENTING THE KNOWN
REMARK 350 BIOLOGICALLY SIGNIFICANT OLIGOMERIZATION STATE OF THE
REMARK 350 MOLECULE CAN BE GENERATED BY APPLYING BIOMT TRANSFORMATIONS
REMARK 350 GIVEN BELOW.  BOTH NON-CRYSTALLOGRAPHIC AND
REMARK 350 CRYSTALLOGRAPHIC OPERATIONS ARE GIVEN.
REMARK 350
REMARK 350 BIOMOLECULE: 1
REMARK 350 AUTHOR DETERMINED BIOLOGICAL UNIT: DIMERIC
REMARK 350 SOFTWARE DETERMINED QUATERNARY STRUCTURE: DIMERIC
REMARK 350 SOFTWARE USED: PISA
REMARK 350 TOTAL BURIED SURFACE AREA: 2310 ANGSTROM**2
REMARK 350 SURFACE AREA OF THE COMPLEX: 15120 ANGSTROM**2
REMARK 350 CHANGE IN SOLVENT FREE ENERGY: 0.0 KCAL/MOL
REMARK 350 APPLY THE FOLLOWING TO CHAINS: A, B
REMARK 350   BIOMT1   1  1.000000  0.000000  0.000000        0.00000
REMARK 350   BIOMT2   1  0.000000  1.000000  0.000000        0.00000
REMARK 350   BIOMT3   1  0.000000  0.000000  1.000000        0.00000
REMARK 375
REMARK 375 SPECIAL POSITION
REMARK 375 THE FOLLOWING ATOMS ARE FOUND TO BE WITHIN 0.15 ANGSTROMS
REMARK 375 OF A SYMMETRY RELATED ATOM AND ARE ASSUMED TO BE ON SPECIAL
REMARK 375 POSITIONS.
REMARK 375
REMARK 375 ATOM RES CSSEQI
REMARK 375      HOH A 621  LIES ON A SPECIAL POSITION.
REMARK 465
REMARK 465 MISSING RESIDUES
REMARK 465 THE FOLLOWING RESIDUES WERE NOT LOCATED IN THE
REMARK 465 EXPERIMENT. (M=MODEL NUMBER; RES=RESIDUE NAME; C=CHAIN
REMARK 465 IDENTIFIER; SSSEQ=SEQUENCE NUMBER; I=INSERTION CODE.)
REMARK 465
REMARK 465   M RES C SSSEQI
REMARK 465     LYS B    19
REMARK 465     ASP B    20
REMARK 465     GLU B    21
REMARK 465     GLY B    22
REMARK 465     GLY B    23
REMARK 465     MET B    34
REMARK 465     GLU B    35
REMARK 465     GLY B    36
REMARK 465     PHE B    37
REMARK 465     VAL B    54
REMARK 465     ALA B    55
REMARK 465     ASN B    56
REMARK 465     VAL B    65
REMARK 465     VAL B    66
REMARK 465     GLU B    67
REMARK 500
REMARK 500 GEOMETRY AND STEREOCHEMISTRY
REMARK 500 SUBTOPIC: TORSION ANGLES
REMARK 500
REMARK 500 TORSION ANGLES OUTSIDE THE EXPECTED RAMACHANDRAN REGIONS:
REMARK 500 (M=MODEL NUMBER; RES=RESIDUE NAME; C=CHAIN IDENTIFIER;
REMARK 500 SSEQ=SEQUENCE NUMBER; I=INSERTION CODE).
