Di Muccio_1987_J.Assoc.Off.Anal.Chem_70_106

Reference

Title : On-column partition cleanup of fatty extracts for organophosphate pesticide residue determination - Di Muccio_1987_J.Assoc.Off.Anal.Chem_70_106
Author(s) : Di Muccio A , Cicero AM , Camoni I , Pontecorvo D , Dommarco R
Ref : J Assoc Off Analytical Chemistry , 70 :106 , 1987
Abstract :

A fast, single-step, and efficient partition between n-hexane and acetonitrile on ready-to-use, disposable mini-columns of Kieselghur-type material has been developed for the cleanup of fatty extracts for organophosphate (OP) pesticide residue determination by gas chromatography with flame photometric detection. Nine OP pesticides (diazinon, etrimfos, chlorpyrifos-methyl, pyrimiphos-methyl, chlorpyrifos, bromophos, bromophos-ethyl, malathion, fenitrothion) most commonly used for protection of stored cereals, oil seeds, and legumes were separated from up to 2.0 g lipidic material with recoveries between 80 and 107% at spiking levels ranging for the different compounds from 0.1 to 5.0 ppm.

PubMedSearch : Di Muccio_1987_J.Assoc.Off.Anal.Chem_70_106
PubMedID: 3558258

Related information

Citations formats

Di Muccio A, Cicero AM, Camoni I, Pontecorvo D, Dommarco R (1987)
On-column partition cleanup of fatty extracts for organophosphate pesticide residue determination
J Assoc Off Analytical Chemistry 70 :106

Di Muccio A, Cicero AM, Camoni I, Pontecorvo D, Dommarco R (1987)
J Assoc Off Analytical Chemistry 70 :106