REMARK 500
REMARK 500 STANDARD TABLE:
REMARK 500 FORMAT:(10X,I3,1X,A3,1X,A1,I4,A1,4X,F7.2,3X,F7.2)
REMARK 500
REMARK 500 EXPECTED VALUES: GJ KLEYWEGT AND TA JONES (1996). PHI/PSI-
REMARK 500 CHOLOGY: RAMACHANDRAN REVISITED. STRUCTURE 4, 1395 - 1400
REMARK 500
REMARK 500  M RES CSSEQI        PSI       PHI
REMARK 500    ASP A  89     -169.34   -163.17
REMARK 500    SER A 155     -119.77     59.84
REMARK 500    PHE A 178      145.77   -171.24
REMARK 500    TYR A 183       65.85     27.22
REMARK 500    SER A 185       78.21   -102.64
REMARK 500    LEU A 205      -68.19     76.25
REMARK 500    SER A 231       78.94   -117.00
REMARK 500    SER A 289      -17.56     65.21
REMARK 500    SER B  52       33.20    -95.39
REMARK 500    HIS B  62       73.23     41.66
REMARK 500
REMARK 500 REMARK: NULL
DBREF  9JU4 A    1   310  UNP    C8WUR3   C8WUR3_ALIAD     1    310
DBREF  9JU4 B    2    67  PDB    9JU4     9JU4             2     67
SEQRES   1 A  310  MET PRO LEU ASP PRO VAL ILE GLN GLN VAL LEU ASP GLN
SEQRES   2 A  310  LEU ASN ARG MET PRO ALA PRO ASP TYR LYS HIS LEU SER
SEQRES   3 A  310  ALA GLN GLN PHE ARG SER GLN GLN SER LEU PHE PRO PRO
SEQRES   4 A  310  VAL LYS LYS GLU PRO VAL ALA GLU VAL ARG GLU PHE ASP
SEQRES   5 A  310  MET ASP LEU PRO GLY ARG THR LEU LYS VAL ARG MET TYR
SEQRES   6 A  310  ARG PRO GLU GLY VAL GLU PRO PRO TYR PRO ALA LEU VAL
SEQRES   7 A  310  TYR TYR HIS GLY GLY GLY TRP VAL VAL GLY ASP LEU GLU
SEQRES   8 A  310  THR HIS ASP PRO VAL CYS ARG VAL LEU ALA LYS ASP GLY
SEQRES   9 A  310  ARG ALA VAL VAL PHE SER VAL ASP TYR ARG LEU ALA PRO
SEQRES  10 A  310  GLU HIS LYS PHE PRO ALA ALA VAL GLU ASP ALA TYR ASP
SEQRES  11 A  310  ALA LEU GLN TRP ILE ALA GLU ARG ALA ALA ASP PHE HIS
SEQRES  12 A  310  LEU ASP PRO ALA ARG ILE ALA VAL GLY GLY ASP SER ALA
SEQRES  13 A  310  GLY GLY ASN LEU ALA ALA VAL THR SER ILE LEU ALA LYS
SEQRES  14 A  310  GLU ARG GLY GLY PRO ALA ILE ALA PHE GLN LEU LEU ILE
SEQRES  15 A  310  TYR PRO SER THR GLY TYR ASP PRO ALA HIS PRO PRO ALA
SEQRES  16 A  310  SER ILE GLU GLU ASN ALA GLU GLY TYR LEU LEU THR GLY
SEQRES  17 A  310  GLY MET MET LEU TRP PHE ARG ASP GLN TYR LEU ASN SER
SEQRES  18 A  310  LEU GLU GLU LEU THR HIS PRO TRP PHE SER PRO VAL LEU
SEQRES  19 A  310  TYR PRO ASP LEU SER GLY LEU PRO PRO ALA TYR ILE ALA
SEQRES  20 A  310  THR ALA GLN TYR ASP PRO LEU ARG ASP VAL GLY LYS LEU
SEQRES  21 A  310  TYR ALA GLU ALA LEU ASN LYS ALA GLY VAL LYS VAL GLU
SEQRES  22 A  310  ILE GLU ASN PHE GLU ASP LEU ILE HIS GLY PHE ALA GLN
SEQRES  23 A  310  PHE TYR SER LEU SER PRO GLY ALA THR LYS ALA LEU VAL
SEQRES  24 A  310  ARG ILE ALA GLU LYS LEU ARG ASP ALA LEU ALA
SEQRES   1 B   66  ARG GLY LYS VAL LYS TRP PHE HIS ASP TYR TYR GLY TYR
SEQRES   2 B   66  GLY PHE ILE THR LYS ASP GLU GLY GLY ASP VAL PHE VAL
SEQRES   3 B   66  ASN ALA ASP ALA ILE ASP MET GLU GLY PHE LYS THR LEU
SEQRES   4 B   66  LYS GLU GLY GLN VAL VAL GLU PHE GLU ILE ASP SER THR
SEQRES   5 B   66  VAL ALA ASN ALA PRO GLN ALA ALA HIS VAL LYS VAL VAL
SEQRES   6 B   66  GLU
HET    PMS  A 401      10
HET    PEG  A 402       7
HET    GOL  A 403       6
HETNAM     PMS PHENYLMETHANESULFONIC ACID
HETNAM     PEG DI(HYDROXYETHYL)ETHER
HETNAM     GOL GLYCEROL
HETSYN     GOL GLYCERIN; PROPANE-1,2,3-TRIOL
FORMUL   3  PMS    C7 H8 O3 S
FORMUL   4  PEG    C4 H10 O3
FORMUL   5  GOL    C3 H8 O3
FORMUL   6  HOH   *176(H2 O)
HELIX    1 AA1 ASP A    4  ASN A   15  1                                  12
HELIX    2 AA2 SER A   26  GLN A   33  1                                   8
HELIX    3 AA3 HIS A   93  ARG A  105  1                                  13
HELIX    4 AA4 PRO A  122  ARG A  138  1                                  17
HELIX    5 AA5 SER A  155  ARG A  171  1                                  17
HELIX    6 AA6 PRO A  194  ASN A  200  1                                   7
HELIX    7 AA7 THR A  207  LEU A  219  1                                  13
HELIX    8 AA8 SER A  221  HIS A  227  5                                   7
HELIX    9 AA9 SER A  231  TYR A  235  5                                   5
HELIX   10 AB1 LEU A  254  ALA A  268  1                                  15
HELIX   11 AB2 GLY A  283  TYR A  288  5                                   6
HELIX   12 AB3 SER A  291  ALA A  310  1                                  20
HELIX   13 AB4 ASP B   30  ILE B   32  5                                   3
SHEET    1 AA1 8 GLU A  47  LEU A  55  0
SHEET    2 AA1 8 ARG A  58  ARG A  66 -1  O  LEU A  60   N  MET A  53
SHEET    3 AA1 8 VAL A 107  VAL A 111 -1  O  SER A 110   N  ARG A  63
SHEET    4 AA1 8 TYR A  74  TYR A  80  1  N  TYR A  79   O  PHE A 109
SHEET    5 AA1 8 LEU A 144  ASP A 154  1  O  ALA A 150   N  ALA A  76
SHEET    6 AA1 8 GLN A 179  ILE A 182  1  O  ILE A 182   N  GLY A 153
SHEET    7 AA1 8 ALA A 244  ALA A 249  1  O  TYR A 245   N  LEU A 181
SHEET    8 AA1 8 VAL A 272  PHE A 277  1  O  PHE A 277   N  THR A 248
SHEET    1 AA2 6 GLY B   3  HIS B   9  0
SHEET    2 AA2 6 TYR B  14  THR B  18 -1  O  TYR B  14   N  HIS B   9
SHEET    3 AA2 6 VAL B  25  ASN B  28 -1  O  VAL B  25   N  ILE B  17
SHEET    4 AA2 6 GLN B  59  LYS B  64  1  O  ALA B  60   N  PHE B  26
SHEET    5 AA2 6 VAL B  45  ASP B  51 -1  N  GLU B  49   O  ALA B  61
SHEET    6 AA2 6 GLY B   3  HIS B   9 -1  N  GLY B   3   O  VAL B  46
LINK         OG  SER A 155                 S   PMS A 401     1555   1555  1.48
CISPEP   1 PRO A   72    PRO A   73          0        -5.15
CISPEP   2 ALA A  116    PRO A  117          0         1.27
CISPEP   3 PHE A  121    PRO A  122          0         3.03
CISPEP   4 GLY A  173    PRO A  174          0         0.58
CRYST1   45.820   46.650  101.260  90.00  93.99  90.00 P 1 2 1       2
ORIGX1      1.000000  0.000000  0.000000        0.00000
ORIGX2      0.000000  1.000000  0.000000        0.00000
ORIGX3      0.000000  0.000000  1.000000        0.00000
SCALE1      0.021825  0.000000  0.001524        0.00000
SCALE2      0.000000  0.021436  0.000000        0.00000
SCALE3      0.000000  0.000000  0.009900        0.00000
TER    2428      ALA A 310
TER    2841      LYS B  64
MASTER      246    0    3   13   14    0    0    6 3038    2   24   30
END